NAVY MIL-L-82653 A-1993 LINER MATERIAL POLYBUTADIENE BASE《聚丁二烯基内衬材料》.pdf

1、c 14 MIL-L-82653A 9999906 L972363 bbb I INCH-POUND I MIL-L-82653A(OS) 15 November 1993 SUPERSEDING 3 1 January 1977 MIL-A-82653(OS) MILITARY SPECIFICATION LINER MATERIAL, POLYBUTADIENE BASE %is specification is approved for use by the Naval Sea Systems Command, Department of the Navy, and is availab

2、le for use by all Departments and Agencies of the Department of Defense. 1. SCOPE 1.1 Scope. This specification covers three types of polybutadiene base liner materials. 1.2 Classification. The liner materials shall be of the following types as specified in the contract or order (see 6.2): Type I CC

3、U-22/A Impulse Cartridge, CCU-22/A/A Impulse Cartridge, or CKU- 7/A Rocket Catapult liner material. Type JI CKU-S/A Rocket Catapult and CKU-S/A/A Rocket Catapult liner material. Type III CKU-SBIA Rocket Catapult liner material. 2. APPLICABLE DOCUMENTS 2.1 Government documents. 2.1.1 Specifications.

4、The following specifications form a part of this document to the extent specified herein. Unless otherwise specified, the issues of these documents are those listed in the issue of the Department of Defense Index of Specifications and Standards (DODISS) and supplements thereto, cited in the solicita

5、tion (see 6.2). AMSC N/A FSC 1377 a DISTRIBUTION STATEMENT A: Approved for public release; distribution is unlimited. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-SPECIFICATIONS MILITARY MIL-P-23942 Polybutadiene, Linear, Carboxyl-Terminated DOD-C

6、-82656 Carbon Black, Thermal MIL-R-82657 Resin, Epoxy, Trifunctional MIL-P-82658 Polymer, Liquid, Polybutadiene, Carboxyl-Terminated DOD-C-82660 Chromium 2-Ethyl Hexoate DOD-C-82665 Carbon Black DOD-T-82666 Tris-l-(2-Methyl Aziridinyl) Phosphine Oxide (Unless otherwise indicated, copies of military

7、specifications are available from Standardization Documents Order Desk, Bldg. 4D, O0 Robbins Avenue, Philadelphia, PA 191 11-5094.) 2.2 Non-Government publications. The following document forms a part of this document to the extent specified herein. Unless otherwise specified, the issues of the docu

8、ments which are DOD adopted are those listed in the issue of the DODISS cited in the solicitation. Unless otherwise specified, the issues of documents not listed in the DODISS are the issues of the documents cited in the solicitation (see 6.2). CHEMICAL PROPULSION INFORMATION AGENCY CPIA Publication

9、 No. 21 JANNAF Solid Propellant Mechanical Behavior Manual (Application for copies should be addressed to the Chemical Propulsion Information Agency, Applied Physics Laboratory, Johns Hopkins University, Johns Hopkins Road, Laurel, MD 20810.) (Non-Government standards and other publications are norm

10、ally available from the organizations that prepare or distribute the documents. These documents also may be available in or through libraries or other informational services.) 2.3 Order of precedence. In the event of a conflict between the text of this document and the references cited herein, the t

11、ext of this document takes precedence. Nothing in this document, however supersedes applicable laws and regulations unless a specific exemption has been obtained. 3. REQUIREMENTS 3.1 Material. The liner material shall be polybutadiene-based compositions as specified herein. 3.2 Chemical composition.

12、 The chemical composition shall be in accordance with table I. The ingredients shall be in accordance with the referenced documents. 2 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-L-82653A W 99999Ob l19723b5 439 W TABLE I. Liner ingredients an

13、d composition, Material Liauid Polvmer, CTPB Linear CTPB Carbon Black Carbon Black, Thermal Chromium 2-Ethyl Hexoate Epoxy Resin, Trifunctional Tris-1 42-Methyl Aziridinyl) Phosphine Oxide Weight Perc Specification Type II Type I MIL-P-82658 - 83.31 2 MIL-P-23942 87.84 - Tvpe II DOD-C-82665 I - I 8.

14、86 DOD-C-82656 I 10.00 I DOD-C-82660 I 0.1 24 I - MIL-R-82657 I 6.564 I - DOD-T-82666 I - 1 3.30 Grade B nt Type 111 86.814 - 6.2325 0.0205 6.933 - 3.3 Modification of liner formulation. 3.3.1 Modification of Type I liner formulation. The properties of the Type I liner may be varied by changing the

15、ratio of epoxy resin to polybutadiene. The total weight percent of epoxy resin, catalyst, and polybutadiene must remain constant at 90.0 percent. 3.3.2 Modification of Type II liner formulation. The properties of the Type II liner may be varied by changing the ratio of Tris-l-(2-Methyl Aziridinyl) P

16、hosphine Oxide to polybutadiene. The total weight percent of Tris-l-(2-Methyl Aziridinyl) Phosphine Oxide and polybutadiene must remain constant at 91.14 percent. 3.3.3 Modification of Type III liner formulation. The properties of the Type III liner may be varied by changing the ratio of epoxy resin

17、 to polybutadiene. The total weight percent of epoxy resin, catalyst, and polybutadiene must remain constant at 93.7675 percent. 3.4 Propellant-to-liner bond strength. Propellant-to-liner bond strength testing shall be required before a new liner ingredient lot set or liner formulation modification

18、(see 4.3.1) is used. the propellant- to-liner bond shall exhibit cohesive failure in the propellant web when tested at 77 f 5F. 3.5 Workmanship. The material shall be uniform and free from contamination and foreign material that would prevent its use for the purpose intended. 4. QUALITY ASSURANCE PR

19、OVISIONS 4.1 Responsibility for inspection. Unless otherwise specified in the contract or purchase order, the contractor is responsible for the performance of all inspection requirements (examinations and tests) as specified herein. Except as otherwise specified in the contract or purchase order, th

20、e contractor may use 3 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-L-82b53A m 9999906 19723bb 375 m MIL-L-82653A(OS) I .4 his own or any other facilities suitable for the performance of the inspection requirements specified herein, unless dis

21、approved by the Government. The Government reserves the right to perform any of the inspections set forth in this specification where such inspections are deemed necessary to ensure supplies and services conform to prescribed requirements (see 6.2). 4.1.1 Responsibility for compliance. All items sha

22、ll meet all requirements of sections 3 and 5. The inspection set forth in this specification shall become a part of the contractors overall inspection system or quality program. The absence of any inspection requirements in the specification shall not relieve the contractor of the responsibility of

23、ensuring that all products or supplies submitted to the Government for acceptance comply with all requirements of the contract. Sampling inspection, as part of manufacturing operations, is an acceptable practice to ascertain conformance to requirements; however, this does not authorize submission of

24、 known defective material, either indicated or actual, nor does it commit the Government to acceptance of defective material. 4.2 Inspection conditions. Unless otherwise specified (see 6.2), all inspections shall be performed as specified in the applicable test method of 4.4. 4.3 Quality conformance

25、 inspection. Quality conformance inspection shall consist of the tests specified in 4.4.1, 4.4.2, and 4.4.3. When specified in the contract, the contractor shall prepare a report giving the results obtained for all inspections and tests performed and a certified statement that meets all requirements

26、 of this specification (see 6.2). 4.3.1 Inspection lot. An inspection lot shall consist of a single liner mix. 4.3.1.1 Liner mix. A liner mix shall consist of one homogeneous blend of ingredients (see 3.2) manufactured at one time in one mixing vessel. 4.3.1.2 Ingredient lot. The ingredient lot set

27、shall be a set of the materials as specified in table I for each type of liner material, where each of the materials is from a single material lot that is acceptable under the quality provisions of this specification. If one or more of the material lots is changed from an established ingredient lot

28、set this constitutes a new ingredient lot set. If the formulation (the weight percent of the individual ingredients) established with a new ingredient lot set is maintained, no additional testing (see 3.4.1) is required. The testing of 3.4.1 shall be performed if any formulation modification is requ

29、ired with an ingredient lot set, or if the ingredient lot set changes. 4.4 Test methods. Unless an alternative inspection method is proposed, tests shall be performed using apparatus and procedures specified herein. Alternative inspection methods may be proposed by the supplier but must be approved

30、by the contracting activity prior to use in acceptance testing. 4.4.1 Ingredient weight. Each liner ingredient shall be weighed to determine compliance with 3.2 prior to mixing. Weights shall be measured with equipment having an accuracy of & 1 percent of the ingredient weight calculated from the pe

31、rcentages specified in the applicable table (see 3.2). 4.4.2 Raw material. Each liner raw material shall be tested to determine compliance with 3.2. 4 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-L-82653A(OS) a 4.4.3 Bond strength. The liner b

32、ond strength specimens shall be prepared and tested in accordance with CPIA Publication No. 21, section 4.7.2. A minimum of 4 samples shall be tested to determine compliance with 3.4. l. 4.4.3.1 Liner test specimen. The propellant from the propellant mix used to cast the test specimens shall meet th

33、e propellant mechanical properties specified in the applicable propellant specification before the liner bond test is completed. If the propellant does not meet the mechanical properties specified in the applicable propellant specification, all bond testing completed with that propellant mix shall b

34、e deemed invalid. a. Sandblast and degrease the inside of the gripping sleeve and the anvil disc using the same solvent used on the motor tubes. b. Coat the inside of the gripping sleeve with a thin layer of liner. Coat the exposed side of the insulator disc with liner, so that, as a minimum, the in

35、sulator disc is fully covered by liner, c. Cure the liner at 170 & 5F for 14 to 18 hours. d. Assemble the test specimen as shown on figure 4.7.2-1 of CPIA Publication No. 21. e. Cast propelIant into the steel tube and cure with the propellant mix as specified in the applicable propellant specificati

36、on. O 5. PACKAGING - (This section is not applicable to this specification.) 6. NOTES (This section contains information of a general or explanatory nature that may be helpful but is not mandatory.) 6.1 Intended use. The liners described herein are used between the case or tube wall and the propella

37、nt of various cartridge devices and rocket motors, specifically: Type I Used in the CCU-22/A Impulse Cartridge, CCU-22/A/A Impulse Cartridge, and the CKU-7/A Rocket Catapult. Type II Used in the CKU-SIA Rocket Catapult and the CKU-SIAIA Rocket Catapult. Type III Used in the CKU-SB/A Rocket Catapult.

38、 5 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-d flIL-L-82653A m 9999906 L972368 148 m MIL-L-82653A(OS) 6.2 Acquisition requirements. Acquisition documents must specify the following: a. Title, number, and date of this specification. b. Issue of

39、DODISS to be cited in the solicitation and, if required, the specific issue of individual documents referenced (see 2. l. 1 and 2.1.2). c. Inspection conditions, if other than as specified (see 4.2). d. Whether Type I, Type II, or Type III material is required (see 1.2). e. Whether the contractor is

40、 responsible for inspection (see 4.1). f. Whether a quality conformance test report is required (see 4.3). 6.3 Data requirements. The following data requirements should be considered when this specification is applied on a contract. The applicable Data Item Descriptions (DIDS) should be reviewed in

41、conjunction with the specific acquisition to ensure that only essential data are requested/provided and that the DIDs are tailored to reflect the requirements of the specific acquisition. To ensure correct contractual application of the data requirements, a Contract Data Requirements List D Form 142

42、3) must be prepared to obtain the data, except where DOD FAR Supplement 27.475-1 exempts the requirement for a DD Form 1423. Ref, ParagraDh DID Number DID Title Tailoring 4.3 DI-T-2072 Reports, Test - me above DID was cleared as of the date of this specification. The current issue of DOD 5010.12-L,

43、Acquisition Management Systems and Data Requirements Control List (AMSDL), must be researched to ensure that only current, cleared DIDs are cited on the DD Form 1423.) 6.4 Manufacturing conditions. This material has been manufactured (processed, applied, and cured) successfully under the following c

44、onditions: a. Humidity: 50 grains of water per pound of dry air, maximum b. Temperature: 21 to 32C (70 to 90F) 6.5 Shelf life. The shelf life of the liner material when kept in a frozen condition in sealed containers is 6 months. 6.6 Changes from previous issue. Marginal notations are not used in th

45、is revision to identify changes with respect to the previous issue due to the extensiveness of the changes. 6 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-6.7 Subject term (keyword) listing. Impulse Cartridge Rocket Catapult Preparing activity (Project 1377-NESS) Navy - OS 7 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-