KS Q ISO 5496-2009 Sensory analysis－Methodology－Initiation and training of assessors in the detection and recognition of odours《感官分析 方法学 气味检测和辨别评审人员的初级培训》.pdf

1、 KSKSKSKSKSKSKSK KSKSKS KSKSK KSKS KSK KS KS Q ISO 5496 KS Q ISO 5496:2009 2009 1 12 http:/www.kats.go.krKS Q ISO 5496:2009 : ( ) ( ) () () ( ) ( ) ： ( ) ( ) : (http:/www.standard.go.kr) ： ： 2003 8 30 ： 2009 1 12 2009-0012 ： ： ( 02-509-7266) (http:/www.kats.go.kr). 10 5 , . KS Q ISO 5496:2009 i ii .

2、1 1 1 2 .1 3 1 4 .1 5 2 5.1 .2 5.2 .2 6 2 6.1 .3 6.2 .6 7 .8 8 .8 8.1 . 8 8.2 .9 8.3 .9 A( ) .10 B( ) .15 C( ) .16 KS Q ISO 5496:2009 ii , . , . . . KS Q ISO 5496:2009 Sensory analysis Methodology Initiation and training of assessors in the detection and recognition of odours 2006 2 ISO 5496, Sensor

3、y analysis Methodology Initiation and training of assessors in the detection and recognition of odours . 1 . ( , , , ) . 2 . . ( ) . KS Q ISO 6658, KS Q ISO 85891), 3 4 4.1 , , , , 4.2 , 96.9 %( ), 1) (ISO 8589： 1998 KS Q ISO 8589： 2009 ). KS Q ISO 5496:2009 2 4.3 , . 4.4 , . a) A.2 , / b) , (： , )

4、( ). (： , ) . . (5 ) , . . 5 5.1 KS Q ISO 8589 . (： ). 5.2 KS Q ISO 6658 , 20 . , 10 . 6 (retro-nasal) . 2) . , (6.1.1) (smelling strips) (6.1.2) (6.1.3) 2) . KS Q ISO 5496:2009 3 . , (6.2.1) (6.2.2) 6.1 6.1.1 6.1.1.1 . 6.1.1.2 6.1.1.2.1 A.2 . 6.1.1.3 6.1.1.3.1 , , , ( 20 mL 125 mL ) . , . , . 6.1.1

5、.4 , A.2 A.1 . 30 , . . , . (： ) (： ) . . 6.1.1.5 KS Q ISO 5496:2009 4 . . , 1 . , (： ) . , , (7. ) ( B ). . 6.1.1.6 8. . 6.1.2 6.1.2.1 . 6.1.2.2 6.1.2.2.1 , A.2 . 6.1.2.3 6.1.2.3.1 , 50 mm 100 mm ( , )3) 6.1.2.3.2 (Strip-holders) , . 6.1.2.3.3 , ( 1 ). 6.1.2.3.4 ( ) 6.1.2.4 A.2 (stock solutions) .

6、. 1 (6.1.2.3.1) ( ). (6.1.2.3.4) 3) (aromatic products) . KS Q ISO 5496:2009 5 . . 5 mm 10 mm . (6.1.2.3.2) . . 6.1.2.5 . cm . , . . , (7. )( B ). . . 6.1.2.6 8. . 6.1.3 6.1.3.1 (micro-encapsulated) . 6.1.3.2 6.1.3.2.1 , A.2 . 6.1.3.3 6.1.3.3.1 , 4) . 6.1.3.4 4) (microcapsules) . . KS Q ISO 5496:200

7、9 6 . 6.1.3.5 . . (6.1.2.5 ). . , (7. )( B ). . . 6.1.3.6 8. . 6.2 6.2.1 5) 6.2.1.1 6.2.1.2 6.2.1.2.1 , A.2 . 6.2.1.3 ( ) . , . 6.2.1.3.1 , 100 mL . 6.2.1.3.2 , . 6.2.1.3.3 5) . . . C .KS Q ISO 5496:2009 7 6.2.1.4 , A.2 A.1 . . 50 mL . 6.2.1.5 1 . . . . . (7. )( B ). . 6.2.1.6 8. . 6.2.2 6.2.2.1 . .

8、6)6.2.2.2 6.2.2.2.1 , , A.2 . 6.2.2.3 6.2.2.3.1 , . 6.2.2.4 , A.2 A.1 . . 6) , . KS Q ISO 5496:2009 8 . 6.2.2.5 . , . . . . , (retro-nasal) . , (7. )( B ). 6.2.2.6 8. . 7 . (perceive) ? (recognize) ? . , . ( B ) . 8 , . . . a) , ( ), , , . b) , . 8.1 KS Q ISO 5496:2009 9 , . . . , . 8.2 . . . 8.3 .

9、. KS Q ISO 5496:2009 10 A ( ) A.1 A.1.1 , . A.2 A.2.1 (stock solution, SS) 1 g 100 g (4.2). A.2.2 (working solution, WS) 1 g 100 g (4.2). A.2.3 A.1 . A.3 A.2 . A.2 . A.1 g/L 1 0.1 g 1 L . 10 52 0.5 g 1 L . 510 53 1 g 1 L . 10 44 5 g 1 L . 510 45 10 g 1 L . 10 36 50 g 1 L . 510 37a1 g 1 L . 10 28a5 g

10、 1 L . 510 2 a 2 %(m/m) . KS Q ISO 5496:2009 11 A.2 A.1 c ab 1 - (D-Limonene) C10H16 , 6 SS 7 5 2 (Citral geranial + neral ) C10H16O 5 SS 6 4 3 (Geraniol) C10H18O 5 SS 6 4 4 -3- -1- (cis-3-Hexen-1-ol) C6H12O 6 SS 7 5 5 (Benzaldehyde) C7H6O , (marzipan) 6 SS 7 5 6 (Butyric acid) C4H8O2 , (： ), 5 SS 6

11、 4 7 (Ethyl butanoate) C6H12O2 , 4 SS 5 3 8 (Benzyl acetate) C9H10O2 , , , 5 SS 8 6 9 - (-Undecalactone) C11H20O2 , 6 SS 7 5 10 2- (2-Phenylethanol) C8H10O , 8 SS 8 7 11 (Methyl anthranilate) C8H9O2 4 SS 5 3 12 (Ethyl phenyl acetate) C10H12O2 , 4 SS 5 3 13 (Anethole) C10H12O 3 SS 4 2 14 (Cinnamaldeh

12、yde) C9H8O 6 SS 7 5 15 (Vanillin) C8H8O3 5 SS 6 4 16 L- (L-Methol) C10H20O d6 SS 8 6 17 (Terpinyl acetate) C12H20O2 , 4 SS 5 3 18 (Thymol) C10H14O , 4 SS 5 3 19 (Diacetyl) C4H6O2 4 SS 4 4 20 - (-Nonalactone) C9H16O2 4 SS 4 4 21 (Eugenol) C10H12O2 SS 5 3 22 1- -3- (1-Octen-3-ol) C8H16O , 4 SS 5 3 23

13、- (-lonone) C13H22O 4 SS 4 4 24 (Methional) C4H8OS , 5 SS 6 4 a . b A.3 . c . 70 % . d . KS Q ISO 5496:2009 12 A.3 1 - (D-Limonene) 2 ( + ) Citral (neral + geranial) 3 (Geraniol) 4 -3- -1- (cis-3-Hexen-1-ol) 5 (Benzaldehyde) 6 (Butyric acid) 7 (Ethyl butanoate) 8 (Benzyl acetate) 9 - (-Undecalactone

14、) 10 2- (2-Phenylethanol) KS Q ISO 5496:2009 13 A.3 ( ) 11 (Methyl anthranilate) 12 (Ethyl phenyl acetate) 13 (Anethole) 14 (Cinnamaldehyde) 15 (Vanillin) 16 L- (L-Menthol) 17 (Terpinyl acetate) KS Q ISO 5496:2009 14 A.3 ( ) 18 (Thymol) 19 (Diacetyl) 20 - (-Nonalactone) 21 (Eugenol) 22 1- -3- (1-Oct

15、en-3-ol) 23 - (-lonone) 24 (Methional) CH3 S CH2CH2CHO KS Q ISO 5496:2009 15 B ( ) ： ： ： ?a ?a , a X . KS Q ISO 5496:2009 16 C ( ) C.1 . . C.2 C.2.1 , A.2 . C.3 C.3.1 , ( , )7) . C.3.2 , . C.3.3 , ( ). C.3.4 ( ) C.4 , A.1 A.2 . . (C.3.1)( ). (C.3.4) . . 5 mm 10 mm . , (C.3.2) . . 7) . KS Q ISO 5496:2009 17 C.5 . . . (