1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32799 2014 2014 327992014 II , - 1.092 . 1.22009 . -, . , , , 1 () 2 3 , ( 25 2014 . 45) : ( 3166) 00497 ( 3166) 00497 AM BY KZ KG RU TJ 4 1 2014 . 854- 327992014 - 1 2016 . 5 - (International Federation of Fruit Juice P
2、roduces) IFUMA57 (1989) (Rev. 2005) Determination of free amino acids ( 57:1989 (Rev. 2005) ). 6 54743 2011 7 - , . () - - . , , 2014 -, - 327992014 1 Juice products. Determination of free amino acids by ion-exchange chromatography 2016 01 01 1 , , - , , , - , - ( ) : , , , , , , -, , , , , , , , ,
3、, , , , . . () 1 /3 (1 /3). () 5000 /3 (5000 /3). . 2 - : 12.1.00776 . . - 12.1.01979*1 . . 6175 . . OIML R 76-12011 . - . 1. . 19978 . 3-. 177074 ( 104283, 478880) . -, , , . 311877 . . ISO 36962013* . - 5725-12003 ( ) -. 1. 5725-62003 ( ) -. 6. 582078 . . 924579 . 965675 . . 1131176 . *1 12.1.0192
4、009 - . . . *1 525012005 -. . 327992014 2 1202676 . / 170252009 - 2228076 . 5,5-. 2533682 . , 2631384 . , 2667185 , -. . 2922791 ( 835-181) . . 1. 316432012 . - - , 1 , - . (), - () . , , , , . 3 - . 100 135 . , , - 570 440 . 4 , , , 4.1 *1, :- ; - ; - 570 440 15 3, - 1 ; - - ; - ( ): 9 x 500 , 6 x
5、200 , 4,6 x 200 270 , 4 x 200 , 3.2 x 140 , - , * 2 2,0 7,0 . . 4.2 4.3 OIML R 76-1 (I) 150 - 0,005 . 4.4 25336: - -2-1000-34; - ; *1 Biochrom 30+ - . . *2 Biotronik BTC 3118 LKB Ultropac 8 - . . 327992014 3 - . 4.5 1 % 29227 1- 1 % -. 4.6 25, 100 250 3 1 %. 4.7 1770: - 1-50-2 1-1000-2; - 2-25-2, 2-
6、50-2, 2-100-2, 2-500-2 2-1000-2; - 1-25-0,1. 4.8 26 3.4.9 0,22 0,45 . 4.10 . 4.11 1000 g . 4.12 -. 4.13 (pH-) 9245 0,05 . pH, - . 4.14 . 4.15 12026. 4.16 *1 4- Li3C6H5O7 4H2O, 98 %. 4.17 *, 98 %.4.18 * 98 %.4.19 11311, 99 %. 4.20 3118, . . 4.21 ( ), C4H10O2 , - 99,8 % nD 1,4071,408. 4.22 , . . 9656.
7、 4.23 58H118O24, 1,03 /3 (CAS No9002-92-0), 30 %. 4.24 2,2-, 99 %. 4.25 (2,2-1,3-), 95 %. 4.26 3- 199 ( 5820), . . . 4.27 61, . . 4.28 (III) 6- TiCl3 6H2O, 15 % , . 4.29 2- C18H10O6, 98 %. 4.30 ( ) 22280, . . . 4.31 , 98 %. 4.32 , 99 %. 4.33 ISO 3696, 1- . 4.34 - ( DL- L- ): -, , , , , , , , , , , , , , , , , , , , - 98 %. , , - , , -, , - . *1 . 327992014 4 5 26313, 26671. - 31643 ( 6.2). 6 , . 6.1 , - 4.2, 2,2, 2,8, 3,0, 3,15, 3,50, 3,55 6 . . 2,2, 2,8, 3,0, 3,15, 3,50, 3,55 6 . 4.164.18 . , - -. 0,01 % (. 4.19) 2,2- (. 4.24). - . 6.2 () , - 4.1. - 4.254.30 - . . 6.3
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