1、Designation: B243 16aB243 17Standard Terminology ofPowder Metallurgy1This standard is issued under the fixed designation B243; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parentheses indic
2、ates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This terminology standard includes definitions that are helpful in the interpretation and application of powder metallurgyterms.1. Scope1.1 This terminology stand
3、ard includes definitions that are helpful in the interpretation and application of powder metallurgyterms.1.2 This international standard was developed in accordance with internationally recognized principles on standardizationestablished in the Decision on Principles for the Development of Internat
4、ional Standards, Guides and Recommendations issuedby the World Trade Organization Technical Barriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:B331 Test Method for Compressibility of Metal Powders in Uniaxial Compaction3. Terminology3.1 Definitions:acicular powder, nneedle-s
5、haped particles.activated sintering, va sintering process during which the rate of sintering is increased, for example, by addition of a substanceto the powder or by changing sintering conditions.agglomerate, nseveral particles adhering together.air classification, nthe separation of powder into par
6、ticle size fractions by means of an air stream of controlled velocity.angle of repose, nthe basal angle of a pile formed by powder when freely poured under specified conditions onto a horizontalsurface.apparent density, nthe mass of a unit volume of powder, usually expressed as grams per cubic centi
7、metre, determined by aspecified method.apparent hardness, nthe hardness of a PM material (including the effects of porosity), measured using macroindentationhardness equipment.DISCUSSIONSee general description of production, properties, and uses of sintered metal powder bearings and structural parts
8、, paragraph on density and mechanicalproperties, information on hardness measurement, Volume 02.05.2apparent porosity, nspecific to cemented carbides, microstructural features that appear to be pores in a properly prepared,unetched surface; these features may result from uncombined carbon or nonmeta
9、llic inclusions as well as actual porosity.1 This terminology is under the jurisdiction of ASTM Committee B09 on Metal Powders and Metal Powder Products and is the direct responsibility of SubcommitteeB09.01 on Nomenclature and Technical Data.Current edition approved Dec. 1, 2016Nov. 1, 2017. Publis
10、hed February 2017November 2017. Originally approved in 1949. Last previous edition approved in 2016 asB243 16.B243 16A. DOI: 10.1520/B0243-16A.10.1520/B0243-17.2 For a discussion of apparent hardness, see the section on Density in General Description of Production, Properties, and Uses of Sintered M
11、etal Powder Bearings andStructural Parts, which appears in the Annual Book of ASTM Standards, Vol 02.05.This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Becauseit may not be techni
12、cally possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current versionof the standard as published by ASTM is to be considered the official document.Copyright ASTM International, 100 Barr Harbor Drive, PO Bo
13、x C700, West Conshohocken, PA 19428-2959. United States1atomization, nthe dispersion of a molten metal into particles by a rapidly moving gas or liquid stream or by mechanical means.atomized metal powder, nmetal powder produced by the dispersion of a molten metal by a rapidly moving gas, or liquid s
14、tream,or by mechanical dispersionbinder, na cementing medium; either a material added to the powder to increase the green strength of the compact, and whichis expelled during sintering; or a material (usually of relatively lower melting point) added to a powder mixture for the specificpurpose of cem
15、enting together powder particles which alone would not sinter into a strong body.binder (MIM), na mixture of polymers or other materials, or both, that when combined with metal powders enables the mixtureto flow during the injection molding process. The binder imparts green strength to the MIM part
16、and allows it to retain its moldedshape.binder removal, nthe chemical or thermal extraction of binder from a compact. Synonymous with debinding.blank, na pressed, presintered, or fully sintered compact, usually in the unfinished condition, requiring cutting, machining, orsome other operation to give
17、 it its final shape.blending, nthe thorough intermingling of powders of the same nominal composition (not to be confused with mixing).blister crack, ntypically small defects (star burst) over or around a bump or blister.DISCUSSIONThese may occur during sintering as a result of rapid outgassing of th
18、e lubricant. The rapid outgassing may be caused by the specified amount oflubricant being subjected to an excessive heating rate. The defects may also be caused by “concentrated balls” of lubricant, or moisture. During thesintering of the copper base PM parts, hydrogen gas from the furnace atmospher
19、e can diffuse into the compact and react with residual oxygen,producing steam that can form blisters and cracks. In that industry, this is also called embrittlement, and is not to be confused with the hydrogenembrittlement of high strength steel.blistered compact, na sintered object characterized by
20、 having blisters or eruptions on the surface.DISCUSSIONIn ferrous materials, this effect is often caused by in situ gas decomposition and soot formation that forces particles apart and causes the compact toblister.bridging, vthe formation of arched cavities in a powder mass.briquet, nsee compact.bro
21、wn part, nan MIM part that has had a majority of the binder (first stage) removed. Synonymous with debound part.bulk density, nthe mass per unit volume of a powder under nonstandard conditions, for example, in a shipping container (notto be confused with apparent density).burn-off, nremoval of organ
22、ic additives (binder or lubricant) from a compact by heating.cake, na bonded mass of unpressed metal powder.DISCUSSIONOften refers to the form of powder as it exits a furnace.carbonyl powder, na metal powder prepared by the thermal decomposition of a metal carbonylcavity (MIM), nthe hollow space of
23、a mold that forms one part.cemented carbide, nsintered material characterized by high strength and wear resistance and comprising one or more carbidesof refractory metals as the main component bonded by metallic binder phase.cermet, nsintered material containing at least one metallic phase and at le
24、ast one nonmetallic phase that is generally of a ceramicnature.chemical deposition, nthe precipitation of one metal from a solution of its salts by the addition of another metal or reagent tothe solution.chemically precipitated metal powder, npowder produced by the reduction of a metal from a soluti
25、on of its salts either by theaddition of another metal higher in the electromotive series or by other reducing agent.B243 172classification, nseparation of a powder into fractions according to particle size.closed pore, na pore not communicating or connected with an exterior surface.coin, vto repres
26、s a sintered compact to obtain a definite surface configuration. Synonymous with emboss (not to be confused withrestrike or size).cold isostatic pressing, nthe pressing of a powder, compact, or sintered object by subjecting it, at ambient temperature, tonominally equal pressure from every direction.
27、cold pressing, nthe forming of a compact at room temperature.cold welding, ncohesion between two surfaces of metal, generally under the influence of externally applied pressure, at roomtemperature.DISCUSSIONOften used to describe the mechanism by which powder particles develop initial bonds and a pr
28、essed compact develops green minuted powder, na powder produced by mechanical attrition of solid metal or powdercommunicating pores, nsee interconnected pact, nan object produced by the compression of metal powder, generally while confined in a die, with or without theinclusion of nonmetallic consti
29、tuents. Synonymous with pactibility, na conceptual term, encompassing the powder characteristics of compressibility, green strength, edge retention,and lamination tendency, that relates to the ability of a powder to be consolidated into a usable green pacting, na process in which a powder held in a
30、die or other container is subjected to an external force in order to densifythe powder and produce a compact of prescribed shape and pacting pressure (uniaxial), napplied force divided by the projected area of contact with the punch(es).compacting tool set, nan assembly of tooling items in which pow
31、der is pressed.DISCUSSIONMay include a die, punches, and core pletely alloyed powder, nsee pre-alloyed posite compact, na metal powder compact consisting of two or more adhering layers, rings, or other shapes of differentmetals or alloys with each material retaining its original posite powder, na po
32、wder in which each particle consists of two or more distinct pound compact, na metal powder compact consisting of mixed metals, the particles of which are joined by pressing orsintering, or both, with each metal particle retaining substantially its original pounding (MIM), nprocess whereby the metal
33、 powders and molten binder constituents are combined to produce pressibility, nthe capacity of a metal powder to be densified under a uniaxially applied pressure in a closed die.DISCUSSIONCompressibility is measured in accordance with Test Method B331 and may be expressed numerically as the pressure
34、 to reach a specified density, oralternatively the density at a given pressure.3compression ratio, nthe ratio of the volume of the loose powder to the volume of the compact made from it. Synonymous withfill ratio.continuous sintering, vpresintering, or sintering, in such manner that the objects are
35、advanced through the furnace at a fixedrate by manual or mechanical means. Synonymous with stoking.3 See Test Method B331.B243 173cooling rate, nthe average temperature change per second between prescribed temperatures during the cooling phase of athermal process.core rod, na member of the compactin
36、g tool set that forms internal features such as splines, diameters, keyways, or other profilesin a PM compact.cored bar, na compact of bar shape heated by its own electrical resistance to a temperature high enough to melt its interior.crack (RD), ngenerally a planar defect.cracked ammonia, nsee diss
37、ociated ammonia.cracks (rigid die system (RD), nthe following names and definitions apply only to items produced in a rigid die system (RD)as opposed to those cracks produced by other systems, that is, metal injection molding, vacuum hot pressing, and so forth.4cross-product contamination, nthe unin
38、tentional mixing of powders with distinct differences in either physical characteristicsor chemical composition or both.cut, nsee fraction.debinding, nsee binder removal.debound part, nsee brown part.dendritic powder, nparticles, usually of electrolytic origin, having the typical pine tree structure
39、.densification crack, na defect caused by differential stresses in a region of a part that has experienced large differences inshrinkage during sintering.density (dry), nsee sintered density.density (wet), nsee impregnated density.density ratio, nthe ratio, often expressed as a percentage, of the de
40、nsity of a porous material to the density of the same materialcompletely free of porosity. Synonymous with relative density.die, na member of the compacting tool set forming the cavity in which the powder is compacted or a PM compact is repressed.die body, nthe stationary or fixed part of a die.die
41、insert, na removable liner or part of a die body.die set, nthe parts of a press that hold and locate the die in proper relation to the punches.diffusion-alloyed powder, na partially alloyed powder produced by means of a diffusion anneal.dimensional change of a compact, nthe difference, at room tempe
42、rature, between the size of the sintered specimen and the diesize.DISCUSSIONThe difference in dimensions is usually reported as a percentage of the die size. It should include a (+) when the sintered part is larger than the diesize and a () when the sintered part is smaller than the die size.disinte
43、gration, nthe reduction of massive material to powder.dispersion-strengthened material, na material consisting of a metal and finely dispersed, substantially insoluble, metallic ornonmetallic phase.dissociated ammonia, na reducing gas produced by the thermal decomposition of anhydrous ammonia over a
44、 catalyst, resultingin a gas of 75 % hydrogen and 25 % nitrogen. Synonymous with cracked ammonia.double-action pressing, na method by which a powder is pressed in a die between opposing moving punches.double press-double sinter, nto repress and sinter a previously presintered or sintered compact.DIS
45、CUSSION4 There is detailed information on numerous cracks, their location, cause, and prevention in a handbook published by Metal Powder Industries Federation, Princeton, NewJersey, “The Common Cracks in PM Compacts” by D. Zenger and H. Cai.B243 174Used to describe a four-step manufacturing process.
46、ejection crack, na defect that occurs during the removal of the compact from the tooling (usually occurs in multilevel parts thatare not supported uniformly on all lower surfaces).electrolytic powder, npowder produced by electrolytic deposition or by the pulverization of an electrodeposit.endothermi
47、c gas, na reducing gas atmosphere used in sintering, produced by the reaction of a hydrocarbon vapor and air overa catalyst with the use of an external heat source. It is low in carbon dioxide and water vapor while containing combustiblesof about 60 atomic percent hydrogen and carbon monoxide combin
48、ed.equalizing, nsee blending.exothermic atmosphere (gas), na reducing gas atmosphere used in sintering, produced by partial or complete combustion ofhydrocarbon fuel gas and air with the associated generation of heat. The maximum combustible content is approximately 25atomic percent.explosive compac
49、tion, nhigh-energy consolidation of powders by means of a detonation shock wave.exudation, nthe action by which all or a portion of the low melting constituent of a compact is forced to the surface duringsintering. Sometimes referred to as “bleed out.” Synonymous with sweating.feedshoe, na part of the compacting press that delivers powder to the die c
