1、 608142013 . , IEC 60814:1997Insulating liquids Oil-impregnated paper and pressboard Determination ofwater by automatic coulometric Karl Fisher titration(IDT) 1 - , , ( ) 4, 2 3 5 2013 . 4-4 60814:1997 . , . - (I 60814:1997 Insulating liquids Oil-impregnated paper and pressboard Determination of wat
2、er by automatic coulometric Karl Fishertitration). - - , 5 1.02012 ( 8). ( 1 ) , -. () . , - - (gost.ru) , 2014 , - - II 6081420131 .11.1 .11.2 .12 .22.1 .22.2 .22.3 22.4 42.5 52.6 .52.7 52.8 52.9 .62.10 .63 .63.1 .63.2 .63.3 .63.4 73.5 83.6 .84 , .84.1 .84.2 .94.3 .104.4 11 () , .12 () ( ) .14III 6
3、08142013 . , Insulating liquids. Oil-impregnated paper and pressboard. Determination of waterby automatic coulometric Karl Fisher titration 201401011 1.1 - ( ) - . 2 - 2 /, 100 2/ 40 . 3 , -, , 100 2/. 4 - 0,1 % . 20 % .1.2 -: 60475:1974 (IEC 60475, Method of sampling liquiddielectrics)* 60567:1992
4、- (IEC 567, Guid for the sampling of gases and ofoil from oil-filled electrical equipment and for analysis of free and dissolved gases)* 595-1:1986 -. 1. (ISO 595-1:1986, Reusable all-glass or metal-and-glass syringes for medicaluse Part 1: Dimensions) 595-2:1987 -. 2. , (ISO 595-2:1987,Reusable all
5、-glass or metal-and-glass syringes for medical use Part 2: Design, performance requirementsand tests)* 60475:2011 (IEC 60475:2011, Method ofsampling insulating liquids).* 60567:2011 . - . (IEC 60567:2011, Oil-filled electrical equipment Sampling ofgases and of oil for analysis of free and dissolved
6、gases Guidance).1 608142013 2 2.1 2 /, 100 2/ 40 . , 2.10, .1 , , .2 . , , , .2.2 , , . , - , , , . , :H2O+I2+SO2+3C5H5N c174 2C5H5N c215 HI+C5H5N c215 SO3; (1)C5H5N c215 SO3+CH3OH c174 C5H5NH c215 SO4c215 CH3. (2) -, - . -, . (1) (2). , , 2I2ec174 I2. (3) , (1), 1 10,72 . , .2.3 2.3.1 , - . () ( ),
7、 ( ) ( ). . ., , (3), (1) (2). - , . , /, . , , - .2.3.2 - . .- 1 , .2 6081420132.3.2.1 2. - , . :- b ( ); ( );b ; ;d ; - ( ); f - ; g ; h 2 3 6081420131 ; 2 ; 3 ; 4 ();5 , ; 6 ; 7 1 - - d, , ;- ( ) , , . , , - , ;- : f;- g;-h ;- . . 2.4.2, d). , - .2.3.2.2 ( ) , - .2.3.2.3 .2.3.2.4 .2.3.2.5 .2.3.2.6 , , (), - . .2.3.2.7 , , - ( , ).2.4 - .2.4.1 , , - . , . - , - , . , . - .2.4.2 ) . , 20 /3.b) , .) . .4 608142013d) . 10 5 3 595-1 595-2 . 100 1 . .2.5 , - .2.6 , .2.6.1 -
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