1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 4097 - - (EPDM) KS M ISO 4097:2009 2009 4 29 http:/www.kats.go.krKS M ISO 4097:2009 : ( ) ( ) () () ( ) : (http:/www.standard.go.kr) : : 2002 11 30 : 2009 4 29 2009-0176 : : ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M ISO 4097:2009 - - (EPD
2、M) Rubber, ethylene-propylene-diene(EPDM) Evaluation procedure . . , . 2007 5 ISO 4097, Rubber, ethylene-propylene-diene(EPDM) Evaluation procedure , . 1 . - - ( EPDM .) EPDM , , 2 . . ( ) . KS M ISO 37, KS M ISO 247, KS M ISO 248, KS M ISO 289 1, 1: KS M ISO 1795, KS M ISO 2393, , KS M ISO 3417, KS
3、 M ISO 6502, KS M ISO 23529, 3 KS M ISO 4097:2009 2 3.1 1.5 kg KS M ISO 1795 . 3.2 (test portion) KS M ISO 1795 . 4 4.1 3.2 KS M ISO 289 1 ( ). (mill roll) 50 5 ( , 35 5 ). , . (100 150 ) / (1 8) 125 ML(1 4) . 4.2 KS M ISO 248 . 4.3 KS M ISO 247 A B . 5 5.1 1 , . 1 (%) 67 % EPDM . 2 (%) 67 % EPDM .
4、3 EPDM . 4 100 50 EPDM . 5 100 50 80 EPDM . 6 100 80 EPDM . . KS M ISO 4097:2009 3 1 EPDM 1 2 3 4 5 6 EPDM 100.00 100.00 100.00 100.00 xa 100.00 yb 100.00 zc 1.00 1.00 1.00 1.00 1.00 1.00 d 80.00 100.00 40.00 80.00 80.00 150.00 ASTM 103 e 50.00 75.00 50.00 xa 5.00 5.00 5.00 5.00 5.00 5.00 1.50 1.50
5、1.50 1.50 1.50 1.50 (TMTD)f 1.00 1.00 1.00 1.00 1.00 1.00 (MBT) 0.50 0.50 0.50 0.50 0.50 0.50 239.00 284.00 149.00 239.00 189.00 yb259.00 zca x 50 100 . b y 50 80 100 . c z 80 100 . d (IRB) . e 0.92 g/m3 Sun Refining and Marketing Company R.E. Carroll Inc., 1570 North Olden Avenue Ext, Trenton, NJ 0
6、8638, USA , . Sunoco Overseas Inc., 1801 Market Street, Philadelphia, PA 19103-1699, USA . . f TMTD Forcoven Products Inc., 22010 E. Martin Dr., Porter, TX 77365, USAIRM 1 . 5.2 5.2.1 , KS M ISO 2393 . 5.2.2 5.2.2.1 . A: B: C: - - . EPDM B . KS M ISO 4097:2009 4 5.2.2.2 A 5.2.2.2.1 ( ) ( ) a) 5 150
7、. 8 rad/s(77 r/min) . 0 0 b) , , , . 0.5 0.5 c) . 2.5 3.0 d) . . 0.5 3.5 e) 150 5 . . 1.5 5.0 ( ) 5.0 f) 2.5 mm 50 5 3 . (KS M ISO 2393 ). 5.05.1+% . g) KS M ISO 23529 30 24 . 5.2.2.2.2 ( ) ( ) a) 40 5 . 8 rad/s(77 r/min) . 0 0 b) 5.2.2.2.1 , . . 0.5 0.5 c) 110 2 . . 1.5 2.0 ( ) 2.0 d) 0.8 mm 50 5 .
8、 e) . f) 6 mm . (KS M ISO 2393 ). 5.05.1+% . g) . h) 2.2 mm , KS M ISO 37 . i) KS M ISO 23529 30 24 . KS M ISO 4097:2009 5 5.2.2.3 B (g) 2 . 50 5 . , , , ( ). ( ) . . ( ) ( ) a) 50 5 0.7 mm . 1.0 1.0 b) , , . 2, 4 5 c) . 13.0 b) c) 14.0 c) 1.3 mm 3/4 . 1.8 mm . 3/4 . . d) 1.8 mm . 3.0 17.0 e) 15 3/4
9、 . 2.0 19.0 f) . 0.8 mm . 2.0 21.0 21.0 g) 6 mm (KS M ISO 2393 ). 5.05.1+ . h) . i) 2.2 mm KS M ISO 37 . j) KS M ISO 23529 2 24 . 5.2.2.4 C 5.2.2.4.1 1 KS M ISO 4097:2009 6 ( ) ( ) a) 5 150 . 8 rad/s(77 r/min) . 0 0 b) , , , . 0.5 0.5 c) . 2.5 3.0 d) . . 0.5 3.5 e) 150 5 . . 1.5 5.0 ( ) 5.0 f) 2.5 m
10、m 50 5 3 . (KS M ISO 2393 ). 5.05.1+% . g) KS M ISO 23529 30 24 . 5.2.2.4.2 2 . . (g) 2 . ( ) ( ) a) 50 5 1.5 mm . . . . 1.0 1.0 b) 15 3/4 . 2.0 3.0 c) . 0.8 mm . 2.0 5.0 5.0 d) 6 mm . (KS M ISO 2393 ). 5.05.1+% . e) . f) 2.2 mm , . g) KS M ISO 23529 2 24 . KS M ISO 4097:2009 7 6 . 6.1 . tS1, t C(50
11、) t C(90) ML, MHKS M ISO 3417 . : 1.7 Hz ( 100 ) : 1 : MH 75 % . 75 % . : 160 0.3 : . 6.2 . tS1, t C(50) t C(90) FL, FmaxKS M ISO 6502 . : 1.7 Hz( 100 ) : 0.5 : Fmax 75 % . 75 % . : 160 0.3 : . 7 . 160 10 , 20 , 30 , 40 50 . t C(90) . , . KS M ISO 23529 16 96 . KS M ISO 37 . KS M ISO 4097:2009 8 8 8
12、.1 ASTM D 3568-036 . ISO/TR 9272: 19863 . 8.2 8.2.1 2 ( ) . (EPDM ) . 8 (A ) International reference black No 6(IRB No 6) . ( ) . 8.2.2 2 ( ) . (EPDM ) . 8 3 (B ) . 8.3 2 3 . 2 3 . r . . (r) %( ) ( , ) . 95 % . R . . (R) %( ) ( , ) . 95 % . KS M ISO 4097:2009 9 2 2 a srr (r) sRR (R) MLdNm 6.7 12.4 0
13、.50 1.42 14.8 1.24 3.51 36.6 MHdNm 32.7 46.9 1.29 3.65 9.2 3.66 10.4 26.1 tS1 2.2 2.7 0.11 0.31 12.4 0.38 1.08 43.2 t C(90) 12.6 15.6 0.64 1.81 12.8 1.20 3.40 24.1 sr sR a 160 , 1.7 Hz, 1 . (r) (R) 3 2 a srr (r) sRR (R) MLdNm 7.00 0.54 1.51 21.57 1.49 4.19 59.86 MHdNm 46.09 1.06 2.96 6.42 2.41 6.74
14、14.62 tS1 2.23 0.05 0.14 6.72 0.25 0.69 30.94 t C(50) 4.43 0.18 0.49 11.06 0.27 0.75 16.93 t C(90) 13.47 0.45 1.25 9.28 0.95 2.67 19.82 sr sR a 160 , 1.7 Hz, 1 . (r) (R) 9 . a) b) c) , ( ) d) (KS M ISO 247 A B ) e) f) g) 5.2.2 h) 5.2.2.2.1 g) 5.2.2.2.2 i) 5.2.2.3 j) 5.2.2.4.1 g) 5.2.2.4.2 g) i) 6. M
15、H Fmax j) 7. k) l) m) n) KS M ISO 4097:2009 10 1 ISO 1382, Rubber Vocabulary 2 ISO 6472, Rubber compounding ingredients Abbreviations 3 ISO/TR 9272: 1986, Rubber and rubber products Determination of precision for test method standards(now withdrawn) 4 ASTM D 88, Standard Test Method for Saybolt Visc
16、osity 5 ASTM D 2161, Standard Practice for Conversion of Kinematic Viscosity to Saybolt Universal Viscosity or to Saybolt Furol Viscosity 6 ASTM D 3568 03, Standard Test Method for Rubber Evaluation of EPDM(Ethylene Propylene Diene Terpolymers) Including Mixtures With Oil - (EPDM) 135513 7017 (02)60094114 (02)600948878 http:/ KS M ISO 4097:2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Rubber, ethylene-propylene- diene(EPDM)Evaluation procedureICS 83.060 Korean Agency for Technology and Standards http:/www.kats.go.kr
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