1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 84221- ( )KS M 8422:2012 2012 12 28 http:/www.kats.go.krKS M 8422:2012 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : :1997 12 24 :2012 12 28 2012-0817 : : ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS M 8422:2012 1- ( ) 1-Naphthol 1 1- ( 1- . ) . 2
2、. . ( ) . KS M 0009, KS M 0024, KS M 8001, 3 3.1 1- , . . 3.2 KS M 0024 3 300 cm 1, 1 600 cm 1, 1 390 cm 1, 1 270 cm 1, 1 080 cm 1, 1 020 cm 1, 790 cm 1 770 cm 1 . , KS M 0024 7.2 a)( ) . 1 . C10H8O FW: 144.17 OH KS M 8422:2012 2 1 4 1- 5. 1 . 1 (GC ) ( ) 2- 99.0 % 95 C97 C 1.0 % 0.02 % 0.1 % 0.1 %
3、5 5.1 (GC ) 5.6 5.7 . KS M 8001 6.32( ) . (%) (cm 1) KS M 8422:2012 3 a) b) 0.5 g (10 mL) 8 mL (A ). A 2 mL( 0.1 g) (10 mL) N,O- ( )1)2.5 mL (X ). c) 10 mg 2- 10 mg 100 mL (B ). A 2 mL (10 mL) B 1 mL ( 0.1 mg, 2- 0.1 mg) N, O- ( )1)2.5 mL (Y ). d) 1) 100 % ( DB-1), 50 % -50 % ( MPS 50) . 2) , 0.25 m
4、m, 25 m, 0.25 m 3) 150 C 160 C 270 C 290 C 240 C 260 C 4) , 30 cm/s 5) (X ) (Y ) 1 L e) . 1) (GC ): 1- (GC ) . 2) : (X ) (Y ) 1- N1, n1, 1- N2, n2 112221NnNnNn 3) 2- : 2) , 2- n3, 2- n4 132413NnNnNn 5.2 2 g (99.5 %) 20 mL . 5.3 1) N.O- ( ) 75 % d) , 1- 2 . KS M 8422:2012 4 KS M 8001 6.4( ) . 5.4 KS
5、M 0009 5.1.4 d)( 4: ) . , 1.0 g 0.1 mg 18 10 mg . 5.5 ( ) KS M 0009 5.4.4 d)( 4: ) . 5 g 1 mL 1 mg . 5.6 5.1 . 5.7 2- 5.1 . 6 . 7 . a) “1- ” “ ” b) c) ( ) d) e) f) g) 1-() 153787 1 92 3(16) (02)26240114 (02)262401489 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M 8422:2012 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS 1-Naphthol ICS 71.040.30