1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS I ISO 16144 SRM 2806 KS I ISO 16144 :2009 2009 12 18 http:/www.kats.go.krKS I ISO 16144:2009 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : :2005 12 14 :2009 12 18 2009-0830 : : ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS I ISO 16144:2009 i ii .1 1
2、1 2 .1 2.1 1 2.2 2 2.3 .2 2.4 .2 2.5 SEM .3 3 .3 3.1 .3 3.2 .4 3.3 .5 3.4 SRM 2806 .7 4 .7 4.1 SRM 28067 4.2 7 4.3 7 5 11 18 KS I ISO 16144:2009 ii APC( ) . ISO 44021 30 . ISO 4402:1991 General Motors 社 ACF TD( ). ACFTD : ACFTD :18 0 m ( )2345 ACFTD , ( 10 m) . ISO 4402 ACFTD 10 m . , ACFTD . (SRM)6
3、 ( ) , 7. KS I ISO 16144:2009 SRM 2806 Hydraulic fluid powerCalibration of liquid automatic particle countersProcedures used to certify the standard reference material SRM 2806 2002 1 ISO/TR 16144, Hydraulic fluid powerCalibration of liquid automatic particle countersProcedures used to certify the s
4、tandard reference material SRM 2806 , . 1 1 SRM 2806 NIST(National Institute of Standards) . SRM 2806 SEM( ) (a number size distribution) ISO MTD(Medium Test Dust). SRM 2806 MIL H5606 ISO MTD . 2 2.1 2.1.1 SRM 2806 . . , KS R ISO 121031 8. SRM 2806 ISO 12103A3 ISO MTD , (batch No.) 4390C. 2.1.2 RM 8
5、631 RM 8632 RM 8631 RM 8632 ISO MTD( No. 4390C) ISO UFTD(ultra fime test dust)(KS I ISO 16144:2009 2 No. 4476J) . KS B ISO 111719 SRM 280610 RM . 3.6 kg RM , 20 mg 147 . . 2.2 ISO MTD . MILH 5606, AIR 3520, NATO H 515 . KS B ISO 1688911 A . (1 500100) pS/m (50 g/g) . 2.3 SRM 2806(400 mL ) , . , , .
6、KS B ISO 1194312 . , 3.1.2 . 1 . 1 (200 L) 2 3 4 1 2.4 KS I ISO 16144:2009 3 KS I ISO 440513 KS M ISO 4407_200114 0.2 m, 25 mm (polycarbonate) . 2.5 SEM SEM JEOL 840. , MicroVax LISPIX . NIST . LISPIX . 3 3.1 3.1.1 , , NIST . NIST . 3.1.2 / NIST . 4 (a, b, c, d) . 320 , 1(a, b, c, d), 2(a, b, c, d),
7、 , 80(a, b, c, d) . ISO 4402:1991 (APC) NIST . 4 (a, b, c, d) 5 %, 30 %, 60 %, 95 % 4 . 4 4 . , 5a, 5b, 5c, 5d, 25(a, b, c, d), 50(a, b, c, d), 75(a, b, c, d) 16 , 6(a, b, c, d), 26(a, b, c, d), 51(a, b, c, d) 76(a, b, c, d) . 3 96 . 320 . 5 m, 7 m, 10 m, 20 m, 30 m 4 %, 4 %, 4 %, 5 %, 7 % , . . 18
8、0 m , . 3.1.3 . . SRM 1 . 2 . . KS I ISO 16144:2009 4 1 m % 5 1.1 10 1.3 15 2.0 20 3.8 30 6.7 2 ISO MTD 4 3.2 3.2.1 NIST SEM SRM 484d SEM x y () , x y . 1 m SRM 1960 , . , . 3.2.2 ( m) (1/mL) () 2 () 3 () 4 () 5 KS I ISO 16144:2009 5 NIST SRM 484d15 1 . SRM . , . ( ) . SRM 1015. 3.3 3.3.1 . . , . .
9、(fields-of-view) . , 3 . , . . , . . . , . 3 3.3.2 . . . , , . . 4 KS I ISO 16144:2009 6 . () . , , 16. , . . , . . . 17. (uncertainty) . , 3 300 270 1 m . 2 3 300 . , 13 50 . 251 , 6070 . 150180 . NIH , Lispix . 4 ISO MTD SEM 3.3.3 . , . , . . . KS I ISO 16144:2009 7 3.4 SRM 2806 SRM 2806 6 . (APC)
10、 . (batch) NIST . , . 4 4.1 SRM 2806 KS R ISO 12103A3 MTD( ) SRM . KS R ISO 12103 No. 4390C ISO MTD MILH5606 2.8 mg/L . 400 mL , 320 . 4.2 . , 0.2 m . , . 100 . ( 0.2 m, 25 mm) . 0.2 m , 1819. SAE(society of automotive) 20 3 . a) mL , . . b) SRM 2806 ( ) . c) . , , . , SRM 2806 . 10 mL 30 mL , . . ,
11、 . 3 . 4.3 4.3.1 KS I ISO 16144:2009 8 . . , . . . . . , ( ) . 4.3.2 SEM SEM SRM 1 . 1 100 m SEM . . 2122232425. 25 mm , SEM (stage) . SEM . , . , 12 . , 5 . 256 SEM . . ( ) 256( ) 40 50 , 20 30 . 2 CDROMs . , 100, 300 , 500, 1 500 3 300 . 0.8 mm 2 , 0.09 mm 2 , 0.03 mm 2 , 0.004 mm 2 , 0.000 8 mm 2
12、 . 6 4 ISO MTD 4 . 6 a): 3 300, 6 b):1 500, 6 c):500, 6 d):100. , . KS I ISO 16144:2009 9 , . 3 300 . . 5 SEM ( 3 300) a) 3 300 b) 1 500 6 4 ISO MTD SEM KS I ISO 16144:2009 10 c) 500 d) 100 6 4 ISO MTD SEM () 4.3.3 . SEM 12 . 8 . 512512 . SRM 484d . . “ ” . . , . , 5 , . . . 7 SEM (A) (B) . 7 c) ( )
13、. MacLispix NIST , NIH 2728. . , , , , . , . KS I ISO 16144:2009 11 (A) , (B) , (C) . , . 7 ISO MTD 3 300 SEM 5 ( ) . . , . SEM . 61 000 . SEM . , . , . , . , KS I ISO 16144:2009 12 . (np) , . . , . A f A eff . A eff/ A f 12d/Ld 2 /L 2 d: d2(area/ ) 1/2 L: , . . SRM 484d . ( ), mm . . . Kriging 29. Kriging . , . (3 % ). .
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