GOST 32982-2014 Solid mineral fuel Determination of total fluorine content《固体矿物燃料 氟总含量的测定》.pdf

1、 (ISO 11724:2004, MOD) , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)329822014(ISO 11724:2004), 1.092 . 1.22009 . , - . , , -, 1 - , , () -, 52 ()3 , (- 20 2014 . 71-) : ( 3166) 00497 ( 3166) 00497 BYKGRUTJ 4 15 2015 . 255- 329822014 (ISO 11724:2004) 1 2016 .5 ISO 11724

2、:2004 Solid mineral fuels Determination of total fluorine in coal, coke and fly ash ( - . , ). , - / , . ISO/C 27 . (en). , - , - . , -, . (MOD)6 II 329822014 -, - . () . , - - , 2015 -, III 329822014:- ;- 6;- 7.5.3 8.3, , . .IV 329822014 Solid mineral fuel. Determination of total fluorine content 2

3、01604011 , , - , , , , ( ) ( ), , - . 0,001 % 0,1 % ( 10 1000 /). . , , - .2 : 6175 . . OIML R 76-12011 . . 1. . 8379 . . ISO 6872012 . . 1) 177074 (O 104283, O 478880) ., , , . 311778 . . 311877 . . 420179 . . 421777 . . 432877 . . 446177 . . 446376 . . ISO 5068-22012 . . 2. - 2)1) 2758991 ( 68774)

4、 . - .2) 529172008 ( 11722:1999, 5068-2:2007) . .1 329822014(ISO 11724:2004) 558378 ( 204673) . - ISO 5725-62003 ( ) . 6. 1) 661694 . 670972 . 2) 1074271 , , , . ISO 117222012 . . 3) 1386768 . 2308378 , . - 2533682 . , - 2731395 ( 117077) . 4) - - - , 1 , . (), (-) . , , , , .3 - 1200 C . - () ().4

5、, . . . 13867.4.1 67095).4.2 , 75 , 1000 C 1 . .4.3 , , 99,5 % 5583. , , .2 3298220141) 5725-62002 ( ) . 6. .2) 525012005 ( 3696:1987) - . .3) 529172008 ( 11722:1999, 5068-2:2007) . .4) , 01.07.2012 542452010 ( 1170:2008) . - .5) 2- 52501. . 52501 2- .4.4 (NaF) 4463.4.5 (4.4), 110 C 1. (0,2210 c177

6、0,0002) 400 3 (4.1) , (4.1) (500,0 c177 0,5) . 200 /. (5.2).4.6 (NaOH) 4328.4.7 , 0,025 /3: 2,0 (4.6) 500 3 (4.1), 2,5 3, (4.1) 2000 . (5.2).4.8 (NaHCO3) 4201.4.9 (Na2CO3) () 83.4.10 : 0,300 (4.8) 1,120 (4.9) 500 3 (4.1) 2 3. (5.2).4.11 (KNO3) 4217.4.12 61.4.13 () 3117.4.14 1,2- (CDTA).4.15 ( 6,5) 1

7、0,0 (4.11), 5,0 1,2- - (4.14) 115 (4.13) 350 3 (4.1). 6,5 (4.12).(4.1)500. (5.2).4.16 20 (4.1), 20 (4.7) 10 (4.15) (5.4). 200 - (4.5) .4.17 (Hl), , c11420= 1,19 /3 3118.4.18 , 10 %: 100 3 (4.17) - (4.1) 1 3.4.19 (HNO3), , c11420= 1,42 /3 4461.4.20 , 10 %: 100 3 (4.19) (4.1) 1 3.5 5.1 : , , , . 1770 25336.5.2 , , - , (4.1), - (4.5, 4.7, 4.10, 4.15). (4.20) (4.18) 24 . (4.1).5.3 10 30 3 - .5.4 , , 125 3, , , .5.5 , 1 3.3 329822014 - 125 3(5.4), - (4.5).5.6 OIML R 76-1:- c1770,1 ;- 200 c1770,001 .5.7 OIML R 76-1:- 600 c1770,01 ;- 3000 c1770,1 .5.8 () 1200 C 6616 . 10 C .5.9 ( 1)