1、Designation: D 2583 07Standard Test Method forIndentation Hardness of Rigid Plastics by Means of a BarcolImpressor1This standard is issued under the fixed designation D 2583; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year
2、 of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope*1.1 This test method covers the det
3、ermination of indentationhardness of both reinforced and nonreinforced rigid plasticsusing a Barcol Impressor, Model No. 934-1 and Model No.935.1.2 The values stated in SI units are to be regarded asstandard. The values given in brackets are for information only.1.3 This standard does not purport to
4、 address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.NOTE 1There is no known ISO equivalent to this test
5、method.2. Referenced Documents2.1 ASTM Standards:2D 618 Practice for Conditioning Plastics for TestingD 883 Terminology Relating to PlasticsD 4000 Classification System for Specifying Plastic Mate-rialsE 691 Practice for Conducting an Interlaboratory Study toDetermine the Precision of a Test Method3
6、. Terminology3.1 DefinitionsFor definitions of technical terms pertain-ing to plastics used in this test method, see Terminology D 883.4. Summary of Test Method4.1 A materials surface hardness is determined through theuse of a Barcol Impressor. The relative depth of penetration ofthe Impressors inde
7、ntor provides a comparative measure ofthe materials hardness. The Model No. 934-1 and Model No.935 Barcol Impressors are designated for use with plastics.Within the range of hardness measured by these Impressors theModel No. 934-1 is used for measuring harder materials andthe Model No. 935 is used f
8、or measuring softer materials.5. Significance and Use5.1 The Barcol Impressor is portable and therefore suitablefor testing the hardness of fabricated parts and individual testspecimens for production control purposes.5.2 Before proceeding with this test method, reference shallbe made to the specifi
9、cation of the material being tested. Table1 of Classification System D 4000 lists the ASTM materialstandards that currently exist. Any test specimen preparation,conditioning, dimensions, or testing parameters or combinationthereof covered in the relevant ASTM material specificationshall take precede
10、nce over those mentioned in this test method.If there are no relevant ASTM material specifications, then thedefault conditions apply.1This test method is under the jurisdiction of ASTM Committee D20 on Plasticsand is the direct responsibility of Subcommittee D20.10 on Mechanical Properties.Current e
11、dition approved March 1, 2007. Published March 2007. Originallyapproved in 1967. Last previous edition approved in 2006 as D 2583 - 06.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume inf
12、ormation, refer to the standards Document Summary page onthe ASTM website.FIG. 1 Barcol Impressor1*A Summary of Changes section appears at the end of this standard.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.6. Apparatus ( Fig. 1
13、and Fig. 2)6.1 Indentor3The indentor shall consist of a hardenedsteel truncated cone having an angle of 26 with a flat tip of0.157 mm 0.0062 in. in diameter. It shall fit into a hollowspindle and be held down by a spring-loaded plunger. See Fig.2.6.2 Indicating DeviceThe indicating dial shall have 1
14、00divisions, each representing a depth of 0.0076-mm 0.0003-in.penetration. The higher the reading is, the harder the materialis.6.3 Calibration Standards“Hard” and “soft” aluminumalloy disks supplied by the manufacturer of the instrument.Other disks should not be used, even if they are of the sameal
15、loy and temper as the manufacturers disks, as the hardnessof aluminum varies within any given alloy-temper parameter.6.4 A smooth glass plate is also needed.7. Test Specimens7.1 The testing area shall be smooth and free from mechani-cal defects.7.2 DimensionsTest specimens shall be at least 1.5 mm11
16、6 in. thick and large enough to ensure a minimum distanceof3mm18 in. in any direction from the indentor point to theedge of the specimen, as well as from test point to test point.8. Preparation and Operation of Apparatus8.1 The preparation and operation of Models 934-1 and 935are identical. Place th
17、e Impressor and the material to be tested(or the calibration disk) on a solidly supported, flat, hard, firmsurface such as stone, metal, or ceramic. If softer supportingsurfaces are used, a false low instrument reading may occur.8.2 Set the point sleeve on the surface to be tested. Set thelegs on th
18、e same surface or on solid material of the samethickness, so that the indentor is perpendicular to the surfacebeing tested. Grasp the instrument firmly between the legs andpoint sleeve. Apply a uniform downward force quickly, byhand, increasing the force on the case until the dial indicationreaches
19、a maximum (Note 3). Take care to avoid sliding orscraping while the indentor is in contact with the surface beingtested. Record the maximum reading.NOTE 2It is recommended that measurements be made with theModel 934-1 Impressor when values above 90 are obtained with theModel 935 Impressor and that m
20、easurements be made with the Model 935Impressor when values less than 20 are obtained with the Model No.934-1 Impressor. Values below 10 using the Model 935 Impressor areinexact and should not be reported.NOTE 3Drift in readings from the maximum occurs in some materialsand can be nonlinear with time
21、.9. Calibration9.1 With the plunger upper guide backed out until it justengages the spring, place the Impressor on a glass surface andpress down until the point is forced all the way back into thelower plunger guide. The indicator should now read 100. If itdoes not, loosen the lock-nut and turn the
22、lower plunger guidein or out to obtain a 100 reading. Next, read the “hard”aluminum alloy disk supplied by the manufacturer of theImpressor and, if necessary, adjust so that the reading is withinthe range marked on the disk. Then do the same with the “soft”disk. If these readings cannot be obtained,
23、 subsequent mea-surements are not valid.10. Conditioning10.1 ConditioningCondition the test specimens at 23 62C 73.4 6 3.6F and 50 6 5 % relative humidity for at least40 h prior to test in accordance with Procedure A of PracticeD 618, unless otherwise specified by the contract or relevantASTM materi
24、al specification. In cases of disagreement, thetolerances shall be 61C 61.8F and 62 % relative humid-ity.10.2 Test ConditionsConduct tests in the standard labora-tory atmosphere of 23 6 2C 73.4 6 3.6F and 50 6 5%relative humidity, unless otherwise specified by the contract or3The sole source of supp
25、ly of the apparatus known to the committee at this timeis Eurotherm/Barber-Colman, 741F Miller Drive, Leesburg, VA 201758993. Ifyou are aware of alternative suppliers, please provide this information to ASTMInternational Headquarters. Your comments will receive careful consideration at ameeting of t
26、he responsible technical committee,1which you may attend.FIG. 2 Diagram of Barcol ImpressorD2583072relevant ASTM material specification. In cases of disagree-ment, the tolerances shall be 61C 61.8F and 62%relative humidity.11. Procedure11.1 Observing the precautions of Section 8, make measure-ments
27、on the specimens to be tested (Note 4). Indentationsshould not be made within 3 mm 18 in. of the edge of thespecimen or of other indentations.NOTE 4Curved surfaces are more difficult to support. When the loadis applied, bending and spring action in the specimen should be avoided.12. Number of Readin
28、gs12.1 Application of the Barcol Impressor to reinforcedplastic (nonhomogeneous) materials will produce greater varia-tion in hardness readings than on nonreinforced (homoge-neous) materials. This greater variation is mainly caused by thedifference in hardness between resin and filler materials inco
29、ntact with the small diameter indentor. There is less variationin hardness readings on harder materials in the range of 50Barcol and higher and considerably more variation in thereadings of softer materials. On homogeneous materials, fivereadings are needed to maintain a variance-of-average of 0.28a
30、t a 60 Barcol reading; for the same variance-of-average at 30Barcol, eight readings are needed. On reinforced plastics, inorder to maintain a variance-of-average of 0.78 at 60 Barcol,ten readings are needed; and 29 readings are needed for thesame variance at the 30 Barcol level (Table 1).NOTE 5These
31、 findings were obtained with a round robin conducted ina workshop with all participants present. Eight plastic materials ofdifferent hardness were evaluated with six different Barcol (934-1)Impressors.13. Report13.1 Report the following information:13.1.1 Identification of material tested,13.1.2 Con
32、ditioning of specimen,13.1.3 Model number of Impressor,13.1.4 Number of readings taken,13.1.5 Average of hardness values rounded to the nearestwhole scale reading,13.1.6 Date of test, and13.1.7 Test method number and published/revision date.14. Precision and Bias414.1 No precision statement using Mo
33、del 935 can be offeredat this time.14.2 Table 2 is based on a round robin conducted in 1981,in accordance with Practice E 691, involving five materialstested by nine laboratories using Model No. 934-1. For eachmaterial, all the samples were prepared at one source. Eachlaboratory obtained three test
34、results for each material. For thematerials shown, the indicated number of individual determi-nations were averaged to calculate each test result as follows:Material No. of Determinationsusing Model No. 934-1SAN 8BMC 22SAN reinforced with 20 % glass 22Polyester Mat Laminate (thermoset) 16SMC (sheet
35、molding compound) 16(WarningThe following explanations of Irand IR(14.3-14.3.3) are only intended to present a meaningful way ofconsidering the approximate precision of this test method. Thedata in Table 2 should not be rigorously applied to acceptanceor rejection of material, as those data are spec
36、ific to the roundrobin and may not be representative of other lots, materials, orlaboratories. Users of this test method should apply theprinciples outlined in Practice E 691 to generate data specificto their laboratory and materials, or between specific laborato-ries. The principles of 14.3-14.3.3
37、would then be valid for suchdata.)14.3 Concept of Irand IRIf Srand SRwere calculatedfrom a large enough body of data, and for test results that wereaverages from the numbers of determinations stated in 14.2:14.3.1 Repeatability, Ir(Comparing two test results for thesame material, obtained by the sam
38、e operator using the sameBarcol Impressor on the same day)The samples representedby the two test results should be regarded as not havingequivalent hardness if the test results differed by more than theIrvalue for that material and condition.4Supporting data are available from ASTM Headquarters. Req
39、uest RR: D20-1087.TABLE 1 Recommended Sample Sizes to Equalize the Varianceof the Average for Model No. 934-1Homogeneous MaterialHardnessM-934ScaleReadingVarianceCoefficient ofVariation, %VarianceofAverageMinimumNumber ofReadings20 2.47 2.6 0.27 930 2.20 1.7 0.28 840 1.93 1.3 0.27 750 1.66 1.1 0.28
40、660 1.39 0.9 0.28 570 1.12 0.8 0.28 480 0.85 0.7 0.28 3Nonhomogeneous Material(Reinforced Plastics)30 22.4 2.9 0.77 2940 17.2 2.2 0.78 2250 12.0 1.7 0.75 1660 7.8 1.5 0.78 1070 3.6 1.2 0.75 5TABLE 2 Precision Data for Model No. 934-1MaterialValues in Units of Barcol HardnessAverage SrASRBIrCIRDSAN 3
41、5 1.04 2.93 3 8BMC 39 0.95 3.75 3 11Reinforced SAN 44 1.11 2.25 3 6Polyester laminate 55 1.45 1.93 4 5SMC 61 1.14 2.15 3 6ASr= within-laboratory standard deviation of the average.BSR= between-laboratories standard deviation of the average.CIr= 2.83 Sr.DIR= 2.83 SR.D258307314.3.2 Reproducibility, IR(
42、Comparing two test results forthe same material, obtained by different operators using differ-ent Barcol Impressors on different days)The samples repre-sented by the two test results should be regarded as not havingequivalent hardness if the test results differed by more than theIRvalue for that mat
43、erial and condition.14.3.3 Any judgment in accordance with 14.3.1 and 14.3.2would have an approximate 95 % (0.95) probability of beingcorrect.14.4 BiasThere are no recognized standards on which tobase an estimate of bias for this test method.15. Keywords15.1 Barcol Hardness Impressor; Models 934-1 a
44、nd 935;hardness; indentation hardness; rigid plasticsSUMMARY OF CHANGESCommittee D20 has identified the location of selected changes to this standard since the last issue(D 2583 - 06) that may impact the use of this standard. (March 1, 2007)(1) Revised 11.1.Committee D20 has identified the location
45、of selected changes to this standard since the last issue(D 2583 - 95(2001) that may impact the use of this standard. (September 1, 2006)(1) Editorial revisions made throughout. (2) Added Summary of Changes section.ASTM International takes no position respecting the validity of any patent rights ass
46、erted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time b
47、y the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will rece
48、ive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM Inte
49、rnational, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D2583074
