KS M 4801-2006 Analytical methods of explosives《炸药化学分析法》.pdf

1、 KSKSKSKS SKSKSKS KSKSKS SKSKS KSKS SKS KS 2006 11 30 KS M 4801 KS M 4801： 2006M 4801： 2006 ( ) ( ) SK R&D center ( ) ( ) ( ) ( ) ： ： 1962 4 23 ： 2006 11 30 2006 0709 ： ： ( ) ( 02 509 72997301) . 7 5 , . ICS 71.100.30 KS M 4801： 2006Analytical methods of explosives 1. KS M 4804 1 . 1 , , , , , , , ,

2、 , , , 2. . . KS M 4804 3. 3.1 5 g (a) , 48 , (b) , (%) . (%) = 100aba3.2 3.1 (b) , (Soxhllet) . , 3040 , 5060 . 50 2 , (c) , (%) . (E )(%) = 100bcb3.3 3.2 (c) , 100 mL . , . 70 , 100 mL . 70 5 , , (d) . , 250 mL , 5. . M 4801： 2006 2 (H)(%) = 100bdc4. ( NG .) a) ( ) 3.2 (E ) . b) E NG . E NG , 50 m

3、L (A). ( 200 mL) A 5 mL 0.1 N (II)(FeCl2) (B) 5 mL ( 1.8) 10 mL . . 10 , MnSO4 4H2O 6.7 g ( 1.7) 13.8 mL ( 1.84) 13 mL , 100 mL . 10 mL B 0.1 N (C) . C V mL , C VmL , B 1 mL NG 0.002 523 g NG(%) = 1005/50)(523 002.0bFVV (%) = E (%) NG(%) F 0.1 N 5. a) 2 , 3.3 H . 2 , . 250 mL , 50 mL 100 mL , (K) .

4、Ba(NO3)2(%) =bK 50/250118.1100 250 mL , 25 mL , 50 mL 0.1 N 75 mL . (半量 ) 35 % 50 mL , . 0.1 N . 0.1 N ( ) q mL NH4NO3(%) =bq 50/250005 008.0100 NH4ClO4(%) =bq 50/25075 011.0100 b) 250 mL 50 mL , 5 mL (Al 45, Cu 50, Zn 5) 3 g , 0.1 N 75 mL M 4801： 2006 3 , ( ) 50 mL . 30 . 0.1 N (mL)( ) (P) . KNO3(%

5、) = 10050/250111 010.0bpNaNO3(%) = 10050/25050 008.0bpc) 2 . d) 50 mL 2 0.1 N q mL , 50 mL 5. b) 0.1 N 9 mL . (p q) NO3 , q (p q) = 2q p . NH4NO3(%) = 10050/250)(500 008.0bqpNH4ClO4(%) = 10050/250)2(75 011.0bpqe) 250 mL 50 mL , (1： 1) 5 mL . . (r) , 1.590 2 . f) 250 mL 50 mL , ( 9.7 g 100 mL .) 3 ,

6、0.1 N . 0.1 N . 0.1 N 1 mL 0.005 846 , (mL) S NaCl(%) = 10050/250846 005.0bS6. 20 g , 100 mL (II) (FeSO4 7H2O 28 g 50 mL , 1 000 mL .) 30 mL 10 0.1 N (X mL) 0.1 N (Y mL) , . NH4ClO3(%) = 100)(69 001.0 XY7. a) 3.3 (d) . (%) = 100bdM 4801： 2006 4 b) (Z) . (%) = 10096.9bZ 2006 12 26 135 513 701 7 (02)6

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9、(062)953 1435 7 Fax. (062)953 1438 641 966 298 7 ( 6 ) (055)212 1212 Fax. (055)212 1213 683 804 758 2( 2 ) (052)289 6601 3 Fax. (052)289 6604 425 020 541 3( 4 ) (031)487 6191 4 Fax. (031)487 6195 730 350 92 30( 8 ) (054)473 6954 Fax. (054)473 6955 480 848 2 487 6( 3 ) (031)829 8182 4 Fax. (031)829 8185 KOREAN STANDARDS ASSOCIATION KSKSKSSKSKS KSKS SKS KSKS SKSKS KSKSKSKS M 4801： 2006 Analytical methods of explosives ICS 71.100.30