1、Designation: D3603 14Standard Test Method forRust-Preventing Characteristics of Steam Turbine Oil in thePresence of Water (Horizontal Disk Method)1This standard is issued under the fixed designation D3603; the number immediately following the designation indicates the year oforiginal adoption or, in
2、 the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope*1.1 This test method covers the ability of steam-turbine oilsto prevent the rusting of
3、 horizontal and vertical ferrous surfaceswhen water becomes mixed with the oil.1.2 The values stated in SI units are to be regarded asstandard. The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its
4、 use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2A108 Specification for Steel Bar, Carbon and Alloy, Cold-FinishedA240/A2
5、40M Specification for Chromium and Chromium-Nickel Stainless Steel Plate, Sheet, and Strip for PressureVessels and for General ApplicationsD91 Test Method for Precipitation Number of LubricatingOilsD665 Test Method for Rust-Preventing Characteristics ofInhibited Mineral Oil in the Presence of WaterD
6、1193 Specification for Reagent WaterE1 Specification for ASTM Liquid-in-Glass ThermometersE2251 Specification for Liquid-in-Glass ASTM Thermom-eters with Low-Hazard Precision Liquids2.2 Other Standards:IP 60/80 Specification for Petroleum Spirit3SAE 30304 Steel, Corrosion-Resistant, Sheet, Strip, an
7、dPlate, 19Cr - 9.2Ni4BS 970:Part 1:1983 Specification for wrought steels formechanical and allied engineering purposes. General in-spection and testing procedures and specific requirementsfor carbon, carbon manganese, alloy and stainless steels5BS 871:1981 Specification for abrasive papers and cloth
8、s3. Summary of Test Method3.1 The test method involves completely immersing a hori-zontal steel disk and vertical steel cylinder in a stirred mixtureof 275 mL of the oil under test and 25 mL of distilled water(water conforming to Specification D1193, Type II) at atemperature at 60 C (140 F).3.2 The
9、horizontal specimen allows water to puddle on thesurface, and the vertical specimen is continually washed withthe oil-water mixture during the test.3.3 The test is run for 6 h and the specimens are evaluated.4. Significance and Use4.1 Horizontal metal surfaces, on which water droplets tendto be reta
10、ined, are more prone to rusting and corrosion thanvertical or sloping surfaces. This test method is therefore morediscriminating than Test Method D665 (Procedure A), since itgives a separate evaluation of the oil on a horizontal and avertical surface. The test method indicates the ability of oils to
11、prevent rusting and corrosion of all ferrous surfaces in steamturbines under full flow and quasi-static conditions. It is usedfor specification of new oils.5. Apparatus5.1 Oil BathA thermostatically controlled liquid bathcapable of maintaining a temperature in the oil sample of 60 C6 1 C (140 F 6 2
12、F). The bath shall have a cover with holesto accommodate the test beakers.NOTE 1The bath used for Test Method D665 may be used with slightmodification, that is, the centers of the beaker holes are moved from1This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products, Liqui
13、d Fuels, and Lubricantsand is the direct responsibility ofD02.C0.02 on Corrosion and Water/Air Separability.Current edition approved Dec. 1, 2014. Published February 2015. Originallyapproved in 1977. Last previous edition approved in 2007 as D3603 07. DOI:10.1520/D3603-14.2For referenced ASTM standa
14、rds, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Available from Energy Institute, 61 New Cavendish St., London, WIG 7AR,U.K., http:/www.
15、energyinst.org.uk.4Available from SAE World Headquarters, 400 Commonwealth Drive,Warrendale, PA 15096-0001.5BSI, British Standards, 389 Chiswick High Road, London W4 4AL, UnitedKingdom.*A Summary of Changes section appears at the end of this standardCopyright ASTM International, 100 Barr Harbor Driv
16、e, PO Box C700, West Conshohocken, PA 19428-2959. United States16.4 mm to 18.3 mm (14 in. to2332 in.) from the axes of the stirrers.NOTE 2To indicate the temperature, a thermometer conforming to therequirements of ASTM Thermometer 9C or 9F, or IP Thermometer 21C,as prescribed in Specification E1 sho
17、uld be used. Thermometric devicessuch as RTDs, themistors, thermocouples, or a thermometer conforming toSpecification E2251 may be used.NOTE 3Thermometer S130C (S130F) in Specification E2251 may besuitable. Temperature range: 7 C to 105 C and scale error, max.: 0.5 Cas compared to Thermometer 9C wit
18、h a temperature range of 5 C to110 C and a scale error, max of 0.5 C.5.2 BeakerA 400 mL, Berzelius-type, tall-form heat-resistant glass (see Note 4) beaker without pourout, as shownin Fig. 1, approximately 127 mm (5 in.) in height measuredfrom the inside bottom center and approximately 70 mm(234 in.
19、) in inside diameter measured at the middle.NOTE 4Borosilicate glass is satisfactory for this purpose.5.3 Beaker Cover and Specimen HolderA flat beakercover (Fig. 2) of methyl methacrylate resin or other fluidresistant material is kept in position by a suitable groove. Threeholes are provided. Two a
20、re located on any diameter of thecover, one for a stirrer, and the other for attachment of a diskspecimen to the underside of the cover for optional vapor phasetesting. The third hole is for a thermometer, located on adiameter perpendicular to that of the other two holes. Theoutside of the polytetra
21、fluoroethylene (PTFE) specimen holder(Fig. 3) is a square, but from the ends of one diagonal, twoequal pieces of PTFE are cut off over the height of the holder.Two vertical threaded holes are made on the other diagonal ofthe square. The inside of the holder consists of two cylindricalholes, one on t
22、op of the other. Four horizontal holes are drilled90 apart on the circumference where the two cylindrical holesmeet. The PTFE specimen holder is connected to the beakercover by two stainless steel holding rods (Fig. 4). Both ends ofeach holding rod are threaded. The surfaces between thethreads are p
23、olished with No. P180 (180) grit emery. The12.7 mm threaded ends of the holding rods are screwed into thetwo vertical threaded holes of the specimen holder. The19.0 mm threaded ends of the holding rods are connected to thebeaker cover by putting them through two holes on a lineperpendicular to the c
24、onnection line of the centers of the earlierNOTE 1All dimensions are in millimetres (inches).NOTE 2Unless otherwise specified, tolerances will be 60.5 60.02.NOTE 3No direct equivalent available for 10-32 SS nut in metricsystem.FIG. 1 Rusting Test ApparatusNOTE 1All dimensions are in millimetres (inc
25、hes).NOTE 2Unless otherwise specified, tolerances will be 60.5 60.02.NOTE 3No direct equivalent available for #9 drill in metric system.FIG. 2 Beaker CoverNOTE 1All dimensions are in millimetres (inches).NOTE 2Unless otherwise specified, tolerances will be 60.1360.005 and 61.NOTE 3No direct equivale
26、nt available for #21 drill rust-preventing characteristics;steam-turbine oilsSUMMARY OF CHANGESSubcommittee D02.C0 has identified the location of selected changes to this standard since the last issue(D3603 07) that may impact the use of this standard. (Approved Dec. 1, 2014.)(1) All figures revised
27、 to update SI units. (2) SI units formatting changes made throughout.ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of an
28、y such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are i
29、nvited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not receiv
30、ed a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of
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