GOST 32587-2013 Grain and products of its processing mixed feeds Determination of ochratoxin A by high performance liquid chromatography《粮食和粮食加工产品和混合饲料 用高性能液相色谱法对赭曲霉毒素A含量的测定》.pdf

1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32587 2013 , (ISO 15141-1:1998, NEQ) 2014 325872013 II , 1.0 92 . - 1.2 2009 . -, . -, , , 1 - ( -) 2 ( 335) 3 , ( 14 2013 . 44-2013) : ( 3166) 00497 ( 3166) 00497 BY KG RU TJ 4 ISO 15141-1:1998 Foodstuffs Determination

2、of ochratoxin A in cereals and cereal products Part 1: High per-formance liquid chromatographic method with silica gel clean up ( . - . 1. - ). (NEQ) 5 30 - 2013 . 2429- 325872013 - 1 2015 . 6 - , . () - - . , . , 2014 -, - . 325872013 1 , Grain and products of its processing, mixed feeds. Determina

3、tion of ochratoxin A by high performance liquid chromatography 20150701 1 ( ) : - ( ) - , - , , , , , (, ) 0,0025 1,0 -1; - ( ) - 0,0004 -1. 1 -1 1 / 1000 /. 2 : 12.1.00491 . . 12.1.00776 . - 12.1.01076 . . - 12.1.01979 . . 6175 . 177074 ( 104283, 478880) . -, , , . 260379 . . 311877 . . ISO 3696201

4、3 . 416676 . . 420477 . . 420977 . 6-. 555681 . 5725-22003 ( ) . 2. 5725-62003 ( ) . 6. 578978 . . 584873 . . 670972 . 699577 . -. 929374 . 996886 . 13586.383 . 325872013 2 1631787 . / 170252009 - 2001588 . 2533682 . . - 26312.184 . 2766888 . 2831189 . - 2922791 ( 835-181) . . 1. OIML R 76-1-2011 .

5、. 1. . - , - 1 , - . (), - () . , , , - , . 3 13586.3, 26312.1, 27668. 100 , - , 1 . . . 4 : - 12.1.019 -; - 12.1.010; - 12.1.004; - 12.1.007. - . , - , - , . , - , 4 %- . 5 5.1 , , , - - . 5.2 , , , -, 5.2.1 -, (330 20) - 325872013 3 (465 20) . - 5 /35.2.2 OIML R 76-1-2011 c 0,01 . 5.2.3 , - - 5 ,

6、5000 - .5.2.4 - , . 5.2.5 200 10 . 5.2.6 , 1 , - . 5.2.7 -12 , 20 50 . 5.2.8 (), 120 -1. 5.2.9 , 25336, - 2,5 10 . 5.2.10 , 200 . 5.2.11 16317. 5.2.12 - 50 /3 2,5 /3. , - 5.3.3.1. 5.2.13 6709 1 ISO 3696. 5.2.14 4166, . 5.2.15 61, . 5.2.16 , - 200 0,025, 0,03 %. 5.2.17 , . . 5.2.18 20015, . 5.2.19 58

7、48, . 5.2.20 4204, . . . 5.2.21 9293. 5.2.22 1 - 3 1(1) 2(2) 2- 1, 2, 5 3 29227. 5.2.23 1 - 4 2- 25, 50, 250 3 1770. 5.2.24 2-25-2, 2-50-2, 2-100-2, 2-500-2 1770. 5.2.25 -10-14/23 -50-14/23 25336. 5.2.26 -1 -1 50, 100, 250 3 25336. 5.2.27 100 1000 3 - 28311. 5.2.28 25336. 5.2.29 -1-50 -1-50 25336. 5

8、.2.30 ( ) 1,5 3. 5.2.31 50, 250, 1000 3 , . 5.2.32 1,0 . 5.2.33 . 5.2.34 . 5.2.35 . , 2,1 120 , - -18 5 , 25 . - . 325872013 4 5.2.36 5556. 5.2.37 100 200 . - . 5.3 5.3.1 5.2.20 ( ), . , 105 . 5.3.2 5.3.2.1 500 3 -, 5 3 (. 5.2.15), 215 3 (. 5.2.16) . - . . 1 . 5.3.2.2 1 % 250 3 200 3 2 3 (. 5.2.15) . - , 1 . 5.3.2.3