GOST 32712-2014 Juice products Determination of fumaric acid by high performance liquid chromatography《果汁产品 采用高效液相色谱法测定反丁烯二酸》.pdf

1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32712 2014 2014 327122014 II , - 1.092 . 1.22009 . -, . , , , 1 () 2 3 , (- 25 2014 . 45) : ( 3166) 00497 ( 3166) 00497 AM BY KZ KG RU TJ UZ UA 4 1 2014 . 851- 327122014 - 1 2016 . 5 - (International Federation of Fruit

2、Juice Produces) IFUMA72 (1998) Fumaric acid (HPL) ( 72 (1998) - ) 6 54685 2011 7 - , . () - - . , , 2014 -, - 327122014 1 Juice products. Determination of fumaric acid by high performance liquid chromatography 2016 01 01 1 , , - , , , , ( ), - () ( ) - . ( ) 1 /3(1) 50 /3 (1) .2 - : 12.1.00776 . . -

3、 12.1.01979 . . - 1 OIML R 76-12011 . - . 1. . 177074 ( 104283, 478880) . -, , , . 36962013 . -2 420477 . . 5725-12003 ( ) -. 1. 5725-22003 ( ) -. 2. 5725-62003 ( ) -. 6. / 170252009 - 2533682 . , 2631384 . , 1 12.1.0192009 . . . 2 525012005 . . 327122014 2 2667185 , -. 2922791 ( 835-181) . . 1. 316

4、432012 . - - , 1 , - . (), - () . , , , , . 3 - () , - . - 210 . 4 26313, 26671, 31643 ( 6.2). 5 , , , 5.1 ( 200 600 ) 10 3 - , 1, - 1 300 7,8 , - , 30 4,6 , , - . 1 - , %, - - - - , , - - - - - - 1,0, . . ., - - - 1,0, . . ., 8 - 0,2 0,003 0,0008 5,0 5,0 2,5 5,0 1 Aminex HPX-87H . . 327122014 3 5.4

5、 OIML R 76-1 150 - 0,001 . 5.5 : - 1-50-2 1-1000-2 1770; - 2-50-2, 2-500-2 2-1000-2 1770; - 1-10-0,1 1-20-0,1 1770; - 1-2-2-1, 1-2-2-2, 1-2-2-5 1-2-2-10 29227. 5.7 25336: - ; - -1-50, -1-100 -1-1000. 5.8 0,45 . 5.9 , 1000 g, . 5.10 . 5.11 . 5.12 () , . 5.13 . 5.14 3696, 2- . 5.15 H4C4O4, 99,5 %. 5.1

6、6 4204, . . , , - , , - , . 6 6.1 , - . . 6.2 : - , 25 5; - , 97 10; - , % 40 80; - , 220 20; - , 50 1. , , - . . 6.3 0,005 /3 1000 3 100200 3 - 0,25 3 , , - . . 7 . 327122014 4 6.4 6.4.1 100 /30,05 , - 500 3, 2/3 . -, . 4 6 .6.4.2 100 /3 1,0 10,0 /3. 50 3 0,5; 1,0; 3,0; 4,0;5,0 3 , . -. 7 7.1 : - , 40 5; - , 3 20;- 6.3; - ; - , 3/ 0,6. . 7.2 . 7.2.1 , 6.4.2, - . 5725-1 ( 3.14) 5725-2. 7.2.2 - Si, . . , - C,i, /3, , iC k S , (1) k ( ), /3 (. . )1, , - , (2) Si i- , . . ; C,i i- , /3;i ; 327122014 5 m . , , - ,