KS M ISO 1628-2-2010 Plastics－Determination of the viscosity of polymers in dilute solution using capillary viscometers－Part 2：Poly(vinyl chloride) resins《用毛细管粘度计测定稀溶液中聚合物的粘度 第2部分 .pdf

1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 16282 2：(PVC) KS M ISO 16282 :2010 2010 7 28 http:/www.kats.go.krKS M ISO 16282:2010 : ( ) ( ) ( )SK ( ) ( ) : (http:/www.standard.go.kr) ： ：2005 12 29 ：2010 7 28 2010-0294 ： ： ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M ISO 16282:2010 2：(

2、PVC) PlasticsDetermination of the viscosity of polymers in dilute solution using capillary viscometersPart 2：Poly(vinyl chloride) resins 1998 2 ISO 16282, Determination of the viscosity of polymers in dilute solution using capillary viscometersPart 2：Poly(vinyl chloride) resins , . 1 PVC ( .) K . .

3、, . ( , , ) . ISO 1269 (0.5 0.1) % . . K () () . K . PVC K . K . PVC . PVC . K . 2 . KS M ISO 16282:2010 2 . ( ) . KS L ISO 1042：2006, KS M ISO 16281：2002, 1 ： KS M ISO 3105：2003, ISO 1269：2005, PlasticsHomopolymer and copolymers resins of vinyl chlorideDetermination of volatile matter(including wat

4、er) 3 KS M ISO 16281 3., 3.3.3( ) 3.3.6(K) . 4 . K . 5 5.1 25 /() 2.0610 6 m 2 s 1 2.3310 6 m 2 s 1 . 155 . . . 6 KS M ISO 16281 5. . . 6.1 KS M ISO 16281 5.1 KS M ISO 3105 B.4 0.77 mm2 % 1C . KS M ISO 16281 K . 6.2 (1 ) KS L ISO 1042 A 50 mL . KS L ISO 1042 20 . 6.3 KS M ISO 16282:2010 3 ( 4050 m)

5、6.4 (6.2) 80 85 . 80 85 . 6.5 0.1 mg . 6.6 0.1 (25.00.5) 0.05 . 6.7 0.05 . 6.8 0.1 . 7 2 . 8 2 . 9 9.1 KS M ISO 16281 6. . (251) (50.1) g/L . (0.2500.005) g 0.2 mg 50 mL (6.2) . 40 mL (5.1) . (6.4) 80 85 1 . . . (251) . 0.1 % . (0.2500.000 25) g 50 mL 1 KS M ISO 16282:2010 4 ( ) K . , K . . 85 K 2.0

6、 , KS M ISO 16281 6.2 . PVC . 9.2 KS M ISO 16281 8. . (6.6 ) (6.7) (250.5) . 0.05 . (6.3 ) . KS M ISO 16281 A . 0.2 . 2 0.25 % . . . . . 10 10.1 I KS M ISO 16281 9. . c t t t I0 0 t t 0 ： () c ： (g/mL) 2 I . 2 I 0.4 % . (50.005) g/L 1 I , I (m 3 /kg)10 3 , mL/g . KS M ISO 16282:2010 5 10.2 K K KS M

7、ISO 16281 9. . 000 1300 150 log 5 . 1 log 5 . 1 2 2 1 1 log 5 . 1 r r r c c K 0 0 r t t ： ( ) t t 0 ： () c ： (g/mL) 2 2 K K . 2 K 0.4 % . (50.005) g/L 1 K . 11 11 4 , s r ( ) s R ( ) . K 50 70 90 s r0.132 0.115 0.120 s R0.420 0.291 0.495 61 124 227 s r0.313 0.458 0.742 s R0.984 1.202 3.042 12 . a) b

8、) c) / K d) e) KS M ISO 16282:2010 6 1 (I ) K (VR) ：(m 3 /kg)10 3 , mL/g 5 g/mL VR I K VR I K VR I K 1.195 1.196 1.197 1.198 1.199 1.200 1.201 1.202 1.203 1.204 1.205 1.206 1.207 1.208 1.209 1.210 1.211 1.212 1.213 1.214 1.215 1.216 1.217 1.218 1.219 1.220 1.221 1.222 1.223 1.224 1.225 1.226 1.227 1

9、.228 1.229 1.230 1.231 1.232 1.233 1.234 1.235 1.236 39.0 39.2 39.4 39.6 39.8 40.0 40.2 40.4 40.6 40.8 41.0 41.2 41.4 41.6 41.8 42.0 42.2 42.4 42.6 42.8 43.0 43.2 43.4 43.6 43.8 44.0 44.2 44.4 44.6 44.8 45.0 45.2 45.4 45.6 45.8 46.0 46.2 46.4 46.6 46.8 47.0 47.2 39.74 39.85 39.95 40.06 40.17 40.27 4

10、0.38 40.49 40.59 40.70 40.80 40.91 41.01 41.12 41.22 41.33 41.43 41.53 41.64 41.74 41.84 41.94 42.05 42.15 42.25 42.35 42.45 42.55 42.65 42.75 42.85 42.95 43.05 43.15 43.25 43.34 43.44 43.54 43.64 43.73 43.83 43.93 1.237 1.238 1.239 1.240 1.241 1.242 1.243 1.244 1.245 1.246 1.247 1.248 1.249 1.250 1

11、.251 1.252 1.253 1.254 1.255 1.256 1.257 1.258 1.259 1.260 1.261 1.262 1.263 1.264 1.265 1.266 1.267 1.268 1.269 1.270 1.271 1.272 1.273 1.274 1.275 1.276 1.277 1.278 47.4 47.6 47.8 48.0 48.2 48.4 48.6 48.8 49.0 49.2 49.4 49.6 49.8 50.0 50.2 50.4 50.6 50.8 51.0 51.2 51.4 51.6 51.8 52.0 52.2 52.4 52.

12、6 52.8 53.0 53.2 53.4 53.6 53.8 54.0 54.2 54.4 54.6 54.8 55.0 55.2 55.4 55.6 44.02 44.12 44.22 44.31 44.41 44.50 44.60 44.69 44.79 44.88 44.98 45.07 45.16 45.26 45.35 45.44 45.53 45.63 45.72 45.81 45.90 45.99 46.09 46.18 46.27 46.36 46.45 46.54 46.63 46.72 46.81 46.90 46.99 47.07 47.16 47.25 47.34 4

13、7.43 47.52 47.60 47.69 47.78 1.279 1.280 1.281 1.282 1.283 1.284 1.285 1.286 1.287 1.288 1.289 1.290 1.291 1.292 1.293 1.294 1.295 1.296 1.297 1.298 1.299 1.300 1.301 1.302 1.303 1.304 1.305 1.306 1.307 1.308 1.309 1.310 1.311 1.312 1.313 1.314 1.315 1.316 1.317 1.318 1.319 1.320 55.8 56.0 56.2 56.4

14、 56.6 56.8 57.0 57.2 57.4 57.6 57.8 58.0 58.2 58.4 58.6 58.8 59.0 59.2 59.4 59.6 59.8 60.0 60.2 60.4 60.6 60.8 61.0 61.2 61.4 61.6 61.8 62.0 62.2 62.4 62.6 62.8 63.0 63.2 63.4 63.6 63.8 64.0 47.87 47.95 48.04 48.13 48.21 48.30 48.38 48.47 48.55 48.64 48.72 48.81 48.89 48.98 49.06 49.15 49.23 49.32 4

15、9.40 49.48 49.57 49.65 49.73 49.81 49.90 49.98 50.06 50.14 50.23 50.31 50.39 50.47 50.55 50.63 50.71 50.79 50.87 50.95 51.03 51.11 51.19 51.27 KS M ISO 16282:2010 7 1 (I ) K (VR) () ：(m 3 /kg)10 3 , mL/g 5 g/mL VR I K VR I K VR I K 1.321 1.322 1.323 1.324 1.325 1.326 1.327 1.328 1.329 1.330 1.331 1.

16、332 1.333 1.334 1.335 1.336 1.337 1.338 1.339 1.340 1.341 1.342 1.343 1.344 1.345 1.346 1.347 1.348 1.349 1.350 1.351 1.352 1.353 1.354 1.355 1.356 1.357 1.358 1.359 1.360 1.361 1.362 1.363 1.364 1.365 1.366 1.367 1.368 1.369 1.370 64.2 64.4 64.6 64.8 65.0 65.2 65.4 65.6 65.8 66.0 66.2 66.4 66.6 66.

17、8 67.0 67.2 67.4 67.6 67.8 68.0 68.2 68.4 68.6 68.8 69.0 69.2 69.4 69.6 69.8 70.0 70.2 70.4 70.6 70.8 71.0 71.2 71.4 71.6 71.8 72.0 72.2 72.4 72.6 72.8 73.0 73.2 73.4 73.6 73.8 74.0 51.35 51.43 51.51 51.59 51.67 51.75 51.83 51.91 51.98 52.06 52.14 52.22 52.29 52.37 52.45 52.53 52.60 52.68 52.76 52.8

18、3 52.91 52.99 53.06 53.14 53.21 53.29 53.37 53.44 53.52 53.59 53.67 53.74 53.82 53.89 53.96 54.04 54.11 54.19 54.26 54.33 54.41 54.48 54.55 54.63 54.70 54.77 54.85 54.92 54.99 55.06 1.371 1.372 1.373 1.374 1.375 1.376 1.377 1.378 1.379 1.380 1.381 1.382 1.383 1.384 1.385 1.386 1.387 1.388 1.389 1.39

19、0 1.391 1.392 1.393 1.394 1.395 1.396 1.397 1.398 1.399 1.400 1.401 1.402 1.403 1.404 1.405 1.406 1.407 1.408 1.409 1.410 1.411 1.412 1.413 1.414 1.415 1.416 1.417 1.418 1.419 1.420 74.2 74.4 74.6 74.8 75.0 75.2 75.4 75.6 75.8 76.0 76.2 76.4 76.6 76.8 77.0 77.2 77.4 77.6 77.8 78.0 78.2 78.4 78.6 78.

20、8 79.0 79.2 79.4 79.6 79.8 80.0 80.2 80.4 80.6 80.8 81.0 81.2 81.4 81.6 81.8 82.0 82.2 82.4 82.6 82.8 83.0 83.2 83.4 83.6 83.8 84.0 55.14 55.21 55.28 55.35 55.42 55.49 55.57 55.64 55.71 55.78 55.85 55.92 55.99 56.06 56.13 56.20 56.27 56.34 56.41 56.48 56.55 56.62 56.69 56.76 56.83 56.90 56.97 57.04

21、57.11 57.17 57.24 57.31 57.38 57.45 57.51 57.58 57.65 57.72 57.79 57.85 57.92 57.99 58.05 58.12 58.19 58.26 58.32 58.39 58.45 58.52 1.421 1.422 1.423 1.424 1.425 1.426 1.427 1.428 1.429 1.430 1.431 1.432 1.433 1.434 1.435 1.436 1.437 1.438 1.439 1.440 1.441 1.442 1.443 1.444 1.445 1.446 1.447 1.448

22、1.449 1.450 1.451 1.452 1.453 1.454 1.455 1.456 1.457 1.458 1.459 1.460 1.461 1.462 1.463 1.464 1.465 1.466 1.467 1.468 1.469 1.470 84.2 84.4 84.6 84.8 85.0 85.2 85.4 85.6 85.8 86.0 86.2 86.4 86.6 86.8 87.0 87.2 87.4 87.6 87.8 88.0 88.2 88.4 88.6 88.8 89.0 89.2 89.4 89.6 89.8 90.0 90.2 90.4 90.6 90.

23、8 91.0 91.2 91.4 91.6 91.8 92.0 92.2 92.4 92.6 92.8 93.0 93.2 93.4 93.6 93.8 94.0 58.59 58.65 58.72 58.79 58.85 58.92 58.98 59.05 59.11 59.18 59.24 59.31 59.37 59.44 59.50 59.57 59.63 59.70 59.76 59.82 59.89 59.95 60.02 60.08 60.14 60.21 60.27 60.33 60.40 60.46 60.52 60.59 60.65 60.71 60.78 60.84 60

24、.90 60.96 61.03 61.09 61.15 61.21 61.27 61.34 61.40 61.46 61.52 61.58 61.64 61.70 KS M ISO 16282:2010 8 1 (I ) K (VR) () ：(m 3 /kg)10 3 , mL/g 5 g/mL VR I K VR I K VR I K 1.471 1.472 1.473 1.474 1.475 1.476 1.477 1.478 1.479 1.480 1.481 1.482 1.483 1.484 1.485 1.486 1.487 1.488 1.489 1.490 1.491 1.4

25、92 1.493 1.494 1.495 1.496 1.497 1.498 1.499 1.500 1.501 1.502 1.503 1.504 1.505 1.506 1.507 1.508 1.509 1.510 1.511 1.512 1.513 1.514 1.515 1.516 1.517 1.518 1.519 1.520 94.2 94.4 94.6 94.8 95.0 95.2 95.4 95.6 95.8 96.0 96.2 96.4 96.6 96.8 97.0 97.2 97.4 97.6 97.8 98.0 98.2 98.4 98.6 98.8 99.0 99.2

26、 99.4 99.6 99.8 100.0 100.2 100.4 100.6 100.8 101.0 101.2 101.4 101.6 101.8 102.0 102.2 102.4 102.6 102.8 103.0 103.2 103.4 103.6 103.8 104.0 61.77 61.83 61.89 61.95 62.01 62.07 62.13 62.19 62.25 62.31 62.37 62.43 62.49 62.55 62.61 62.67 62.73 62.79 62.85 62.91 62.97 63.03 63.09 63.15 63.21 63.27 63

27、.33 63.38 63.44 63.50 63.56 63.62 63.68 63.73 63.79 63.85 63.91 63.97 64.02 64.08 64.14 64.20 64.26 64.31 64.37 64.43 64.49 64.54 64.60 64.66 1.521 1.522 1.523 1.524 1.525 1.526 1.527 1.528 1.529 1.530 1.531 1.532 1.533 1.534 1.535 1.536 1.537 1.538 1.539 1.540 1.541 1.542 1.543 1.544 1.545 1.546 1.

28、547 1.548 1.549 1.550 1.551 1.552 1.553 1.554 1.555 1.556 1.557 1.558 1.559 1.560 1.561 1.562 1.563 1.564 1.565 1.566 1.567 1.568 1.569 1.570 104.2 104.4 104.6 104.8 105.0 105.2 105.4 105.6 105.8 106.0 106.2 106.4 106.6 106.8 107.0 107.2 107.4 107.6 107.8 108.0 108.2 108.4 108.6 108.8 109.0 109.2 10

29、9.4 109.6 109.8 110.0 110.2 110.4 110.6 110.8 111.0 111.2 111.4 111.6 111.8 112.0 112.2 112.4 112.6 112.8 113.0 113.2 113.4 113.6 113.8 114.0 64.71 64.77 64.83 64.88 64.94 65.00 65.05 65.11 65.17 65.22 65.28 65.33 65.39 65.45 65.50 65.56 65.61 65.67 65.72 65.78 65.83 65.89 65.95 66.00 66.06 66.11 66

30、.17 66.22 66.27 66.33 66.38 66.44 66.49 66.55 66.60 66.66 66.71 66.76 66.82 66.87 66.93 66.98 67.03 67.09 67.14 67.19 67.25 67.30 67.36 67.41 1.571 1.572 1.573 1.574 1.575 1.576 1.577 1.578 1.579 1.580 1.581 1.582 1.583 1.584 1.585 1.586 1.587 1.588 1.589 1.590 1.591 1.592 1.593 1.594 1.595 1.596 1.

31、597 1.598 1.599 1.600 1.601 1.602 1.603 1.604 1.605 1.606 1.607 1.608 1.609 1.610 1.611 1.612 1.613 1.614 1.615 1.616 1.617 1.618 1.619 1.620 114.2 114.4 114.6 114.8 115.0 115.2 115.4 115.6 115.8 116.0 116.2 116.4 116.6 116.8 117.0 117.2 117.4 117.6 117.8 118.0 118.2 118.4 118.6 118.8 119.0 119.2 11

32、9.4 119.6 119.8 120.0 120.2 120.4 120.6 120.8 121.0 121.2 121.4 121.6 121.8 122.0 122.2 122.4 122.6 122.8 123.0 123.2 123.4 123.6 123.8 124.0 67.46 67.51 67.57 67.62 67.67 67.73 67.78 67.83 67.88 67.94 67.99 68.04 68.09 68.15 68.20 68.25 68.30 68.36 68.41 68.46 68.51 68.56 68.61 68.67 68.72 68.77 68

33、.82 68.87 68.92 68.97 69.03 69.08 69.13 69.18 69.23 69.28 69.33 69.38 69.43 69.48 69.53 69.59 69.64 69.69 69.74 69.79 69.84 69.89 69.94 69.99 KS M ISO 16282:2010 9 1 (I ) K (VR) () ：(m 3 /kg)10 3 , mL/g 5 g/mL VR I K VR I K VR I K 1.621 1.622 1.623 1.624 1.625 1.626 1.627 1.628 1.629 1.630 1.631 1.6

34、32 1.633 1.634 1.635 1.636 1.637 1.638 1.639 1.640 1.641 1.642 1.643 1.644 1.645 1.646 1.647 1.648 1.649 1.650 1.651 1.652 1.653 1.654 1.655 1.656 1.657 1.658 1.659 1.660 1.661 1.662 1.663 1.664 1.665 1.666 1.667 1.668 1.669 1.670 124.2 124.4 124.6 124.8 125.0 125.2 125.4 125.6 125.8 126.0 126.2 126.4 126.6 126.8 127.0 127.2 127.4 127.6 127.8 128.0 128.2 128.4 128.6 128.8 129.0 129.2 129.4