1、2014 13 () - / ( / ) ( ). ISO 16000-13:2008 Indoor air Part 13: Determination of total (gas and particle phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins / dibenzofurans (PCDDs / PCDFs) Collection on sorbent backed filters (IDT) 16000-13 2012 16000-132012II1
2、- ( ) , 42 457 3 - 23 2012 . 1155-4 16000-13:2008 - . 13. - () - / ( / ) ( ). (ISO 16000-13:2008 Indoor air Part 13: Determination of total (gas and particle phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins / dibenzofurans (PCDDs / PCDFs), Collection on sorbe
3、nt backed filters) - , 5 1.02012 ( 8). - ( 1 - ) , -. () - . , - (gost.ru) , 2014 , - - 16000-132012III1 12 13 .24 35 .36 47 .88 99 11 () .12 () .20 () , 21 () .26 27 16000-132012IV 16000 , - , - , . - (), - () - () . - (), . , 12884, - . , / - 16000-12. / . - 209 (), 75 135 . - , . -2,3,7,8- (2,3,7
4、,8-). , ; . / , , (), -, . - / . (. . : -28, -52, -101, -138, -153 -180, 5) 10 ( / 3). / , - , ; ( / 3) ( / 3). / - , , , , . , 108, - . - . , - - - . / - . , . - . - () - / ( / ). / , 16000-14. 16000-132012 1 201312011 (), - () () (. 1). - / . - / , - . , 16000-14 ( 16000-13 16000-14 / ). , 16000-1
5、4, - - ( / ), / 0,2 / 3 . 0,2 / 3 , . - 50 3. 360 3( 24 16 3/ 7 - 2 3/ ). . 1000 3. , , 25 % , 50 % . -, .2 : 12884 . - ( ). - (ISO 12884, Ambient air Determination of total (gas- and particle-phase) polycyclic aromatic hydrocarbons Collection on sorbent-backed filters with gas chromatographic / mas
6、s spectrometric analyses) 13 () - / ( / ) ( ). Indoor air. Part 13: Determination of total polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins / dibenzofurans (PCDDs / PCDFs) (gas and particle phase). Collection on sorbent backed filters 16000-1320122 16000-12 . 12. -
7、(), - (), - () () ISO 16000-12, Indoor air Part12: Sampling strategy for polychlorinated biphenyls (PCBs), polychlorinated dibenzo-p-dioxins (PCDDs),polychlorinated dibenzofurans (PCDF) and polycyclic aromatic hydrocarbons 16000-14 . 14. - () - / ( / ) ( )., - - ISO 16000-14, Indoor air Part 14: Det
8、ermination of total (gas and particle-phase) polychlorinateddioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins / dibenzofurans (PCDDs / PCDFs) Ex-traction, clean-up and analysis by high-resolution gas chromatography and mass spectrometry3 :3.1 ES(sampling efficiency): , . ES , %, , ,
9、 , - .3.2 Er (dynamic retention efficiency): - , , , , , - , .3.3 Er(dioxin-like PCB): - - , - (Ah) , , 2,3,7,8- / , 1). 1 . 5.2 . .1 .2.3.4 (marker PCB): . PCB-28, -52, -101, -138, -153 -180.3.5 (spiking): , 1312.3.6 (operational performance characteristic): , - . , , , - , 1.3.7 (field blank): - ( , () ), , , , - . , - , , - , .3.8 (analytical blank): , -1) . 16000-1320123 , , , .3.9 (sampling standard): , -
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