NAVISTAR MPAPS K-6927-2016 Glass Bonding Part 1 and 2.pdf

1、This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 1 of 14 NAVISTAR, INC. Material, Parts, and Process Specificati

2、ons (MPAPS) NUMBER: MPAPS K - 6927 Former Designation: TMS-6927 TITLE: Glass Bonding: Part 1 and 2 CURRENT REV No.: 1602 DATE: Feb. 2016 WRITTEN/EDITED BY: S. Brailey APPROVED BY: R. Goluch SUPERSEDES: Rev. 1504 April 2015 PRINTED COPIES OF THIS DOCUMENT MUST BE VERIFIED FOR CURRENT REVISION This sp

3、ecification may involve hazardous materials, equipment, and procedures. This specification does not purport to address all of the safety issues associated with its use. The user is responsible to consult appropriate safety and health practices and to determine the applicability of regulatory limits

4、prior to use. Change Notice: Changed 9000 bead dimensions Part 2 Table 1 1.0 APPLICATION Part 1 of the specification covers material properties, performance requirements, production quality control, suppliers responsibilities, source approvals and quality controls, in addition to approved sources fo

5、r adhesive systems. Part 2 of the specification covers manufacturing and assembly process controls and general information. 2.0 SCOPE This specification covers bonding systems, including adhesives and primers, used for bonding glass in the construction of truck and tractor cabs, sleeper boxes, and/o

6、r other parts used in truck cab manufacturing. The bonds developed by these systems retain adhesion and physical properties while resisting exposure to weathering conditions. 2.1 Restricted Chemical Substances Effective January 1, 2007, all product supplied to the requirements of this specification

7、must comply with the requirements of the MPAPS B-50 specification. 3.0 REFERENCE DOCUMENTS Unless otherwise specified, the latest issue of all referenced standards shall apply. The following Specifications, Standards, and Regulations are referenced in this specification. Quality System Std ISO 9001

8、or TS-16949 ASTM B117 SAE J1720 NAVISTAR Engineering Design Std. A-16 ASTM D2247 SAE J1721 NAVISTAR Manufacturing Std. MS-D-13 ASTM D2369 SAE J1885 CFR Title 29, Section 1910 ASTM D2196 SAE J243 NAVISTAR MPAPS B-50 NAVISTAR MPAPS G-5 ASTM D1084 ASTM D1200 SAE J1529 NAVISTAR TMS-6915 ASTM G53 NAVISTA

9、R MPAPS D-7016 NAVISTAR TMS-9522 NAVISTAR MPAPS P-9543 NUMBER: MPAPS K - 6927 TITLE: Glass Bonding: Part 1 and 2 REVISION: 1602 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume

10、 all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 2 of 14 Part 1 General, Property, and Performance Requirements 4.0 REQUIREMENTS Material supplied to this specification shall bond glass and substrates together to produce a permanent structural bond. General properties of received mat

11、erials, in the uncured state, are shown in Table 3. 4.1 Compatibility Material supplied to this specification shall be compatible with all subsequent cleaning, pre-treatment, and paint operations for the assembly plant process, in addition to material substrate combinations for which the bonding sys

12、tem approval is sought. It is the adhesive suppliers responsibility to demonstrate and insure compatibility of the bond systems materials and procedures with the assembly plant material and process combinations. 4.2 Uncured Properties See Table 3 for specific requirements for each material. Test pro

13、perties and methods are shown below. Requirement: Test Method Percent Solids ASTM D 2369 Viscosity - Method A SAE J243, Procedure ADS-1, Unagitated, Conditioning Method A, Pressure Flow Method 275 kPa (40 psi), 25 1C (77 2F), 20 g. - Method B ASTM D 1200, Cup #4, 24C. - Method C ASTM D 2196, Method

14、A. - Method D ASTM D 1084, Cup #1, 24C 4.3 Cured Properties 4.3.1 Sample Preparation A minimum of five samples shall be prepared for each test condition and substrate unless otherwise specified. Prepare glass samples per SAE J1529 except as indicated below. The surface condition tested shall be repr

15、esentative of production conditions and will be fully described in the test report. The cure condition shall also be representative of production conditions and be described fully in the test report. The test conditions will be listed in Table 1 and be reproducible for future testing. Substrate test

16、 matrices are described in section 5.0 Qualification. 4.3.2 Lap Shear Strength 4.3.2.1 Method: Prepare samples as directed in Sample Preparation (Section 4.3.1). Test per SAE J1529, as appropriate. Tensile machine jaw separation rate shall be 13 mm (.5 in) per minute. Test overlap shear at the follo

17、wing specified temperatures (listed in Table 1) after holding at temperature for 30 minutes. Report the average of five tests and their failure modes. 4.3.2.2 Required: See Table 1 for requirements and APPROVED SUBSTRATES list in Table 2. 4.3.3 Corrosion 4.3.3.1 Method: Prepare samples as directed i

18、n Sample Preparation (Section 4.3.1). Test per ASTM B117 salt spray test for the length of time listed in Table 1. 4.3.3.2 Required: See Table 1. NUMBER: MPAPS K - 6927 TITLE: Glass Bonding: Part 1 and 2 REVISION: 1602 This document is restricted and may not be sent outside Navistar, Inc. or reprodu

19、ced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 3 of 14 4.3.4 Water Immersion 4.3.4.1 Method: Prepare samples as directed in Sample Preparation (Section 4.3.1). Immerse samples in distilled wa

20、ter at 38 C (100 F) 2 C (3.6 F) for 240 hours. 4.3.4.2 Required: See Table 1. 4.3.5 Humidity 4.3.5.1 Method: Prepare samples as directed in Sample Preparation (Section 4.3.1). Test per ASTM D2247 for the length of time listed in Table 1. 4.3.5.2 Required: See Table 1. 4.3.6 Heat-Aging 4.3.6.1 Method

21、: Prepare samples for lap shear strength test. Heat-age in a recirculating air oven for 330 hours at 82 2C (180 3.6F). 4.3.6.2 Required: See Table 1. 4.3.7 Accelerated Weathering 4.3.7.1 Method A QUV: Perform 500 hours QUV-B (FS40 bulbs) test as per ASTM G53. Cycle = 8 hours UV 140F - 4 hours dark c

22、ondensing humidity 122F - repeat cycle for test duration 4.3.7.1.1 Required: See Table 1. Material should not crack, lose adhesion, nor have more than a slight color change. 4.3.7.2 Method B Weatherometer: Test per SAE J1885 on samples prepared for shear strength. Test for 2000 hours. 4.3.7.2.1 Requ

23、ired: See Table 1. Material should not crack, lose adhesion, nor have more than a slight color change. 4.3.8 Quick Knife Adhesion 4.3.8.1 Method: Prepare and test specimens per SAE J1720. 4.3.8.2 Required: Test specimens should exhibit cohesive failure. 4.3.9 Tape Link-Up 4.3.9.1 Method: Prepare and

24、 test specimens per SAE J1721. 4.3.9.2 Required: Test specimens exhibit 100% adhesion in less than eight hours. 4.3.10 Cold-Crack 4.3.0.1 Method: Prepare and test specimens per MPAPS GT Paint, GT-14C. 4.3.0.2 Required: See Table 1. Material should not crack, lose adhesion, nor have more than a sligh

25、t color change. 4.3.11Time Study A quick knife test study shall be performed to determine open time of the top-coat to receive the new adhesive system. The adhesive is to be applied to topcoat at 4hr, 72hr, 7 days, and 14 days from the topcoat being cured under nominal top coat bake conditions as de

26、scribed in section 5.0. The top coated panels shall be stored at standard laboratory conditions during the waiting period. Test conditions shall be initial adhesion and humidity exposure. In addition two colors shall be tested NAV9219 and NAV2503. NUMBER: MPAPS K - 6927 TITLE: Glass Bonding: Part 1

27、and 2 REVISION: 1602 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 4 of 14 5.0 QUALITY Materials and processe

28、s submitted for approval to this specification shall include a detailed, signed test report per MPAPS P 9543, test coupons or photographs showing failure modes for each test, the complete test procedure, and a description of the adhesive, substrate(s), and any chemicals/primers used for bonding. 5.1

29、 E-Coat Test Matrix Each new material must be tested with current E-coat substrates using a nine-condition test matrix. The matrix evaluates the adhesion of the urethane to E-coated panels that have been exposed to nominal oven conditions of 30 minutes at 350 F, over-bake conditions of 60 minutes at

30、 390 F, and under-bake conditions of 15 minutes at 325 F. The matrix includes test conditions in which film thickness is varied at 0.6 mil, 0.9 mil, and 1.2 mil. Ten (10) 4“x12“ panels are tested at each condition. 5.2 Primerless to Top Coat - Full Substrate Test Matrix Each new material seeking pri

31、merless approval to top coat must be tested with current top coated substrates at nominal (30min 250F), under bake (20min 200F), and over bake conditions (40min 260F). Paint film build shall be nominal as recommended by the paint manufacturer. The adhesive shall be applied to the fresh top coat with

32、out prior ageing of the top coat and within the nominal manufacturing cycle time. The test matrix is to include the current base coat/clear coat system at catalyzed and uncatalyzed clear coat conditions in the following colors: NAV0001, NAV9219, NAV2503, and NAV4587. The test matrix is also to inclu

33、de thermoset acrylic monocoats, catalyzed and uncatalyzed urethane monocoats, and re-paint base coat/clear coat panels simulating two and three tone paint jobs. 5.3 Primerless to Top Coat - Screening Substrate Test Matrix In the event of material screening the Full Test Matrix may be truncated to in

34、clude only the nominal bake, one pass, base coat/clear coat panels on all four colors as described in Section 5.6, and omitting the accelerated weathering and cold crack tests. 5.4 Primerless to Top Coat - Manufacturing Validation Test Matrix Manufacturing validation shall consist of a 9 week panel

35、audit at each plant. A total of four colors and four panels per color shall be tested per week per plant by quick knife adhesion at initial conditions and after 240hrs of humidity exposure. The panels shall be tested as quickly as possible upon receipt from the plant. 6.0 QUALIFICATION 6.1 Quality C

36、ontrol Plan A Quality Control Plan for products supplied to the requirements of this specification will be established by mutual agreement between NAVISTAR and the supplier. Unless specific exception is noted, the following characteristics, where applicable*, shall be included in the plan as feature

37、s for management by statistical process control.* * Other characteristics for inclusion in the control plan may be specified on the engineering drawing and/or purchase order. * See NAVISTAR Engineering Design Standard A-16 Bead height NUMBER: MPAPS K - 6927 TITLE: Glass Bonding: Part 1 and 2 REVISIO

38、N: 1602 This document is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 5 of 14 7.0 SOURCE APPROVAL AND QUALITY CONTROL 7.1 Sup

39、plier Requirements All suppliers to NAVISTAR are required to be registered to ISO 9001 Quality System Requirements. NAVISTAR will also accept TS-16949 registration as long as the supplier can also fulfill all AIAG PPAP (Production Part Approval Process) documentation and approval requirements. Suppl

40、iers must maintain their certification with an accredited registrar and must furnish copies of registration certificates to their Corporate Buyer upon request. 7.2 Approval Parts supplied against contracts or purchase orders citing this specification shall be equivalent in all respects to those samp

41、les which were approved by the purchaser. No changes in formulation or processing practices are permitted without approval. In the event that changes in material, properties, processing practices, construction, color, or labeling of the product are required, the supplier shall notify NAVISTAR Materi

42、als Engineering and Purchasing and Supplier Development of the proposed change(s). Test data indicating conformance to all requirements of this specification, test samples, and new or amended or updated Material Safety Data Sheet(s) (MSDS), in accordance with CFR Title 29, Part 1910 shall be submitt

43、ed with the request for change. 7.3 Process Control The supplier shall either perform and report results of tests on specific lots of parts produced using ISO 9001 or TS-16949 guidelines, or provide statistical evidence of the lot having been produced in a state of statistical control and with a pro

44、cess capable of providing all required properties. The part supplier and the quality control manager of the using NAVISTAR plant may determine testing and reporting requirements on specific products. 8.0 SHIPPING AND HANDLING Shipping and identification shall be in accordance with NAVISTAR Manufactu

45、ring Standard MS-D-13. Parts shall be packaged so as to avoid any damage in shipment detrimental to the appearance of the part. 9.0 DESIGNATION ON DRAWINGS Example of note to use on drawings: Bond per MPAPS K-6927 or Bond per MPAPS K-6927, System A (to designate the adhesive system) Adhesive per MPA

46、PS K-6927 or Adhesive A4/A5 MPAPS K-6927 (to designate a single specific material) 10.0 TECHNICAL INFORMATION For further information related to the technical content of this specification, contact: Suppliers may purchase controlled copies of this specification by contacting: Materials Engineering a

47、nd Technology Dept. 10400 W. North Avenue Melrose Park, IL 60160 E-mail: MaterialsEngineeringN IHS Global Inc. 15 Inverness Way East Englewood CO 80112-5776 Phone: 1-800-854-7179 E-mail: AutomotiveIHS.com Website: http:/ NUMBER: MPAPS K - 6927 TITLE: Glass Bonding: Part 1 and 2 REVISION: 1602 This d

48、ocument is restricted and may not be sent outside Navistar, Inc. or reproduced without permission from Corporate Technical Standards. Suppliers are required to assume all patent liability. 2016 by Navistar, Inc. FEBRUARY 2016 Page 6 of 14 A.0 GENERAL INFORMATION TABLE 1: BOND STRENGTH (1) E-Coated M

49、aterial to Glass Quick Knife Condition Lap Shear. (3) Min Percentage of Qualification Value Retained. MPa psi 23 2C (73 3.6F) * (2) 3.5 500 (1) Pass (1) -40 2C (-40 3.6F) * 95 %(1) N/A * 70 2C (158 3.6F) * 75% (1) N/A * 330 h Heat Age (158 3.6F) * 90% (1) Pass (1) 240 h Water Immersion 85% (1) Pass (1) 240 h Humidity 90% (1) Pass (1) 500