KS H ISO TR 22305-2007 Cigarettes-Measurement of nicotine-free dry particulate matter nicotine water and carbon monoxide in cigarette smoke-Analysis of data from collaborative studlity.pdf

1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS H ISO/TR 22305 (NFDPM), , , KS H ISO/TR 22305 ：2007 (2012 ) 2007 11 1 http:/www.kats.go.krKS H ISO/TR 22305：2007 : ( ) ( ) () () () ( ) () KT&G ( ) KT&G ( ) KT&G : (http:/www.standard.go.kr) ： ：2007 11 1 ：2012 12 28 20120807 ： ： (ISO/TC126) ( 02-509-7270

2、) (http:/www.kats.go.kr). 10 5 , . KS H ISO/TR 22305：2007 . iii iv 1 1 2 (r), (R) 1 2.1 (r), (R) 1 2.2 .2 3 .4 3.1 4 3.2 .4 4 2003 CORESTA .5 4.1 .5 4.2 CCS-03 (r ) 5 20 4.3 CCS-03 (R ) .5 20 4.4 R .6 100 5 7 5.1 .7 5.2 .7 5.3 .7 5.4 8 5.5 .9 6 9 7 9 A() .33 A.1 .33 A.2 .33 A.3 .34 B() .35 B.1 .35 B

3、.2 .35 B.3 .36 B.4 .36 B.5 .37 B.6 .38 C() (2002 3 ).43 C.1 43 C.2 .43 i KS H ISO/TR 22305：2007 C.3 45 C.4 45 C.5 48 C.6 / .49 C.7 49 D() .61 E() 11 2002/2003 .73 E.1 .73 E.2 .74 E.3 76 E.4 77 E.5 80 F() 2003 CORESTA ISO NFDPM, , CORESTA , 2003 9 .87 F.1 .87 F.2 .88 F.3 .88 F.4 CORESTA 90 F.5 .93 F.

4、6 .93 F.7 .98 F.8 CORESTA 98 148 ii KS H ISO/TR 22305：2007 ISO(the International Organization for Standardization) (ISO ) . ISO . . ISO . ISO (IEC) . ISO/IEC , 2 . . . 75 % . ( “ ”) , (Technical Report) . , . . ISO . ISO/TR 22305 ISO/TC 126, . iii KS H ISO/TR 22305：2007 2006 1 ISO/TR 22305, Cigarett

5、esMeasurement of nicotine-free dry particulate matter, nicotine, water and carbon monoxide in cigarette smokeAnalysis of data from collaborative studies reporting relationships between repeatability, reproducibility and tolerances , . 0.1 ISO/TC 126/WG 8 “ ” , . nicotine-free dry particulate matter(

6、NFDPM, ), . . , . . , . (r 20 ) 1) (R 20 ) 2 ) (Confidence Intervals：CIs) . r R , . 2003 CORESTA Study . , . , . R 20 r 20 (CIs) 3) . 4 ) . . 100 . , . 1) 20 . 2) 20 . 3) KS H ISO 8243 NFDPM 2003 , ISO/TC 126/WG 8 . 4) KS H ISO 4387 KS H ISO 8243 iv KS H ISO/TR 22305：2007 , R 100rndg 5) . R 100rndg

7、, . NFDPM , . CORESTA 2003 Study R 100rndg . KS H ISO 8243 6) . . 1.5 mg 20 % R 100rndg 1 mg 25 % R 100rndgratio 1.5 mg 22 % (CO/NFDPM) 20 %, 25 % 1.5 mg . KS H ISO 8243 . . . 0.2 ISO (r) (R) . KS A ISO 57251 1 KS A ISO 57252 2 . . () ( ) . , . . , ( ) , . 5) 100 . 6) NFDPM 15 %, 20 %. NFDPM 20 %, 2

8、5 % . NFDPM 1 mg, 0.1 mg. v KS H ISO/TR 22305：2007 vi . 3 , 4,5 , 6 , 7,8 9 ISO . ( A ) . . . . r R . , . 0.3 KS H ISO 8243 10 . . EU (Directive 2001/37/EC) . ISO/TC 126 2003 WG 8 1991 , . KS H ISO 8243 2003 . NFDPM . , , ISO . (NFDPM), . 0.4 KS H ISO 3308 . ISO ( B, C, D ) NFDPM ( ). CORESTA 7) . (

9、 KS H ISO 3308 ) , . CORESTA 2003 , F . 7) KS H ISO/TR 22305：2007 (2012 ) (NFDPM), , , CigarettesMeasurement of nicotine-free dry particulate matter, nicotine, water and carbon monoxide in cigarette smoke Analysis of data from collaborative studies reporting relationships between repeatability, repr

10、oducibility and tolerances 1 KS H ISO 8243 (CO) . 2 (r), (R) 2.1 (r), (R) KS A ISO 57251 KS A ISO 57252 r R . , (KS A ISO 57251：2002 6.3.4 r R 8 15 ), ISO ( . KS A ISO 57251：2002 6.4.2) (KS A ISO 57251：2002 6.4.1 5 ). ISO r R . NFDPM(KS H ISO 4387), (KS H ISO 10315), (KS H ISO 8454) r R . r2.8* s wK

11、S H ISO/TR 22305：2007 R2.8*s b 2 s w 2 s w 20 , r (20 ) 95 % , . s b , R (, 20 ) 95 % , . , , 20. 1 4 5 . , 1 . 20 r 20 R 20 . s b s w , . , r R . KS A ISO 57252：2002 . . 7.2.5 KS A ISO 5725 . . . r R . R . , , 2 3 . 2.2 r 20 R 20 95 % NFDPM . . NFDPM , (, ) . , 0.5 0.5 ( - ). NFDPM 0.083 , 0.000 83

12、 2 KS H ISO/TR 22305：2007 . . r 20 R 20 . , , 12 , KS H ISO 8243 . 3.2 4.4 C . C , NFDPM . , 95 % , . 95 % CI22(Ps w 2 )/5s b 2 P L Rounding 1/2 (1) P ： s b 2：s P L： s w 2：20 Rounding . ( ) ( ) 100 , 5 20 . (1) 100 R 100 . R 100 22s w 2 /5s b 2 1/2 (2) (2) R 100 ( 4 5) R 100rndg ( 6 7) . , . . (1) . . , 95 % . P( ) 5 (, ). 3 KS H ISO/TR 22305：2007 3 3.1 r R . ( KS A ISO/IEC 17025 ) D . 2003 CORESTA (CCS-03) . CORESTA Analytical Methods Group(CAMG) COTESTA Asia Collaborative Study(ACS) 5 . 1 , CORESTA Collaborative Study ( F). 1 KS H ISO 4387：2007, KS H ISO 10315：2007, KS H ISO 8