1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 84232- ( )KS M 8423:2012 2012 12 28 http:/www.kats.go.krKS M 8423:2012 : ( ) ( ) ( ) : (http:/www.standard.go.kr) : :1997 12 24 :2012 12 28 2012-0817 : : ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS M 8423:2012 2- ( ) 2-Naphthol 1 2- ( 2- .) . 2 .
2、 . ( ) . KS M 0009, KS M 0024, KS M 8001, 3 3.1 2- . . 3.2 KS M 0024 , 3 270 cm 1, 1 630 cm 1, 1 510 cm 1, 1 280 cm 1, 1 220 cm 1, 840 cm 1 740 cm 1 . , KS M 0024 7.2 a)( ) . 1 . C10H8O FW: 144.17 OHKS M 8423:2012 2 1 4 2- 5. 1 . 1 (GC ) ( ) 1- 99.0 % 121 C123 C 1.0 % 0.02 % 0.1 % 0.1 % 5 5.1 (GC )
3、5.6 5.7 . KS M 8001 6.32( ) . a) (%) (cm 1)KS M 8423:2012 3 b) 0.50 g (10 mL) 8 mL (A ). A 2 mL( 0.1 g) (10 mL) N,O- ( )1)2.5 mL (X ). c) 10 mg 1- 10 mg 100 mL (B ). A 2 mL (10 mL) B 1 mL ( 0.1 mg, 1- 0.1 mg) N,O- ( )1)2.5 mL (Y ). d) 1) 100 % ( DB-1), 50 % -50 % ( MPS 50) . 2) , 0.25 mm, 25 m, 0.25
4、 m 3) 150 C 160 C 270 C 290 C 240 C 260 C 4) , 30 cm/s 5) (X ) (Y ) 1 L e) . 1) (GC ) 2- (GC ) . 2) (X ) (Y ) 2- N1, n1, 2- N2, n2 112211NnNnNn 3) 1- 2) , 1- n3, 1- n4 132413NnNnNn 5.2 2 g (99.5 %) 20 mL . 5.3 KS M 8001 6.4( ) . 1) N,O- ( ) 75 % d) 2- 2 . KS M 8423:2012 4 5.4 KS M 0009 5.1.4 d)( 4:
5、) . , 1.0 g 0.1 mg 18 10 mg . 5.5 ( ) KS M 0009 5.4.4 d)( 4: ) . 5 g 1 mL 1 mg . 5.6 5.1 . 5.7 1- 5.1 . 6 . 7 . a) “2- ” “ ” b) c) ( ) d) e) f) g) 2-() 153787 1 92 3(16) (02)26240114 (02)262401489 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M 8423:2012 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS 2Naphthol ICS 71.040.30