KS M ISO 5435-2012 Rubber compounding ingredients－Carbon black－Determination of tinting strength《橡胶复合材料 炭黑 着色强度的测定》.pdf

1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 5435 KS M ISO 5435:2012 2012 9 17 http:/www.kats.go.krKS M ISO 5435:2012 : ( ) ( ) ( ) : (http:/www.standard.go.kr) ： ：2012 9 17 2012-0435 ： ： ( 02-509-7270) (http:/www.kats.go.kr). 10 5 , . KS M ISO 5435:2012 i ii 1 1 2 1 3 1 4 .2 5 2 6 .3 7 3 7.1

2、3 7.2 4 8 .12 9 13 10 .13 A( ) .14 16 KS M ISO 5435:2012 ii 2008 4 ISO 5435, Rubber compounding ingredients Carbon blackDetermination of tinting strength . KS M ISO 5435:2012 Rubber compounding ingredients Carbon black Determination of tinting strength . , . . 1 (industry tint reference black) (tint

3、ing strength) . . (standard reference black) ASTM D4821 (control limits) . Densichron (reflectometer) Meeco Colormaster , . 2 . . ( ) . KS M ISO 1126, ASTM D4821, Standard Guide for Carbon Black Validation of Test Method Precision and Bias 3 (industry tint reference black： ITRB) . (mulled) , (spread

4、). (shades of grey) . , 2 (relative tinting strength) . KS M ISO 5435:2012 2 4 4.1 (epoxidized soybean oil)1), 0.92 0.99 . (turbidity) 20 . 4.2 (ITRB)2)4.3 , , (ITZnO)3) . 4.4 (standard reference blacks)4)5 5.1 , 0.1 mg . 5.2 (muller)5)5.3 , 125 1 5 . 5.4 , (100 150) mm . 5.5 , 0.02 cm3 . 1) Paraple

5、x G-62 120 South Riverside Plaza, Suite 1620, Chicago, IL 60606 HallStar . ISO . . 2) ITRB 227 Somerset St., Borger, TX 79007 Balentine Enterprises, Inc. . ISO . . 3) ITZnO 300 Frankfort Rd., Monaca, PA 15061 Horsehead Corp. . ISO . . 4) 227 Somerset St., Borger, TX 79007 Balentine Enterprises, Inc.

6、 . ISO . . 5) PO Box 218, State Highway 693, Hiwassee, VA 24347 Hoover Color Corp. (： ) Hoover Automatic Muller, M5 J. Engelsmann AG, Frankenthaler Str. 137-141, D-67059 Ludwigshafen Automatic Pigment Muller (： infoengelsmann.de) JEL 25/53 . ISO . . KS M ISO 5435:2012 3 5.6 (light-measuring instrume

7、nt), (7. ). 5.7 , 7. 6 , (232) (505) % (272) (655) % . 7 7.1 7.1.1 KS M ISO 1126 ITZnO(4.3) . , (re-drying) , ITRB(4.2) . 7.1.2 ITRB(7.1.10 7.1.11 ) 1 mg( .) . 3.750 g1 mg ITZnO . 7.1.3 (5.5) , 2.2 cm3 (4.1) (5.2) . 2.2 cm3 2.0 cm3 . 7.1.4 ITZnO (pool) . 7.1.5 (5.4) . 7.1.6 (arm) 0.017 MPa ( 18.4 cm

8、 445 N ) . 25 (mull). 7.1.7 , (scrape) . , , . 2 . 7.1.8 7.1.6 7.1.7 3 . , 425 . 7.1.9 . . 24 . 7.1.10 , 1 2 . 7.1.11 , . N100 N400 0.100 g N500 N700 0.200 g KS M ISO 5435:2012 4 1 IRTB g % 0.090 90 0.100 100 0.110 110 0.120 120 0.130 130 0.140 140 7.2 7.2.1 (5.6) . . 7.2.2 (Erichsen) 7.2.2.1 (5.1 5

9、.5 ) 7.2.2.1.1 6), 517 527 527 (head) . 7.2.2.1.2 , 0.08 mm 0.04 mm (wet film thickness) . 7.2.2.1.3 , 750 mm500 mm10 mm . 7.2.2.2 7.2.2.2.1 . (7.2.2.1.3) . (5.4) , 100 % (7.1.10 ) (mulled) . (7.2.2.1.2) , (2 3) . 7.2.2.2.2 (drawdown) . 3 , 75 mm 3.0 . , . 6) Erichsen Tint Tester Am Iserbach 14, D-5

10、8675 Hemer Erichsen GmbH u. Co KG (： infoerichsen.de) . ISO . KS M ISO 5435:2012 5 7.2.2.2.3 7.2.2.2.1 . , 3 . , . 3.00.02 . 2 . 7.2.2.2.4 , (5.4) . 7.2.2.2.5 , . 7.2.2.2.6 0.02 . 7.2.2.2.7 3 , (7.1.10 ) . 7.2.2.2.8 . (linear) . 7.2.2.2.9 , (4.4) , , . 7.2.2.3 7.2.2.3.1 7.1.1 7.1.10 100 % . 7.2.2.3.

11、2 7.2.2.2.1 7.2.2.2.6 3.0 . 7.2.2.3.3 (7.1.11 ) , 7.1.1 7.1.9 . 7.2.2.3.4 3 , . 7.2.2.3.5 7.2.2.2.8 . 7.2.3 Densichron ( ) 7.2.3.1 (5.1 5.5 ) 7.2.3.1.1 Densichron , 7.2.3.1.2 , 0.08 mm 0.04 mm (wet film thickness) . 7.2.3.1.3 , 750 mm500 mm10 mm . KS M ISO 5435:2012 6 7.2.3.1.4 (tint roller spreader

12、), 7.2.3.2 7.2.3.2.1 7.2.3.2.1.1 (7.2.3.1.3) . (5.4) , 100 % (7.1.10 ) (mulled) . (7.2.3.1.2) , (2 3) . 7.2.3.2.1.2 2 . 3882A 4.76 mm . (drawdown) . 3 , 75 mm 80 . , . 7.2.3.2.1.3 7.2.3.2.1.1 . , 3 . , . 800.5 . 2 . 7.2.3.2.1.4 , (5.4) . 7.2.3.2.1.5 , 0.100 g ITRB . 7.2.3.2.1.6 0.5 . 7.2.3.2.1.7 3 ,

13、 (7.1.10 ) . 7.2.3.2.1.8 . (linear) . 7.2.3.2.1.9 , , (4.4) , , . 7.2.3.2.2 7.2.3.2.2.1 (5.4) , 100 % (7.1.10 ) (mulled) (7.2.3.1.4) . 0 2 . , 80 KS M ISO 5435:2012 7 . 0 . . 100 % 1 2 . 7.2.3.2.2.2 800.5 . 7.2.3.2.2.3 , 0.100 g ITRB . 7.2.3.2.2.4 0.5 . 7.2.3.2.2.5 (7.1.10 ) . 7.2.3.2.2.6 (linear) .

14、 7.2.3.2.2.7 , , (4.4) , , . 7.2.3.3 7.2.3.3.1 7.1.1 7.1.10 100 % . 7.2.3.3.2 7.2.3.2.1.1 7.2.3.2.1.6 7.2.3.2.2.1 7.2.3.2.2.4 80 . 7.2.3.3.3 (7.1.11 ) , 7.1.1 7.1.9 . 7.2.3.3.4 3 , . 7.2.3.3.5 7.2.3.2.2.6 , . 7.2.4 Meeco Colormaster 7.2.4.1 (5.1 5.5 ) 7.2.4.1.1 Meeco Colormaster( ) 7.2.4.1.2 , 750 m

15、m500 mm10 mm . 7.2.4.1.3 , 75 mm50 mm(1.22 mm0.05 mm) . 7.2.4.1.4 , 6.5 mm250 mm . 7.2.4.1.5 ( 1 ) KS M ISO 5435:2012 8 7.2.4.2 7.2.4.2.1 (7.2.4.1.3) . (5.4) , 100 % (7.1.10 ) . 7.2.4.2.2 ( 1 ). (7.2.4.1.4) 3 . . (masking) 0.5 mm ( 1 ). 7.2.4.2.3 . (7.2.4.2.2 ) , . 7.2.4.2.1 7.2.4.2.2 . 0.6 % . 7.2.

16、4.2.4 , 0.100 g ITRB . 7.2.4.2.5 0.6 % . 7.2.4.2.6 (7.1.10 ) . 7.2.4.2.7 (linear) . 7.2.4.2.8 , (4.4) , , . KS M ISO 5435:2012 9 1 (750 mm500 mm10 mm) 2 ( 0.5 mm) 3 4 ( 1.22 mm) 1 Meeco Colormaster 7.2.4.3 7.2.4.3.1 7.1.1 7.1.10 100 % , 7.2.4.2.3 . 7.2.4.3.2 (7.1.11 ) , 7.1.1 7.1.9 . 7.2.4.3.3 7.2.4

17、.2.3 , 7.2.4.2.7 . 7.2.5 Hunter Miniscan 7.2.5.1 (5.1 5.5 ) 7.2.5.1.1 Hunter Miniscan7), XE XE Plus 7) Hunter Miniscan 11491 Sunset Hills Road, Reston, VA 20190-5280 Hunter Associates Laboratory . ISO . KS M ISO 5435:2012 10 7.2.5.1.2 , 0.08 mm 0.04 mm (wet film thickness) . 7.2.5.1.3 , 750 mm500 mm

18、10 mm . 7.2.5.2 7.2.5.2.1 . 7.2.5.2.2 . 7.2.5.2.3 , . CIE XYZ (color scale) D65 10 (observer) 3 7.2.5.2.4 (7.2.5.1.3) . (5.4) , 100 % (7.1.10 ) . (7.2.5.1.2) , (2 3) . 7.2.5.2.5 75 mm 3 . Y- . 0.100 g Y- 2.60 . , . 7.2.5.2.6 7.2.5.2.4 . , 3 . , . Y- Y- 0.02 . . 7.2.5.2.7 , (5.4) . 7.2.5.2.8 , . 7.2.

19、5.2.9 0.02 . 7.2.5.2.10 3 , (7.1.10 ) . 7.2.5.2.11 . (linear) . KS M ISO 5435:2012 11 7.2.5.2.12 , (4.4) , , . 7.2.5.3 7.2.5.3.1 7.1.1 7.1.10 100 % . 7.2.5.3.2 7.2.5.2.4 7.2.5.2.9 . 7.2.5.3.3 (7.1.11 ) , 7.1.1 7.1.9 . 7.2.5.3.4 3 , . 7.2.5.3.5 7.2.5.2.11 , . 7.2.6 Photochron 7.2.6.1 (5.1 5.5 ) 7.2.6.1.1 Photochron8), TR-200P 7.2.6.1.2 , 0.08 mm 0.04 mm (wet film thickness) . 7.2.6.1.3 , 750 mm500 mm10 mm . 7.2.6.2 7.2.6.2.1 . (7.2.6.1.3) . (5.4) , 100 %