1、 549042012 , , , - 1 ( )2 335 - 3 17 2012 . 71-4 1.02012 ( 8). ( 1 ) , -.()- . , - (gost.ru) , 2013 , - - II 5490420121 .12 13 .24 .25 , , , .26 56.1 56.2 .56.3 .66.4 .87 97.1 97.2 107.3 107.4 118 118.1 / .118.2 .119 .1110 .1211 1312 .1412.1 .1412.2 .1413 14 () 1515III 549042012 , , , - Food product
2、s, food raw materials.Method for determination of sulfonamides, nitroimidazoles, penicillins, amphenicols by high performance liquidchromatography mass spectrometry 201307011 , -, , , , , , , - - , , , . 0,2 1000 /, 1,0 1000,0 /.2 : 5725-62002 ( ) . 6. 12.1.0192009 . . 5144799 ( 3100-191) . 52121200
3、3 . 532282008 . 1. . 535972009 , . 536692009 . 12.1.00588 . - 12.1.00776 . . 12.2.0852002 , . . - 177074 ( 104283, 478880) ., , , . 584873 . . 1386768 . 1 549042012 197922001 . 2680986 . , 313392006 , . - - - , 1 , . - , , (). - , , , , - , . , , , , .3 3.1 , , , - (-/).3.2 , , - .3.3 .4 :- (20c177
4、10) ;- .(90c177 16) ;- .(220c177 20) ;- .(50c177 1) ;- (55c177 25) %. , .5 , , , 5.1 , , -, , -:- -, 50 500 (. . .), 500, 0,1 . . ., - ( /);- , , , 50 ;- - ;- 53228, - c177 0,01 c177 1,00 ;2 549042012- 110, 10100, 2001000 3 - , c177 2 % (Transferpettor Brand,)*;- 50 ;- - ;- - 3 150 2500 /;- 5000 / 4
5、 20 , 15 3 1,5 3;- 20 1 3;- - 150 3,5 ;- ;- 12 3, - 50 ;- 15 3 - ;- 0,2 ;- () 2 3 - 9 ;- -2-10-14/23 1770;- 2-100-2, 2-1000-2 1770.5.2 , , -, :- , . .;-,.;- 5848, . . .;-,.;- . 2 (. .) 3 (. . .) 13867.5.3 , , -, :5.3.1 :- 99,0 % (HPLC, Sigma)*;- 99,0 % (HPLC, Sigma)*;- 99,0 % (HPLC, Sigma)*;- 95,0 %
6、 (HPLC,Sigma)*;- 99 % (HPLC, Sigma)*;- 99,5 % (HPLC, Sigma)*;- 99,9 % (HPLC, Sigma)*;- 99,0 % (HPLC,Sigma)*;- 99,1 % (HPLC, Fluka)*;- 99,1 % (HPLC, Sigma)*;- 99,5 %, (Fluka)*;- 99,9 % (HPLC, Sigma)*;- 99,8 % (HPLC,Sigma)*;- 99,2 % (HPLC, Sigma)*;- 99,9 % (HPLC, Sigma)*.* . - .* . .3 5490420125.3.2 :
7、- 99,9 % (HPLC, Witega)*;- 99,9 % (HPLC, Witega)*;- 99,5 % (HPLC, Witega)*;- 99,5 % (HPLC, Witega)*;- 99,0 % (HPLC, Witega)*;- 99,0 % (HPLC, Witega)*;- 99,0 % (HPLC,Witega)*;- 99,0 % (HPLC, Sigma)*;- 99,0 % (HPLC, Witega)*.5.3.3 :- 99,3 % (HPLC, Riedel-de Haen)*;- 98,7 % (HPLC, Riedel-deHaen)*;- 98,
8、1 % (HPLC,Riedel-de Haen)*;- 98,5 % (HPLC,Riedel-de Haen)*;- , 99,8 % (HPLC, Riedel-deHaen)*;- 99,7%(HPLC,Riedel-deHaen)*;- 99,7 % (HPLC, Riedel-deHaen)*.5.3.4 :- 99,1 % (HPLC, Sigma)*;- 99,3 % (KRKA)*;- 99,37%(HPLC,LaboratoriosHIPRA)*.5.3.5 :-4 99 % (Isotopic purity, TRC)*;- -4 99 % (Isotopic purity, TRC)*;- -4 99 % (Isotopic purity, TRC)*;-4 99 % (Isotopic purity, TRC)*;-9 99 % (Isotopic purity, TRC)*;- -4 99 % (Isotopic purity, TRC)*.5.3.6 :- -3 99,8 % (HPLC, Witega)*;- -3 99,5 % (HPLC, Witega)*;- -3 99,0 % (HPLC, Witega)*;- -D3 99,5 % (HPLC, Witega)*;- -3 99,0 % (HPLC, Witega)*;-
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