SN T 4675.31-2019 出口葡萄酒中丙三醇碳稳定同位素比值的测定 液相色谱-稳定同位素比值质谱法.pdf

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1、书书书 犐犆犛 犆 G21G22G23G24G25G26G27G28G29G2AG2BG2CG2BG2DG2EG2FG30G31 犛犖 犜 G28G32G33G34G35G21G36G37G38G39G3AG3BG3CG3DG3EG3FG40G41G42G3B G43G44G45G46 G3AG3BG3CG3DG3EG3FG40G47G46G48 犇犲狋犲狉犿犻狀犪狋犻狅狀狅犳犮犪狉犫狅狀狊狋犪犫犾犲犻狊狅狋狅 狆 犲狉犪狋犻狅狅犳 犵 犾 狔 犮犲狉狅犾犻狀狑犻狀犲犳狅狉犲狓 狆 狅狉犲 犔犆犐犚犕犛犿犲狋犺狅犱 G49G4A G4BG4C G21G22G23G24G25G26G27G28G

2、29G2AG2B G49 G4A 书书书 G21 G22 G21G22G23G24 G25G26G21: G27 G26G21:G28G29G2AG2BG2CG2DG2EG2FG30G31G32 G33G34; G27 G26G21:G28G29G2AG2BG2CG2D , G35G36G37G30G31G32 G38G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG3CG37G3DG32G3EG3FG40G41G42G43G30G31G32; G27 G26G21:G28G29G2AG2BG2CG2DG44G45G30G31G32 G33G34; G27

3、 G26G21:G28G29G2AG2BG2CG2DG46G47G45G30G31G32 G48G49G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG2AG2BG4A、G4BG4AG4CG4DG4AG30G31G32; G27 G26G21:G28G29G2AG2BG2CG2DG3CG4EG30G31G32 G38G39G3AG3B G4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2D G50G51G52G53G4EG30G31G32 G54G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG36

4、G2EG37G30G31G32 G38G39G3AG3B G4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG55G56G57G58G41 G30G31G32 G54G39G3AG3B G4FG3BG4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2D G59G5AG3AG5BG30G31G32 G5CG5DG5EG54G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG5FG60G33G30G31G32 G54G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2D ,

5、, G61G62G63G51G64G65G66G67G30G31 G38G39G3AG3B G4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG68G69G57G41G30G31G32 G54G39G3AG3B G4FG3BG4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG6AG6BG45、G6CG6DG3CG45G4CG6EG62G63G51G45G30G31G32 G54G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG6FG70G45G30G31G32 G54G39G3AG3B G4FG3

6、BG4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG35G52G71G72G67G30G31G32 G38G39G3AG3B G4FG3BG4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG36G73G74G75G52G51G45G76G65G66G67G30G31G32 G77G78G38G39G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG79、G7A、G7B、G7C、G7D、G7E、G7F、G80、G81、G82、G83、G84、G85、G86G30G31G32; G27 G26G21:G28

7、G29G2AG2BG2CG2DG87G88G89G41G30G31G32 G8AG8BG8CG8DG8EG48G49G8FG4FG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG90G5FG91G92G47G93G30G31G32 G48G49G3AG3BG34; G27 G26G21:G28G29G2AG2BG2CG2DG94G36G95G96G73G30G31G32 G42G3AG34; G27 G26G21:G28G29G2AG2BG2CG97G2AG2BG98G2DG75G99G30G31G32 G9AG9BG9CG9DG21G9EG9FG34; G27 G2

8、6G21:G28G29G2AG2BG2CGA0GA1GA2GA3GA4GA5G30G31G32 G21GA6GA6GA7GA8G34; G27 G26G21:G28G29G2AG2BG2CGA9G3AG30G31G32 ( )G3AG78GAAG34; G27 G26G21:G28G29G2AG2BG2CGABGA7G30G31G32 GACGADGA6G34; G27 G26G21:G28G29G2AG2BG2CGAEG91GAFG21G30G31G32; G27 G26G21:G28G29G2AG2BG2CG2DGB0G60、G57G60G97GB1GB2G30GA8GA5; G27 G2

9、6G21:G28G29G2AG2BG2CG2DG2CGB3GB1GB2GB4GB5 GB6GB7GB8GA6 G34; G27 G26G21:G28G29G2AG2BG2CG2DGB9GBAGBBG8DGB1GB2GB4GB5 GB8GA6 G34; G27 G26G21:G28G29G2AG2BG2CG2DGBCG61G37G3EG3DG32G3FG40G41G42G43G30G31G32 G54G39G3AG3B G3DG32G3FG40G41G42G43G4F G3BG34。 GBDG26G21GBE G30G27 G26G21。 GBDG26G21GBFGC0 GC1G28G30GC2

10、GC3GC4GC5。 GC6GC7GC8GBDGC9GCAG30GCBGCCGCDGCEG90GCFGD0G97GD1GD2,GBDGC9GCAG30GD3GD4G47GD5GD6GD7GD8GD9GDAGDBGCCGD1GD2G30GDCGDD。 GBDGC9GCAGDEG2DGDFGE0GE1GE2G4CGE3GE4GE5G94GE6GE7G28GE8GE9G29。 GBDGC9GCAGEAGEBGECG40:G2DGDFGE0GE1GE2G4CGE3GEDGEEGEFG28GE4GE5、G2DGDFGE0GE1GE2G4CGE3GF0GF1GE4GE5、G2DGDFGE0GE1GE2G4

11、CGE3GF2GE4 犛犖 犜 GE4GE5、G2DGDFGE0GE1GE2G4CGE3GF3GF4GE4GE5。 GBDGC9GCAGF5GF6GEAGEBGE0:GEDGF7、GF8GF9GFA、GFBGFCGFD、GFEGFF、G21G5CG22、G23G24G25、G3CG26G27、G28G29、G2AG2B、G2CG2DG2E、 G2FG30G31。 犛犖 犜 G23G24G25G26G27G28G29G2AG2BG2CG2DG2EG2FG30G31G32G33G34G35G2E G36G37G38G39G2DG2EG2FG30G31G32G33G3AG39 G3BG3C GBDG

12、26G21GC2G32G32G2AG2BG2CG2DGBCG61G37G30G3EG3DG32G3FG40G41G42G43( )G30G54G39G3AG3B G3DG32G3FG40G41G42G43G4FG3BG31 G32G33G34。 GBDG26G21G34G35G36G37G2AG2BG2C、G38G39G2AG2BG2C、G39G2AG2BG2CG8EG3AG59G2AG2BG2CG2DGBCG61G37G3EG3DG32G3FG40G41G42G43G30G31G32。 G3DG3BG3EG3FG40G41G42 G24G3BG3CG3DG6EG36GBDG3CG3DG30G

13、3EG35GBEG3FGD6G90G40G30。G41GBEGC7G42G43G30G44G35G3CG3D,G45GC7G42G43G30G46GBDG34G35G36GBDG3C G3D。G41GBEGD6GC7G42G43G30G44G35G3CG3D,G47G48G49G46GBD(G4AG4BG4CG46G30G4DG4EGEC)G34G35G36GBDG3CG3D。 G21G9EGB6GB5G4FG35G6AGC2G50G4CG51GB5G33G34。( , : ) G43G44G45G46 G2AG2BG2CG52G53G54G55G54G39G3AG3BG21G48G56,G3

14、AG57G21G58G59G5AG95G96G5BG5CG36G95G96G3E,G5DG38G8FG5EG5FG60GDEG5FG61G39G2DG62G63 G38G9C,G5DG55G64G65G56GDEG63G38G66G62G3DG32G3FG40G41G4FG3BG30G48G49G67。GD6G3FG4FG67GA5G30 G68G4FG3BG2DG5AG8AG48G56G54G55G69 G6AG21G48,GDEG61G25G34G6BG27G6CGBBG6DG6EG6FG4FG70G42( )G22 、 G4C G61G59G48G49G30G71G72G29GA7,G5

15、4G55 G4C G73 G59G48G49G30G71G72G29GA7G90G6EG28 G30G42G43,G5DG74GE3G75GC9GCAG76G4F G42G77,GA8G78G28G2EG2FG30G3EG3DG32G3FG40G41 G42G43,G23 G79G7A。 G47G48G49G4AG4B G7BG7CGDAGC2G32G7D,G4CG35G51G61G7EG22G21G9EG7F,G6AG22 GC2G32G30G80G81G6A。 G82G73G45:G83G81G7F。 G84G45:G83G81G7F。 G55G36G73G45G79:G83G81G7F。

16、 G73G45G5FG54:G85 G82G73G45( ),G86G6AG87G87G88 ,G89G8A。 G84G45G5FG54:G85 G84G45( ),G86G6AG87G87G88 ,G89G8A。 G55G36G73G45G79G5FG54:G8BG85 G55G36G73G45G79( ),G86G6AG87G87G88 ,G89G8A。 G8CG38:G7FGA7 。 G8DG8EGC9GCAG8FG90G38G36G95G96G3E:G7FGA7 。 G8FG90G76G4F:G90G91G92GE3G75G93G49GCFG47GD5( )G94G47G69G95G6

17、EGE3G75GE3GEEG96G90G30G8FG90G76G4F,G97G98GB6G75G8DG8E G99GF6G91G92G47G2DG80G59G94G9AG59,G9B (G4DG4A, G43: )G8EG9CGC9G32G36G95G96G3E ( ),G9DG35G36G95G96G3E( )G9CGC9G32G8DG8EG8FG90G76GBCG61G37( )。 G8DG8EG8FG90G76:GBCG61G37,G7FGA7 ,G47 G43G5DG8FG90G76G4FG9EGCA。 GC9GCAG8DG8EG54G30G9FGA0:G85G8DG8EG8FG90G

18、76GBCG61G37( ) ,G35G6AG87G87G88 ,G9FGA0G5CG82GA7G22 ( )GBCG61G37G8DG8EG54。 犛犖 犜 G4CG4DG49G4EG4F G2DG2EG2FG30G31G32G33G3AG39G4C( 犐犚犕犛 ) G35G36G31G67G3DG32G3FG40G41G42G43,G9FGA1G61G25G34G6BG27G6CG6DGA2GA3,G3FGB7G31G67 、 G4C G30 G48G49G29GA7。G3EG9FGA1G80G25GA4GA5GA6GA7G94GA8G35G9AG9BG9CGA6GA7,G68G2DGA9

19、G52G53G32G67GAAGABG94G2DG62G4FG3BG31G67GACGADGAEG47G69 GAFG76G2DG21G48G28G36G95G96G3E。 G36G37G38G39G4C G54G39G3AG3BG9F( )G54G55GBBG29G74G3DG32G3FG40G41G42G43G4FG3BG9FG9AGBB,GBBG29GDEG95G96GB0G3EGA3G4CG5EG5FG60G57G5C,G54G39 G3AG3BG9FGB1G32G3AG3BGB2G56GCFG68GD6GA8G35G46G47G5FG61G94GB3G86G61G30GB4GB5G2

20、4GB6G52G53G2DG30GBCG61G37G4CG47GB7G76G4FG2DGA9G46G5E G21G48。 G47G50G34G51G4FG52G53G54 G55G56G57G58G34G50G59G51G4F G6EG36G4AGA7G77GB8G30G2AG2BG2CG52G53G9BG64G2AG2BG2C、GB9G64G2AG2BG2C,GA8G35G6AG6EG2AG2BG2CG52G53G87G87 GBA,G55 GBBGBCG92G47GBDG60,GA1G31。G68 G24GBEGBFG24GC0。GA0G52GC1G8EG55GC2G2DG3EGC3GC4

21、G52G53GC5G6FGC6GC7G94GD3GC8G5AG31G76G72G67G30 GC9G96。 G55G56G57G5AG34G50G59G51G4F G6EG36G4AGA7G77G5DG30G2AG2BG2CG52G53G9BGB9GCAG2AG2BG2C、GCAG2AG2BG2C,GA8G35G6AG6EG2AG2BG2CG52G53G87G87 GBA,G55 GBBGBCG92G47GBDG60,GA1G31。G68 G24GBEGBFG24GC0。GA0G52GC1G8EG55GC2G2DG3EGC3GC4G52G53GC5G6FGC6GC7G94GD3GC8G5AG3

22、1G76G72G67G30 GC9G96。 G35G2EG5BG5C G35G2EG5DG42 G36G37G38G39G5EG5FG5DG42 G3AG3BGB2:G8FGCBGCCGCDG30G63G3CGCE G36G3CGCEG52G63GCFG8DG76G3AG3BGB2GD0G63GD1G48G49( )GB2, ( ), G94G8EG5EG30GB2G49。 G9CG9DG39: G73G45G5FG54( )。 G9CGD2: 。 G2DG52G67: 。 GB2GD3: 。 G60G61G62G63G4DG5EG5FG5DG42: G9CG9DG39: G84G45G5FG

23、54( ); G55G36G73G45G79G5FG54( )。 G9CGD2: 。 G47GB7G95G96GB0G3EGA3G8FG90GD4G3DG8FGD5GD6GD7 。 犛犖 犜 G2FG30G31G3AG39G5EG5FG5DG42: G48G49G67:G8AG49GD8GD9G48G49G67( G67)。 G47GB7G4FG3BG8FG90GD4G3DG8FGD5GD6GD7 。 G50G59G35G2E GDAG85GBCG61G37GC9GCAG8DG8EG54( ) G36G2DG52GDBG2D,GBEGBFGA1G35,G8EG22GC9GCAG52G53。GD

24、CG96G3DG32G3FG40G41G4FG3B G9F、G54G39G3AG3BG30G8DG8EGDDGDE、G38GBEG91、G48G49G4FGDFG78GA7G8EGA4GC9G7EGE0G8DG4FG3BGE1GA9GF6GE2。GD2G35G8FG90G38G2DGA9G4FG3BG3D G32G91GB4G31, G57G8FG90G38GC9GCAGE3GE4( )G3EG26G36 。GDCG96GA5G98GE5GA2GA6GA7GE6GB1GE7GDC,G3FGF6GB7G2DGA9G39G3EGE8 GE9。GBFGC0 G2DGD4G3DG31G32G52GBD

25、,G4FG3BGEAGEBG8FGD5GD6GD7GEB 。 G3AG64G65G51 G52G53GB4G31GADG2DGA9 G59GC9GCAG52G53G31G32, G59G21G9EG30G3EG3DG32G3FG40G41G42G43G74GC9GCAGDFGB6G43GECG6EGE3GE4G3EG26G36 ,GEDGC3G3EGB4GEEG9FGA3GE8GE8GE9G21G9EG8FGA5。G3FG80G52G53GEFGF0G31G32 G59,GC9GCAGE3GE4( )G3EG26G36 ,GED GC3G3EGEFG49G31G32。G52G53GF1G3BG

26、2DG97G98G52G53G67GE6GB1G39G3EG30G4FGF2GC9GCA。 G66G67G68G69G49G6AG6B G52G53G2DG2EG2FG30G3EG3DG32G3FG40G41G42G43G54G55G42G77GF3G31G52G53G74G5D G9EGE7G30G8DG8EGC9GCAGACGAAG30GE4GF4,G35 G43G79G7A。G68G21G9EG2D,G44G62G30G36G95G96G3EG8FG90G38G8F,GF5GF6G35G96G90G30 G9EGCAG30GE3G75GC9GCAG2DGA9G9EGCA。 G43G74G

27、8DG8EG8FG90G38G8FG30GE5GA6G79GF7GD5GF8( ): 犆狊犪犿 狆犾犲 狉犲 犳 ( ) 犚狊犪犿狆犾犲 犚狉犲 犳 () ( ) 犚狊犪犿狆犾犲 G4C 犚狉犲 犳 G21GDAG22G52G53G4CG8FG90G38G8FG36G95G96G3E( )G30 G43。 G43G4C G30GE5GA6G79GF7GD5GF8( ): 犆狊犪犿 狆犾犲 犞 犘犇犅 犆狊犪犿 狆犾犲 狉犲 犳 犆狊犪犿 狆犾犲 犞 犘犇犅 犆狊犪犿狆犾犲狉犲犳 犆狉犲犳犞犘犇犅 ( ) GBEGF9GF6G31G32G30G8DG8EGC9GCAG74 G30GE3GE4 G

28、DEG36G9FGA3GFAGFBG30G4EGC9,G31G32GB7G90GCFGD3GC8G77G26G30GC9G96。G68GDBG59GB4GB5G24,G52G53G3EG97G98G8DG8EGC9GCAG4CGB6G75G43 GFCG23G9EGE7,GFDG32GFEG25G8FG90G52G31G67GACGAAG30GC9G96G22GFFG91,G2DG21G6EG22G4BG9EGE7。G8FG90G52G3EG68G52G53GF1G3BG23G24GACGADG4C GACG56G2DGA9G31G32,G90GD2G35GFFG91G25G43G6EG22G

29、4BG2DGA9G9EGE7。G26G27G30G52G53G21G9EGF1G3BGE6GB1G8FGD5GD6GD7 。 犛犖 犜 G6C G6D 犃 (G6EG4BG3EG6CG6D) G4CG4DG6FG70G5DG42 G8FG90G95G96GB0G3EGA3GD4G3DG9BG24: ) G8CG38G63G38G28G29: 。 ) G74G4FG3BG30GBBG29GCDG2AG2BG38G28G29: 。 ) G36G95G96G3EGC9GCAG38G28G29: 。 ) G95G96GB0G3EGA3GD3GA7: 。 G8FG90G4FG3BGD4G3DG9BG24

30、 ) G48G49G67G8AG28: 。 ) GDFG78GA7: 。 ) G2CG2DG38G28G29: 。 G2EG2FG30G91G31G32:GD6GD7G4CG3BG8FG90G9FGA3G8DG8EGD4G3DGBEG68 G27G3DG32G3FG40G41G42G33G4FG3BG9FGF2G34G5CG30,G35G36G3BG28 G51GB5G35G9FGA3G27G72G45G22GE7G37G8FG90,GE8GD6GD0G97G2FG30G38G30,G39G3AGC9GCAGA8G35G3BG3CG51GD6G3FG3DGEEG94G27G72G30G9FGA

31、3。 犛犖 犜 G6C G6D 犅 (G6EG4BG3EG6CG6D) G3AG39G71G72 G72 犅 G50G59G34 犔犆犐犚犕犛 G3AG39G71G72 犛犖 犜 G6C G6D 犆 (G6EG4BG3EG6CG6D) G50G59G35G2EG73G74G4EG2EG75G76 GF2GA0G52G53 GF2GA0G52G53 GF2GA0G52G53 G52G53 G52G53 G52G53 G52G53 G52G53 G52G53 G3EG25G52G53G31G32 G59。 G52G53 G52G53 G52G53 GF2GA0G52G53 GF2GA0G52G53 GF2GA0G52G53G90G23GBEGE3G75GC9GCAG76G4F,G3FG90G23GBEG40GDCG31G67G55 G43(G41G9B,G35G89G41G21G9EG9F G3DG32G3FG40G41G42 G43G4FG3BG9FG31G32)G30GBCG61G37G5FG54,G90G6EG31G67GF1G3BG2DG90GCFG30G42GDAG2DGA9GB4GEEG4CG22G4BG4DGE7。 犛犖 犜

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