1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 31803 2012 318032012 II , 1.092 . 1.22009 . , , . , , 1 - () 2 , 3 , ( 01.10.2012 51-) : ( 3166) 004 97 ( 3166) 004 97 AZ BY KZ KG MD - RU TJ UZ 4 22308 (STM 223-08 Standard test methods for analysis of sulfuric acid). 1
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3、D 1193-06(2011) Specification for reagent water ( ) ASTM E 1-07 Specification for ASTM liquid-in-glass thermometers ( ASTM) ASTM E 60-11 Practice for analysis of metals, ores, and related materials by molecular absorption spectrometry ( , ) ASTM E 100-10 Specification for ASTM hydrometers ( ASTM) AS
4、TM E 180-03 Practice for determining the precision of ASTM methods for analysis and testing of industrial and specialty chemicals ( ASTM- )2) ASTM E 200-08 Practice for preparation, standardization, and storage of standard and reagent solutions for chemical analysis ( , ) 1) - ASTM www.astm.org : se
5、rviceastm.org. ASTM - ASTM. 2). - ASTM www.astm.org. 318032012 2 3 3.1 , , . . 4 4.1 . , , , 3). , , . 4.2 , , , II III ASTM D 1193. 5 5.1 , . . 5.2 . , . . 6 6.1 , , , ASTM E 60. 7 7.1 . 7.2 , . 7.3 - . 8 8.1 75 % (m/m) 99 % (m/m). : . 3) , , Washington, DC. , , . : AnalaR , , BDH Ltd., Poole, Dors
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7、 0,0001 . , . , . 400 , 100 . . ( 2 3). , . 3 5 . NaOH 0,5 / (N) . 0,02 . 1 , , 1. 1 H2SO4, % (m/m) , 98 1,9 2,2 94 2,0 2,3 90 2,1 2,4 85 2,2 2,6 80 2,3 2,7 77 2,4 2,8 75 2,5 2,9 2 NaOH, . , , , , , . 3 . 13.2 ( ) . 1 ( 1). , . , . , . 0,0001 . 400 , 100 . , ( 4). , 50 70 . . . 5) ASTM E 200. 318032012 5 3 5 . NaOH 0,5 / (N) . 0,02 . 4 , . 14 14.1 V t. 14.2 : N = Ns+ 0,00014(s - t), (1) N NaOH t , / (N); Ns NaOH s ,/ (N); s NaOH ; t NaOH . 14.3 , % (m/m) , : 1000,04904) ()( % , WVNm/m , (2) V NaOH, , ; N NaOH,
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