1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 0032 KS M 0032 :2009 2009 11 30 http:/www.kats.go.krKS M 0032:2009 : ( ) ( ) SK R&D center () () () ( ) : (http:/www.standard.go.kr) : : 1989 12 23 : 2009 11 30 2009-0741 : : ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M 0032:2009 General rules
2、for ICP emission spectrochemical analysis 1 . a) b) c) d) 2 . . ( ) . KS A ISO 572516, ( )16 KS M 0001, KS M 0016, KS M 1122, () KS M 8001, 3 . 4 KS M 0001 . 5 . KS M 0032:2009 2 5.1 (plasma) 5.2 (sequential spectrometer) 5.3 (simultaneous spectrometer) 2 () 5.4 (sample) 5.5 (sample solution) 5.6 (g
3、rating) 6 6.1 1 . 1 () 6.2 , , . KS M 0032:2009 3 6.2.1 , . . 2 . 2 () 6.2.2 . 6.3 , , . 3 , 10 L/min . , (27.12 MHz) . . 6.3.1 , 6.3.1.1 . (1 kW2 kW) . . . , . 0.05 % . (160) MHz, 27.12 MHz 40.68 MHz . . KS M 0032:2009 4 3 () 6.3.1.2 , . . 6.3.1.3 . . . 6.3.2 3 3 . 5 mm, 1 L/min . (1020) L/min , ,
4、(00.7) L/min . 6.4 . KS M 0032:2009 5 6.4.1 . , , . , . 170 nm , (3040) 0.5 . 4 . 4 () 6.4.1.1 1 1 . , . 6.4.1.2 1 1 . 20 mm20 m, . 2 1 nm . 6.4.1.3 . , . , 2 , 3 . , 1 . 800 nm 1 400 nm 2 266 nm 3 2 1 0 400 nm 1 200 nm 2 133 nm 3 KS M 0032:2009 6 , 1 m . 1 200 /mm 2 1 1.0 nm/mm . 6.4.1.4 2 2 , , ,
5、. 6.4.2 6.4.1 , 5 . , . 2 . 5 () 6.5 , . . a) b) c) 1 d) 1) 2) 3) e) 7 1 2 KS M 0032:2009 7 , . , . 8 , 8.1 1) , 1 S/cm (25 ) 2), (110 ) 1 mg/kg 3) 60 . , 4) . 8.2 . a) . b) 8.1 , . c) . d) , , , . 8.3 KS M 1122 99.995 % . 9 9.1 . a) b) c) d) ( ) e) 1) , (0.11) m . 2) . 3) 500 mL (0.002 mol/L) 0.2 m
6、L (1:1) 2 mL . 4) , , . KS M 0032:2009 8 f) g) h) i) j) k) 9.2 , , . . X . . 9.3 KS A ISO 572516 . 10 . a) , . b) 1 . c) . . 2 , . d) . e) , . f) , , . g) , , , . h) , RF . i) , . 11 . KS M 0032:2009 9 a) , b) c) d) (, ) e) ( , ) f) ( , , , ) g) (, ) 153787 1 92 3(13) (02)26240114 (02)262401489 http:/ KS M 0032 :2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS General rules for ICP emission spectrochemical analysis ICS 17.280.20;71.040.40 Korean Agency for Technology and Standards http:/www.kats.go.kr
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