GOST 32194-2013 Feeds compound feeds Determination of organochlorine pesticides residues by gas chromatographic method《饲料 复合饲料 使用气相色谱法测定有机氯农药残留量》.pdf

1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32194null 2013 (ISO 14181:2000) , (ISO 14181:2000, MOD) 2014 32194null2013 , 1.092 . 1.22009 . -, . , , , 1 - ( ) - , 4 2 ( 004) 3 , ( 442013 14 2013 .) : ( 3166) 00497 ( 3166) 00497 AM RU UZ 4 22 - 2013 . 1885- 32194nul

2、l2013 (ISO 14181:2000) 1 2015 . 5 ISO 14181:2000 Animal feeding stuffs - Determination of residues of organochiorine pesticides nullGas chromatographic method ( . . ). ISO/TC 10 - ISO/TC 34 (ISO). (en). , , - . - . : -, , 1.52001 4.14.1. - . , , , . , , , , , . - . - . (MOD) II 32194null2013 6 - , n

3、ull . () - - . , null III 32194null2013 , 2014 -, - IV 32194null2013 , Feeds, compound feeds. Determination of organochlorine pesticides residues by gas chromatographic method null 2015null07null011 . : - ; - op-DDE; - pp-DDE; - op-DDT; - pp-DDT; - ; - ; - ; - HCB; - -HCH (-BHC); - -HCH ( -BHC); - -

4、HCH (-BHC); - - (-); - ; - ; - op-TDE (op-DDD); - pp-TDE (pp-DDD); - . : - 0,01 / op-DDT pp-DDT; - 0,05 / ; - 0,005 / . 2 : 177074 ( 104283, 478880) . -, , , . 260379 . . 416676 . . 423377 . . 5725-12003 ( ) . 1. 5725-22003 ( ) . 2. 1 32194null2013 670972 . 914780 . 929374 ( 243573) . 1202676 . 1349

5、6.080 , . 241042001 . 2533682 . , - 2922791 (IS 835-181) . . 1. 312182003 (IS 649898) , , . - , 1 , - . (), - () . , , , , . 3 , , , , - 10 %- - . 4 4.1 6709. 4.2 . 4.3 2603, . . . 4.4 . 4.5 , 10 %. 60 63 200 130 C . - , 10 %. - 30 , 30 , . 6 . 4.6 , , 20 % . 1 4 . 4.7 , , 9293, . . 4.8 4166, . 4.9

6、4233, . 4.10 : - (1R,4S,4aS,5S,8R,8aR)-1,2,3,4,10,10-1,4,4a,5,8,8a-1,4:5,8-; - op-DDE o,p- (1,1 -2,2- (4-); - pp-DDE p,p- (1,1 - -2,2- (4- ); - op-DDT o,p - (1,1,1 - -2,2- (4- ); - pp-DDT p,p-(1.1.1-2,2-bis(4- ); - (1R,4S,4aS,5R,6R,7S,8S,8aR)-1,2,3,4,10,10-1,4,4a,5,6,7,8,8a-6,7-1,4:5,8-; - (6,7,8,9,

7、10,10-1,5,5a,6,9,9a-6,9-2,4,3- 3-); 2 32194null2013 - (1R,4S,4aS,5S,6S,7R,8R,8aR)-1,2,3,4,10.10- -1,4,4a,5,6,7,8,8a-6,7-1,4:5,8- ; - HCB (); - -HCH ( -BHC) (-1,2,3,4,5,6- ); - -HCH ( -BHC) ( -1,2,3,4,5,6- ); - -HCH ( -; ) ( -1,2,3,4,5,6- ); - -HCH ( -BHC) ( -1,2,3,4,5,6- ); - (1,4.5,6,7,8,8- -3a,4,7

8、,7 -4,7-); - (-); - p-TDE (p-DDD) o,p-1,1-2,2- (4-); - pp-TDE (pp-DDD) p,p-1,1-2,2-bis (4-); - 1,1,1-2,2-(4-) . 4.11 : (1,3,5 ) . 4.12 4.12.1 1000 /3 (. 5.10) 0,1 , (. 4.10) (. 4.11), - 1000 /3. . , , , . - . -HCH, . 4 C 6 . 4.12.2 10 /3 (. 5.13) 1 3 (. 4.12.1) 100 3 (. 5.11). . 4 C 3 . -. , 15 18 C

9、, - 1 /3 3 18 C. . - () - . 20 C. , . ( ) 10 % - , . , 3 ( , 25 3). , ( 2 3) 4 C 3 . 4.12.3 0,5 /3 (. 5.13) 5 3 (. 4.12.2) 100 3(. 5.11) . 4 C 1 . (. 4.12.2). , - , , , , . - , . - - . -. . 3 32194null2013 5 , 5.1 , 500 3 - (PTFE). 5.2 1(2)-500 25336. 5.3 3 9147. 5.4 10 3, (PTFE). 5.5 , 300 , 810 , P 100 ( 40100 ) 1 . 5.6 , -1(2)-100(500)-19/26(29/32, 34/36)- 25336 (40 2) C. 5.7 . 5.8 , : - ; - ; -