1、Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-CHANGE NOTICES ARE NOT CUMULATIVE AND SHALL BE RETAINED UNTIL SUCH TIME AS THE STANDARD IS REVISED. FED. TEST METHOD STD. NO.63BAIGEN May 9,1976 CHANGE NOTICE 1 March 29.1994 FEDERAL TEST METHOD STANDAR
2、D SOAP AND SOAP-PRODUCTS (INCLUDING SYNTHETIC DETERGENTS), SAMPLING AND TESTING The following changes, which form a part of FED. TEST METHOD STD. 536AIGEN, dated May 9, 1975, are approved by the Commissioner, Federal Supply Service, General Services Administration. to be used by all federal agencies
3、. REMOVE: Standard Test Method 6701 of May 9, 1975 ADD: REVISED Standard Test Method 6701.1 of March 29. 1994. ADD: PAGE 6a AFTER PAGE 6 OF FED. TEST METHOD STD. NO. 536AIGEN. RETAIN THIS CHANGE NOTICE AND INSERT BEFORE THE INFORMATION SHEET ON FEDERAL STANDARDS. Orders for this publication may be p
4、laced with GSA Specification Section (BFBP-W), Suite 8100, 470 LEnfant Plaza. S.W., Washington, DC 20407. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-_ FED-STD-53bA 77 7747477 0004347 3 W INFOiUW“ON SHEET ON FEDERAL STANDARDS Thiu Federal Standar
5、d is ieeued in loose leaf form to permit: the insertion or removal of new or revised sections and methods. All uuerc) of Federal Standard8 should keep them up to date by inserting revise8 or new sections and methods as iseued and removing superseded and canceled pages. Naw and revised material and c
6、ancellatione will be issued under Change Noticee which will be numbered coneecutively and will bear the date of iesuanca. Change Noticea ehould be retained and filed in front; of the Numerical Index of the Standard until such time a6 they are superseded by a reiesuance of the entire Standard. Provid
7、ed by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED-STD-53bA 77 W 7979777 O004400 b 9 FED. TEST METHOD STD. NO, 536A/GEN FEDERAL TEST METHOD STANDARD SOAP AND SOAP-PRODUCTS (INCLUDING SYNTHETIC DETERGENTS): SAMPLING AND TESTING This standard was approved b
8、y the Commissionerr Federal Supply Service, General Services Administration, for the use of all Federal agencies. 1. SCOPE AND NUMBERING SYSTEM 1.1 SCO e, This standard covers methods of sampling and testing which shall be used offdly in the sampling and routine testing of soaps and soap products in
9、cluding those containing synthetic detergents, purchased under Federal specifications. The Government reserves the right to use any additional information to determine whether the material ordered meets the requirements of the applicable purchase specification. 1.2 Numbering system. The Federal Test
10、 Methods herein are identified by numbers consistingfederal Test Method Standard number, a slant mark (/I, and a whole nwnber, e.g., FED. STD. TEST METHOD 536/101. Revision numbers, if any, are placed after a decimal point, e.g., the second revision is FED. STD. TEST METHOD 536/101.2. this standard
11、have been superseded by ASTM test methods. Test Methods are crpss referenced alphabetically and numerically to applicable sections of the superseding ASTM standards. Active Federal Test Methods are so designed and are printed herein. The superseding ASTM test methods are listed separately in numeric
12、 sequence with their titles. 1.3 Supersession. Most of the Federal Test Methods listed in the prior issue of These superseded Federal One Federal Test Method is canceled without supersession. 2. APPLICABLE DOCUMENTS 2.1 The following documents, of the issues in effect on date of invitation for bids
13、or request for proposal, form a part of this standard to the extent specified herein. Federal Specification: RR-S-366 - Sieve, Test. (Activities outside the Federal Government may obtain copies of Federal Specifica- tions and Standards as outlined under General Information in the Index of Federal Sp
14、ecifications and Standards and at the prices indicated in the Index. The Index, which includes cumulative supplements as issued, is for sale on a subscription basis by the Superintendent of Documents, U.S. Government Printing Office, Washington, DC . 20402. (Single copies of this standard and of Fed
15、eral Specifications required by activi- ties outside the Federal Government for bidding purposes are available without charge from Business Service Centers at the General Services Administration Regional Offices in Boston, New York, Atlanta, Chicago, Kansas City, MO, Ft, Worth, Denver, San Francisco
16、, Los Angeles, Seattle, WA, or from Specification Sales, GSA, Bldg. 1971 Washington Navy Yard, Washington, D.C. 20407. Additional copies may be purchased from the Specification Sales Office, Washington, D.C. 20407. standards from established distribution points in their agencies.) (Federal Governmen
17、t activities may obtain copies of Federal Specifications and Laws and Regulations: 26 CFR 212 - Formulas for Denatured Alcohol and Rum. (The Code of Federal Regulations (CFR) and the Federal Register (FR) are for sale on a subscription basis by the Superintendent of Documents, U.S. Government Printi
18、ng Office, Washington, DC 20402. When indicated, reprints of certain regulations may be obtained from the Federal agency responsible for issuance thereof,) Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,- FED-sTD-A 77 qqqq777 oooqqol %D. TEST METHOD
19、STD. NO. 536A/GEN 2.2 Other publicahione. The following documents form CI part of this standard to the extent specified herein. Unless a apeciZic issue is identified, the i68Ue in effect on date of invitation for bids or request for proposal shall apply. American Society for TeBting and Materials (A
20、STM) Standards: ASTM D - Standard Methods for Sampling and Chemical Anaylsia of Soape and Soap ACTM D - Standard Methods of Chemical Analysis of Soaps Containig Synthetic (Application for copies should be addressed to the American Society or Teeting ProdUCt6, Detergents. and Hatarialr, 1916 Race Str
21、eet, Philadelphia, PA 19103.) 3. GENERAL NOTE6 3.1 Neutral ethyl alcohol (95 percent). Where this reagent is specified, it i6 prmf#ible to U88 either formula 3A or 30, denatured ethyl alcohol, 95 percent, neutral to phenolphthalein, described in subpart D of 26 CFR 212. Provided by IHSNot for Resale
22、No reproduction or networking permitted without license from IHS-,-,-I FED-STD-53bA 77 W 7977777 0004402 T = FED. TEST METHOD STD. NO. 536A/GEN NUMERICAL LIST OF TEST METHODS STATUS : ACTIVE, CANCELED OR SUPERSEDED BY: Title of Method Fed. Std. Test Method No. ASTM Method No. SOAPS AND SOAP PRODUCTS
23、: S amp 1 ing Moisture and Volatile Matter (oven method) Moisture (distillation method) Alcohol-insoluble matter Free Alkali or free acid Matter insoluble in water Alkaline salts Free alkali and potassium carbonate in soaps Total anhydrous soap and combined alkali Chlorides Unsaponified plus pnsapon
24、ifiable matter Unsaponifiable matter Unsaponified saponifiable matter Rosin Preparation of total fatty matter Titer test Acid Number of fatty acids Iodine number (Wijs method) of fatty acids Borax Silica present as alkaline silicates Carbonates (Gravimetric Method) Carbonates (Volumetric Method) Tot
25、al Phosphates Tetrasodium pyrophosphate Sulfates Sugars (Qualitative) . Glycerol in the absence of sugars Glycerol in the presence of sugars Starch Sugars Volatile Hydrocarbons Cfxined srdium and potassium oxides 101.2 201.1 202.2 301.3 302.3 303.1 304.3 305.2 401.3 501 601.2 602.1 603.1 701.3 801.1
26、 901 1001.1 1101.2 1201.1 1301 1401.2 1402.1 1501.1 1502.1 1601.1 1701 1702 1703.1 1704 1705.1 1801 1901 ACTIVE D460 1111 D460 112-15 D460 116-17 D460 118 D460 $19 D460 Y20 D460 827 D460 121-22 D460 150-52 D460 1130-32 0460 1133-35 D460 #36 D460 1137-40 D460 1/41-42 D460 443-44 D460 Y45 D460 #47-49
27、D460 153-55 D460 $56-57 D460 X61 D460 #62-65 D820 #21-28 D460 174-76 D460 177-78 ACTIVE D460 179-81 D460 %82-83 D460 184-85 D460 t86-87 D460 #88-92 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. NO. 536A/GEN NUMERICAL LIST OF T
28、EST METHODS (Cont.) STATUS : OR SUPERSEDED BY: ACTIVE, CANCELED Title of Method Fed. Std. Test Method No. ASTM Method No. SOAPS AND SOAP PRODUCTS (CONT. ) : Sudsing test 2001.2 ACTIVE Sieve tests 2101 ACTIVE SOAPS AND SOAP PRODUCTS CONTAINING SYNTHETIC DETERGENTS: Sampling 5101.1 ACTIVE Qualitative
29、test for synthetic detergent 5103 Moisture and Volatile matter (oven method) 5201 Free alkali or free acid 5301.2 Anhydrous, salt-free, soda soap Alcohol-soluble matter 5601.1 5701.1 CANCELED 0460 tll DE20 117-8 DE20 #9-12 DE20 #13-14 Matter insoluble in water 5801 D820 #15 Alkaline salts Silica pre
30、sent as alkaline silicates Fatty matter Chlorides in alcohol-soluble matter Rosin Starch Synthetic detergent Neutral inorganic salts (calculation) Cleaning efficiency test 5901.1 6001 6101.1 6201.1 6301.2 6401 6501 6601 6701 DE20 #17 DE20 #18-20 D820 #35-38 D820 #39-41 DE20 142-45 D460 X84-85 DE20 #
31、46 D20 #47 ACTIVE Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED-STD-53bA CHG NOTICE 1 9999977 O033058 T52 FED. TEST METHOD STD. NO. 536A/GEN CHANGE NOTICE 1, NUMERICAL LIST OF TEST METHODS (Cont.) STATUS: ACTIVE, CANCELED OR SUPERSEDED BY: Fed.
32、 Std Test Title of mod Method No. ASTM Method NQ, SOAPS AND SOAP PRODUCTS (CONT.): Sudsing test 2001.2 ACTIVE Sieve tests 2101 ACTIVE SOAPS AND SOAP PRODUCTS CONTAINING SYNTHETIC DETERGENTS: Sampling 5101.1 ACTIVE Qualitative test for synthetic detergent 5103 CANCELED Moisture and Volatile matter (o
33、ven method) 5201 D460 #i 1 Free alkali or free acid 5301.2 0820 #7-8 5601.1 O820 -12 Anhydrous, salt-free, soda soap Alcohol-soluble matter 5701.1 O820 #13-14 Matter insoluble in water 5801 D820 #15 Alkaline salts 5901.1 D820 #i 7 Silica present as alkaline silicates 6001 D820 #i 8-20 Fatty matter C
34、hlorides in alcoholsoluble matter Rosin Starch Synthetic detergent Neutral Inorganic Salts Cleaning efficiency test Supersedes page 6 of May 9, 1976 6101.1 6201.1 6301.2 6401 6501 6601 6701.1 D820 #35-38 D820 #39-41 D820 M2-45 0460 M-85 0820 #46 D820 #47 ACTIVE Provided by IHSNot for ResaleNo reprod
35、uction or networking permitted without license from IHS-,-,-I FED-STD-53bA 77 m 7777777 OOOLI404 3 m FED. TEST METHOD STD. NO. 536A/GEN ALPHABETICAL LIST OF TEST METHODS STATUS : ACTIVE, CANCELED OR SUPERSEDED BY: Title of Method Fed. Std. Test Method No. ASTM Method No. Acid , Free Acid Number of f
36、atty acids Alcohol-insoluble matter Alcohol-soluble matter Alkali, free Alkali, combined Alkaline salts Anhydrous soap Borax Carbonates (gravimetric method) Carbonates (volumetric method) Chlorides Chlorides in alcohol-soluble matter Cleaning efficiency test Combined sodium and potassium oxides Dete
37、rgent, synthetic Fatty matter (determination of) Fatty matter (fatty and rosin acids), Free alkali or free acid preparation of Glycerol (in the absence of sugars) Glycerol (in the presence of sugars) Hydrocarbons, volatile Y Inorganic salts, neutral x Insoluble matter in alcohol Insoluble matter in
38、water Iodine number of fatty acids Moisture and volatile matter (oven method) Moisture (distillation method) # *Neutral inorqanic salts 302.3 5301.2 1001.1 301.3 5701.1 302.3 5301.2 401.3 304.3 5901.1 401.3 1201.1 1401.2 1402.1 50 1 6201.1 6701 1901 6501 6101.1 801.1 302.3 5301.2 1702 1703.1 1801 66
39、01 301.3 303.1 5801 1101.2 201.1 5201 202.2 6601 D460 #i8 D820 #7-8 D460 #45 D460 116-17 D820 #13-14 D460 #18 D820 #7-8 D460 121-22 D460 #20 D820 #17 D460 #21-22 D460 1153-55 D460 #61 D460 #62-65 0460 #50-52 D820 139-41 ACTIVE D460 #23-26 D820 #46 D820 #35-38 D460 #41-42 D460 f18 D820 #7-8 D460 879-
40、81 D460 W82-83 D460 #88-92 D820 1147 D460 R16-17 D460 819 D820 W15 D460 147-49 D460 #11 D460 1111 D460 112-15 D820 147 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED. TEST METHOD STD. NO. 536A/GEN ALPHABETICAL LIST OF TEST METHODS (Cant.) STATUS
41、 : ACTIVE, CANCELED OR SUPERSEDED BY: Title of Method Fed. Std. Test Method No. ASTM Method No. . Phosphates, total Potassium carbonate and free alkali Pyrophospate, tetrasodium Qualitative test for synthetic detergent in potash-paste soaps Rosin Sampling, methods of Sieve tests Silica present as al
42、ka Soap anhydrous tne s Soap anhydrous, salt-free Sodium Silicate Starch cates Sudsing test Sugars Sugars (Qualitative) Su 1 fa tes Synthetic Detergent Titer of fatty acids Unsaponified plus unsaponifiable matter Unsaponifiable matter nsaponified saponifiable matter Volatile Hydrocarbons Volatile ma
43、tter and moisture 1501.1 305.2 1502.1 5103 701.3 6301.2 101.2 5101.1 2101 1301 401.3 5601.1 6001 1704 6401 2001.2 1705.1 1701 1601.1 6501 901 601.2 602.1 603.1 1801 201.1 5201 DE20 121-28 D460 127 D460 174-76 CANCELED D460 #37-40 DE20 #42-45 ACTIVE ACTIVE ACTIVE D460 #56-57 D460 #21-22 D820 89-12 DE
44、20 Y18-20 D460 184-85 D460 1184-85 ACTIVE D460 #86-87 ACTIVE D460 177-78 DE20 146 D460 143-44 D460 130-32 D460 133-35 D460 #36 D460 #88-92 0460 111 D460 1111 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-FED-STD-53bA 77 B 7777777 000440b 7 = FED. T
45、EST METHOD STD. NO. 536A/GEN ASTM NUMERICAL INDEX SUPERSEDING ASTM STANDARD AND Title of Method Fed. Std. Test Method No. AND SECTION(S) Moisture and Volatile matter (Oven Method) Moisture and Volatile matter (Oven Method) Moisture (Distillation Method) Alcohol insoluble matter Free acid Insoluble m
46、atter in water Alkaline salts Alkali, combined Combined sodium and potassium oxides Free alkali and potassium carbonates Unsaponified plus unsaponifiable matter Uncaponifiable matter Unsaponified matter Rosin Preparation of total fatty matter Titer test Acid number of fatty acids Iodine number of fa
47、tty acids Chlorides Borax Silica Carbonates (Gravimetric method) Carbonates (Volumetric method ) Tetrasodium pyrophosphates Sulfates Glycerol in the absence of sugars Glycerol in the presence of sugars Starch Sugars Volatile hydrocarbons Free acid Anhydrous, salt-free soda soap Alcohol soluble matte
48、r 7 -i 201.1 5201 202.2 301.3 302.3 303.1 304.3 401.2 1901 305.2 601.2 602.5 603.1 701.3 801.1 901 1001.1 1101.2 501 1201.1 1301 1401.2 1402.1 1502.1 1601.1 170 2 1703.1 6401 1705.1 1801 5301.1 5601.1 5701.1 D460 #li D460 #li D460 #12-15 D460 #16-17 D460 C18 D460 119 D460 820 D460 121-22 D460 823-26
49、 D460 827 D460 P30-32 D460 #33-35 0460 #36 D460 #37-40 D460 #41-42 D460 143-44 D460 #45 D460 947-49 D460 #50-52 0460 #53-55 D460 856-57 D460 #61 D460 862-65 D460 #74-76 D460 877-78 D460 #79-81 D460 #82-83 D460 #84-85 D460 C86-87 D460 #88-92 D820 #7-8 D820 #9-12 D820 #13-14 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-
