1、b )P ICS 67.080.20 X26 konjac gel food DB 0843/354-2007 2007-09-1 0 111 2007-1 0-1 0 :ijffi 0843/ 354-2007 -mi1f n 1 111 2 .mmtt51JtJJt14= 3 Ji:.:X. .!:j * . . 4 t cB 216o fz!Jill: OO“it;Hfl ootz!Jill: GB!f 4789.5-2003 3j(:)t819!tl5E:Jr#.i: GB!f 5009.11-2003 9=I,1i$7CtJL1i$8JE GB!f 5009.12-2003 9=I
2、,ff-B“JlftW5E GB!f 5009.34-2003 9=IIYJint1i819!5E1J#.i: GB!f 5009.35-2003 9=IirnltBJfiJ85E1J#.i: GB 5749 ffit.Jffl;j(JIfl GB 6543 K:m*i GB 7718 J:V!;jiffi-JJJtru!fz!Jill:;f:i! GB!f 10786 -2005 ffii 8fz!Jill:1J#.i: rr141-19 m*ffii# GB 14881 :; oo*m:ttz,fiD c 2oo5) 75%4-5Eii-E1;gw1J,M: 0843/ 354-2007
3、3.1 .)( rJO*if!lJE5Cifflr*tllo il:1Rtt Jb:fH tV.1.k, il:il:7J -=t l*t-t, 3R -t;:IJU7.k 1ffJ!E:, :IJumWHt, m:IJu fiJfmttJbm:IJuifiJ, IRJJ=ftill#tJi!lmi!JiJffltJb!lmlitI*JIDs11LE1tt:IJuiffiiJmsIRi!JiJJbo 3.2 tlHiill :!tx-t 8 11iE 1tt :;f J:lJ , “ilJ ?t :7J il:ill :!E. !IT. , il:ill :!E. !1m tt Jb o 3.
4、2.1 il:ill:!t!SItV.7.k, il:il:7J-=tl*t-t, milljt!SI!Sllf3tf11IE:1Jurmsj!JR 111u Jb o 33 W!_t raril: . 0 3.2.2 il:ill:!t!JmttJblV.7.k, il:il:7J-=EI*t-t, till#!JmlitI*JJllIDtf, 51f, J!fr1!.11iEtt:IJuiffltsIR1!JuJb o oto 4 * 4.1 :*ffl*4* 4.1.1 7.)( 5Jf.lI1“-1=il GB5749 BJEo 4.1.2 il:J.lI-=f7CtJ/, X12J!
5、fr:Jmo 4.1.3 il:f;tf.lI1-1=i! NYff494 BJEo 4.1.4 :t1-ttJ.lI1-1=iJffl* C B:Jto 4.2 e* 1t-T-m1“-1=il* I sJEo ttg,;R JYl 13 l!ll.51!/J,) e t A-m-eseSeo %7t if-3:$ m. x. tltimo iri Jl;j(;fiE(JI;j( Al!ll.8-4:JI5l(5filif1JI5l(, X1MY, :JGJFJI;j(o :ffgffi;, 7JC;jjjffi;:;f,-fif GB6543 8* _iftM1Eo 7.2 tf-i.R!
6、:Jtf- 7.2.1 J:Jf,iRLllrif GB191 lJEo 7 .2.2 ;j:Jf,mrif GB7718 lJE, :;J:Jf,tt JiHJl.FYL 4 0843/354-2007 7.2.3 fltf$f!lilt 1:.f“itPJ iiltllB% o 7.3 m :iEImmi, 1:., :JC5, mlflllf 8 Bli, FIIT#t19:1if!L F:ft$:ft 5!Jo/Jto 7.4 iif 1Jf-mf!JjfJ?:, T:i*, mM, 1:., lflllJffR, lllitl19:tiffio /F1xtf“lf5B“J!Jo/J-
7、1, i:!1:-f1 a 7Cr 0 7.5 f*:M tm-EIiltf*M 121-Ji o 5 0843/354-2007 llftA -*$*:1f;fl tH 1.0mg/kgo A.2 fflHJ ff:?kML t7t)Jo.AJlJlW:fF.:Jg I*J;t. ttiiiY!l7tm:pz:-J:tBMiFiim815“ ito IV. KGM :51-ritBM-7:;:jcttfDi=tBM*tiit-i=tBM ( KGM) *it . . IV. -15“it-*itBM ( KGM) ilM* b) imnx1Sl; c) Jli.-T#t; d) 1-Ef3W
8、/E. tL-Z:.f, 7C7J(.lji;fffiiff.ffim 1.0 ml, JJOAJIJlW:I*Jti 1.0 ml, ntE 70 OCJt8-imD)t c) ;fYft!(FID)250 c; ttt.ffii 160 c(%1# 10 min), IV. 20 c/min J!-$7tt.ffii 200 .C(,BH# 5 min), :P !), 30 c/min J!-$7ttlffi. 230 ccf%1# 5 min); d) ft!i Nzft“=.; e) tt?Jitii 1.20ml/min; f) )j-?Jitr:l:J 1:59o A.4.4 i
9、:$HJT !liz. 1 ml ;f;f,f-FlJ!nJif1rr1:. !mIliz.f;f-1!5E:i:o tr:mll, iFlli2ZPJ;f;f!lmlJ!nJif1rr1:.!lm4.;f5*0000 A 1 o A.5 tt llf:tf=it.rblZ:Fq=riJi=fll ( KGM) 5fOti:fJt(Starch)tjjiJfS-Jiit:tmr: KGM (%) = (n+l)xManxlOOx0.9x10-3 xlOO (A. 1) m(l-a) Starch(%)= (Glu- n) x Manx lOOx 0.9x 10-3 x lOO . (A. 2)
10、 m(l-a) :r.;9=: KGM-it.fb 9=riJitfm1ti-Ji(IV, Tit), i(!ft:l:Js Jt; Starch-ti:17i-Ji(IV. -Tit), i(!ft:l:Js ?t; Glu-5iYft!5EiJl!ijlJ!sm, 1f!1ft7:!; Man-5iYft!,J5Eit:mtsm. l(!ft:l:J; 10o-?(mta5E-f*. i(!ft:l:JJt; n-KGM ?t-=f9=rit:mtl5fOiJl!ijlJ!BJfl$ tffi(:I!O:ft=*;f;f,=#, !J!UiJittl itIliz.it:mtl5fOiJl
11、!ijfm8: :tlo;f;f,s=. !J!Ulliz.it:m lJ!5fOijl!ijlJ!Jfl$ tffi 1.69, f!P n 7:1 0.592); o.9-:FtJittti:Jt:xt?t-=t-mt:m5J1f!tst:xt?t-=t-mt:mzt; m-;f.Fi, i(!ft:l:Jo a -WJ-T!lm1ti?(ft, i(!il:l:Js ?to A.6 ffibt ttt#r1E*:xtffiSrl#ffi1o 7 0843/354-2007 lltl8 *$=tt*;oo ( *Ji;!mtillf1 ) 8.1 m:11 *mm=-Oo *:ff:;:1
12、;f.:tfi Jg 0.0144g/kgo 8.2 m1iM-M-M1WHtm. =5J=tif-*f:l31;1G:tJJX:m51-tif!W. ;l:tW!5 5J=1k.BtJJX:lfr:ft:*, :f:ffi5j;fE?ft 388nm 9.H:i:o 8.3 -)( .!:.iil-ftr 8.3.1 :)ttJT:JCf-(fifij_Jj 0.0001 g)o 8.3.2 )l:)t:JftJ!tBtit(fiH3fM“:;1Jff)o 8.3.3 ntmo 8.4 ii:jfiJ.1G?(f$11G, ffl lmol!L 1iMffi:fHtffU lOOml, Mi
13、 1:1*5-Jt;:ffiJ#a, 1i!07(1*11kffl)o 8.4.3 TiOz:fi1E#M-11kffi?fi(f$1f$ 500ml :fiHELJf:tiJBt, lZ:,:J;ffi“jfffitjf1!kfflo iffileyJtij; lmg TiOz)o 8.4.4 TiOzti1E1tffltfi(i1EfifB;f$J lOOug TiOz)o 8.5 HJTi!7 8.5.1 FII ( li-litt-fJ!MU:R) .f:f$?m-T:7G8fll!E?fif:$:HEtl:l. A.:JTtmW, ? o fil1:1f8fll!E885/Gffi!
14、W .!J!IJ:bo M Ig mm1-tm8fl. Ni=ft!PJ;f$ 25o 7t:i!:#aJtmtm7tt1Jli. :t.mlt If$ TiOz:i:PJftBffU ), 11fflmtm7j(t1Jli. :f.ft ); fl= iro ?fi 0 8.5.2 * ;W!u 8.5.2.1 tr-Jt !HxiliU :)tjjlj;f$:1fEftffl?fi 0.00, 0.20, 0.40, 0.60, 0.80, l.OOml 25ml t-,tg (if TiOzlO.OO, 20.00, 40.00, 60.00, 80.00, lOO.OOug ), :b
15、OA 5%Vc-ID!J(ffi 2ml, :f,Fg11:1Jo 25g/L =tHif*ffi;I:JG m?fl5ml. fflmf3l7tygliJlJi30mino :tf388nm!xt, m lOmm t51ill, :filsftt. i9W :JftBt #Jij;fEfltlo 8.5.2.2 ;j$iY)Ij I c-iJti!ilJ;Et m-EIJ:. if!m; v-mJ;Ef$:. mfh vz-!;7T; v3-mff1a s“JJ;Effi:. if!f.V:J;:rr; V-11!ilf$:f,R, if!.LJ;3T a 8.6 it.Jl t!11k4rgjt18w;JX!R:ll.i!ilE5f!:BfXtta:IG11m:i1Jlt:;t(fBJta8“J 10%a 9 DB43/ 354-2007 Jfff *:fil:VJ Ca(OH),it,% !#( ( Fit) , mg/kg l!i :i: .1m ( V) P b it ) , mg/kg f:( Pbit ), mg/kg I!#C *ffl();* ( 511til!# ) I ll;fil:i:Jm( VJ Mgit ),% 10 t tr-95 -100.5 0.5 3 !l)j!i 150 30 10 4.8
