KS M ISO 6225-1-2009 Rubber raw natural－Determination of castor oil content－Part 1：Determination of castor oil glyceride content by thin-layer chromatography《天然生胶 蓖麻油含量的测定 第1部分 薄层色.pdf

1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS M ISO 6225 1 1： KS M ISO 6225 1:2009 2009 12 30 http:/www.kats.go.krKS M ISO 6225 1:2009 : ( ) ( ) () () ( ) : (http:/www.standard.go.kr) ： ：2009 12 30 2009-0915 ： ： ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M ISO 6225 1:2009 1： Rubber, raw, natu

2、ral Determination of castor oil content Part 1： Determination of castor oil glyceride content by thin-layer chromatography 2006 2 ISO 6225 1, Rubber, raw, natural Determination of castor oil content Part 1： Determination of castor oil glyceride content by thin-layer chromatography . . . . 1 . . 0.05

3、 % . 2 . . ( ) . KS M ISO 1407, 3 . (spots) KS M ISO 6225 1:2009 2 . 4 . 4.1 , TLC 4.2 ( 40 60 ), 50： 50： 1 . 4.3 4.3.1 (Phosphomolybdic acid), 95 %( ) 100 cm3 15 g . 4.3.2 (Anisaldehyde), 10 cm3, ( 1.84 Mg/m3) 0.5 cm3 0.5 cm3 . 4.4 4.4.1 , . 4.4.2 4.5 4.5.1 0.5 g0.01 g (pharmaceutical grades have b

4、een found satisfactory) (5.8) (4.4.2) 100 cm3 . 4.5.2 5 g , 0.2 %, 0.4 %, 0.6 %, 0.8 % 1.0 %( ) (4.5.1) 2 cm3, 4 cm3, 6 cm3, 8 cm3 10 cm3 (4.4.2) 10 cm3 . 5 1) . 5.1 , (KS M ISO 1407 1, 2 3 ) 5.2 1) (mL) Twelfth Confrence Gnrale des Poids et Mesures cm3 . mL . . KS M ISO 6225 1:2009 3 5.3 (TLC) , 20

5、0 mm200 mm , 0.25 mm (4.1) . . 5.4 (applicator) 5.5 , TLC (5.3) 5.6 , (4.3) . 5.7 , 100 5 . 5.8 , 5 cm3, 10 cm3 100 cm3 . 5.9 , (700 nm1 nm 1 %) , 10 mm . . 6 (bale) 10 g , ( 1 mm3 mm) . , . , 10 g . . 7 7.1 5 g0.1 g (5.1) (thimble) . , . 7.2 7.2.1 (syphon cup) , 100 cm3 (4.4.1) , 10 20 (5.2) 16 . 7

6、.2.2 ( , 2 cm3 .). 7.2.3 10 cm3 (5.8) , (4.4.2) , . 7.2.4 7.2.3 5 L 4.5.2 5 L TLC (5.3) . 7.2.5 TLC (4.2) 100 mm . KS M ISO 6225 1:2009 4 7.2.6 , (4.3.1) (4.3.2) . (5.7) . 10 . “ ” ( , ). “ ” , . (4.3.2) . 7.2.7 , 8.1 8.2.4 . , 8.1 . . 8 8.1 (Rf, 0.2) (spots) (test portion) (%, ) . 8.2 , , . 8.2.1 (

7、8.1 ) , 1 cm3 . . 5 cm3 ( ) . . 8.2.2 (5.9) 700 nm (8.2.1 ) ( ) . . 8.2.3 (spots) (%, ) . 8.2.4 (%, ) . 8.3 0.05 %( ) . 9 . a) b) c) d) e) 1： 153787 1 92 3(13) (02)26240114 (02)262401489 http:/ Korean Agency for Technology and Standards http:/www.kats.go.kr KS M ISO 6225 1:2009 KSKSKS SKSKS KSKS SKS KS SKS KSKS SKSKS KSKSKS Rubber, raw, naturalDetermination of castor oil contentPart 1：Determination of castor oil glyceride content by thin-layer chromatography ICS 83.040.10