1、 中华人民共和国行业标准 白兰地、威士忌浸出物的试验方法 QB/T 1326.8-91 1 主题内容与适用范围 本标准规定了用比重瓶法测定白兰地、威士忌酒浸出物的试验方法。 本标准适用于白兰地、威士忌酒浸出物的测定。 2 引用标准 QB/T 1326.3 白兰地、威士忌、俄得克酒精度的试验方法 3 原理 以蒸发法去除试样中的酒精,向蒸发后的残液中补加水,恢复原体积,然后用比重瓶法 测其比重,根据比重查附录 A 比重-浸出物对照表(补充件), 求得浸出物含量。 4 试验方法 4.1 仪器 4.1.1 瓷蒸发皿:150 mL 。 4.1.2 高精度恒温水浴:20.0 0.1。 4.1.3 附温度计
2、比重瓶:25 或 50 mL 。 4.2 分析步骤 4.2.1 样品制备 用容量瓶量取 20试样 100 mL 于瓷蒸发皿中,蒸发至约原体积的 1/3 时,取下,冷却, 补 加水于 20恢复至原体积,混匀。 4.2.2 测定 制备好的样品, 按 QB/T 1326.3 中 3.2.2 和 3.2.3 同样操作,测其比重,根据比重查附录 A 比重-浸出物对照表,求得浸出物含量(g/L) 。 所得结果表示至一位小数。 5 结果的允许差 平行试验测定值之差,不得超过平均值的 5 。 附 录 A 比重-浸出物对照表 ( 补充件) 表 A1 - 比 重 浸出物 比 重 浸出物 比 重 浸出物 比 重浸出
3、物 (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) - 1.000 0 0.00 1.005 0 12.791.010 0 25.70 1.015 0 38.75 1.000 1 0.25 1.005 1 13.041.010 1 25.96 1.015 1 39.00 1.000 2 0.50 1.005 2 13.291.010 2 26.21 1.015 2 39.26 1.000 3 0.74 1.005 3 13.551.010 3 26.47 1.015 3 39.52 1.000 4 0.99 1.005 4 13.
4、801.010 4 26.72 1.015 4 39.78 1.000 5 1.24 1.005 5 14.051.010 5 26.98 1.015 5 40.04 1.000 6 1.49 1.005 6 14.391.010 6 27.23 1.015 6 40.29 1.000 7 1.74 1.005 7 14.721.010 7 27.57 1.015 7 40.55 1.000 8 1.99 1.005 8 15.061.010 8 27.91 1.015 8 40.81 1.000 9 2.24 1.005 9 15.311.010 9 28.25 1.015 9 41.07
5、1.001 0 2.49 1.006 0 15.571.011 0 28.50 1.016 0 41.32 1.001 1 2.74 1.006 1 15.821.011 1 28.76 1.016 1 41.58 1.001 2 2.99 1.006 2 16.071.011 2 29.01 1.016 2 41.84 1.001 3 3.24 1.006 3 16.321.011 3 29.27 1.016 3 42.10 1.001 4 3.49 1.006 4 16.581.011 4 29.52 1.016 4 42.35 1.001 5 3.74 1.006 5 16.831.01
6、1 5 29.78 1.016 5 42.61 1.001 6 3.99 1.006 6 17.081.011 6 30.03 1.016 6 42.87 1.001 7 4.33 1.006 7 17.331.011 7 30.28 1.016 7 43.13 1.001 8 4.66 1.006 8 17.591.011 8 30.54 1.016 8 43.38 1.001 9 5.00 1.006 9 17.841.011 9 30.80 1.016 9 43.64 1.002 0 5.25 1.007 0 18.091.012 0 31.06 1.017 0 43.90 1.002
7、1 5.50 1.007 1 18.341.012 1 31.32 1.017 1 44.16 1.002 2 5.75 1.007 2 18.591.012 2 31.58 1.017 2 44.42 1.002 3 6.00 1.007 3 18.851.012 3 31.83 1.017 3 44.68 1.002 4 6.25 1.007 4 19.101.012 4 32.09 1.017 4 44.94 1.002 5 6.50 1.007 5 19.361.012 5 32.34 1.017 5 45.20 1.002 6 6.75 1.007 6 19.611.012 6 32
8、.60 1.017 6 45.45 1.002 7 7.00 1.007 7 19.871.012 7 32.85 1.017 7 45.71 1.002 8 7.25 1.007 8 20.121.012 8 33.11 1.017 8 45.97 1.002 9 7.50 1.007 9 20.371.012 9 33.36 1.017 9 46.23 1.003 0 7.75 1.008 0 20.631.013 0 33.62 1.018 0 46.48 1.003 1 8.00 1.008 1 20.881.013 1 33.87 1.018 1 46.74 1.003 2 8.25
9、 1.008 2 21.131.013 2 34.13 1.018 2 47.00 1.003 3 8.50 1.008 3 21.381.013 3 34.39 1.018 3 47.26 1.003 4 8.75 1.008 4 21.641.013 4 34.65 1.018 4 47.52 1.003 5 9.00 1.008 5 21.891.013 5 34.90 1.018 5 47.78 1.003 6 9.25 1.008 6 22.141.013 6 35.16 1.018 6 48.04 1.003 7 9.50 1.008 7 22.401.013 7 35.41 1.
10、018 7 48.30 1.003 8 9.75 1.008 8 22.651.013 8 35.67 1.018 8 48.55 1.003 9 10.00 1.008 9 22.911.013 9 35.93 1.018 9 48.81 1.004 0 10.26 1.009 0 23.161.014 0 36.18 1.019 0 49.07 1.004 1 10.51 1.009 1 23.411.014 1 36.44 1.019 1 49.33 1.004 2 10.77 1.009 2 23.671.014 2 36.70 1.019 2 49.59 1.004 3 11.02
11、1.009 3 23.921.014 3 36.95 1.019 3 49.85 1.004 4 11.27 1.009 4 24.181.014 4 37.21 1.019 4 50.11 1.004 5 11.53 1.009 5 24.431.014 5 37.46 1.019 5 50.37 1.004 6 11.78 1.009 6 24.691.014 6 37.72 1.019 6 50.63 1.004 7 12.03 1.009 7 24.941.014 7 37.98 1.019 7 50.89 1.004 8 12.28 1.009 8 25.191.014 8 38.2
12、3 1.019 8 51.15 1.004 9 12.53 1.009 9 25.451.014 9 38.49 1.019 9 51.41 - 续 表 A1 - 比 重 浸出物 比 重 浸出物 比 重 浸出物 比 重浸出物 (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) - 1.020 0 51.67 1.025 0 64.71 1.030 0 77.62 1.035 0 90.65 1.020 1 51.93 1.025 1 64.97 1.030 1 77.89 1.035 1 90.92 1.020 2 52.19 1.0
13、25 2 65.24 1.030 2 78.15 1.035 2 91.19 1.020 3 52.45 1.025 3 65.50 1.030 3 78.42 1.035 3 91.45 1.020 4 52.70 1.025 4 65.76 1.030 4 78.68 1.035 4 91.72 1.020 5 52.96 1.025 5 66.03 1.030 5 78.95 1.035 5 91.99 1.020 6 53.22 1.025 6 66.29 1.030 6 79.21 1.035 6 92.26 1.020 7 53.48 1.025 7 66.55 1.030 7 7
14、9.48 1.035 7 92.53 1.020 8 53.74 1.025 8 66.81 1.030 8 79.74 1.035 8 92.79 1.020 9 54.00 1.025 9 67.08 1.030 9 80.01 1.035 9 93.06 1.021 0 54.35 1.026 0 67.34 1.031 0 80.27 1.036 0 93.33 1.021 1 54.70 1.026 1 67.60 1.031 1 80.53 1.036 1 93.60 1.021 2 55.05 1.026 2 67.86 1.031 2 80.80 1.036 2 93.86 1
15、.021 3 55.26 1.026 3 68.13 1.031 3 81.06 1.036 3 94.13 1.021 4 55.47 1.026 4 68.39 1.031 4 81.33 1.036 4 94.40 1.021 5 55.67 1.026 5 68.65 1.031 5 81.60 1.036 5 94.67 1.021 6 55.88 1.026 6 68.91 1.031 6 81.86 1.036 6 94.93 1.021 7 56.09 1.026 7 69.18 1.031 7 82.13 1.036 7 95.20 1.021 8 56.35 1.026 8
16、 69.44 1.031 8 82.39 1.036 8 95.47 1.021 9 56.61 1.026 9 69.70 1.031 9 82.66 1.036 9 95.74 1.022 0 56.87 1.027 0 69.96 1.032 0 82.92 1.037 0 96.00 1.022 1 57.13 1.027 1 70.22 1.032 1 83.19 1.037 1 96.27 1.022 2 57.39 1.027 2 70.49 1.032 2 83.45 1.037 2 96.54 1.022 3 57.65 1.027 3 70.75 1.032 3 83.72
17、 1.037 3 96.81 1.022 4 57.91 1.027 4 71.01 1.032 4 83.99 1.037 4 97.08 1.022 5 58.17 1.027 5 71.28 1.032 5 84.25 1.037 5 97.35 1.022 6 58.43 1.027 6 71.54 1.032 6 84.52 1.037 6 97.56 1.022 7 58.70 1.027 7 71.80 1.032 7 84.79 1.037 7 97.78 1.022 8 58.96 1.027 8 72.07 1.032 8 85.05 1.037 8 97.99 1.022
18、 9 59.22 1.027 9 72.33 1.032 9 85.32 1.037 9 98.21 1.023 0 59.48 1.028 0 72.60 1.033 0 85.58 1.038 0 98.42 1.023 1 59.74 1.028 1 72.86 1.033 1 85.85 1.038 1 98.69 1.023 2 60.00 1.028 2 73.13 1.033 2 86.11 1.038 2 98.96 1.023 3 60.26 1.028 3 73.39 1.033 3 86.38 1.038 3 99.23 1.023 4 60.52 1.028 4 73.
19、66 1.033 4 86.65 1.038 4 99.50 1.023 5 60.79 1.028 5 73.92 1.033 5 86.92 1.038 5 99.77 1.023 6 61.05 1.028 6 74.18 1.033 6 87.18 1.038 6 100.04 1.023 7 61.31 1.028 7 74.45 1.033 7 87.45 1.038 7 100.30 1.023 8 61.57 1.028 8 74.71 1.033 8 87.71 1.038 8 100.57 1.023 9 61.83 1.028 9 74.97 1.033 9 87.92
20、1.038 9 100.84 1.024 0 62.09 1.029 0 75.18 1.034 0 88.14 1.039 0 101.11 1.024 1 62.35 1.029 1 75.39 1.034 1 88.35 1.039 1 101.38 1.024 2 62.61 1.029 2 75.61 1.034 2 88.57 1.039 2 101.65 1.024 3 62.88 1.029 3 75.82 1.034 3 88.78 1.039 3 101.92 1.024 4 63.14 1.029 4 76.03 1.034 4 89.05 1.039 4 102.19
21、1.024 5 63.40 1.029 5 76.30 1.034 5 89.32 1.039 5 102.46 1.024 6 63.66 1.029 6 76.56 1.034 6 89.58 1.039 6 102.73 1.024 7 63.93 1.029 7 76.83 1.034 7 89.85 1.039 7 103.02 1.024 8 64.19 1.029 8 77.09 1.034 8 90.12 1.039 8 103.30 1.024 9 64.45 1.029 9 77.36 1.034 9 90.39 1.039 9 103.59 - 续 表 A1 - 比 重
22、浸出物 比 重 浸出物 比 重 浸出物 比 重浸出物 (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) - 1.040 0 103.87 1.045 0 116.85 1.050 0 129.74 1.055 0 142.96 1.040 1 104.13 1.045 1 117.12 1.050 1 129.96 1.055 1 143.24 1.040 2 104.38 1.045 2 117.38 1.050 2 130.24 1.055 2 143.46 1.040 3 104.64 1.045 3 117.65 1.050
23、 3 130.51 1.055 3 143.68 1.040 4 104.89 1.045 4 117.92 1.050 4 130.79 1.055 4 143.91 1.040 5 105.11 1.045 5 118.14 1.050 5 131.06 1.055 5 144.13 1.040 6 105.32 1.045 6 118.36 1.050 6 131.34 1.055 6 144.35 1.040 7 105.54 1.045 7 118.57 1.050 7 131.62 1.055 7 144.63 1.040 8 105.75 1.045 8 118.79 1.050
24、 8 131.89 1.055 8 144.91 1.040 9 105.97 1.045 9 119.01 1.050 9 132.17 1.055 9 145.18 1.041 0 106.24 1.046 0 119.28 1.051 0 132.45 1.056 0 145.46 1.041 1 106.51 1.046 1 119.56 1.051 1 132.72 1.056 1 145.74 1.041 2 106.78 1.046 2 119.83 1.051 2 133.00 1.056 2 146.02 1.041 3 107.05 1.046 3 120.10 1.051
25、 3 133.27 1.056 3 146.29 1.041 4 107.32 1.046 4 120.38 1.051 4 133.54 1.056 4 146.57 1.041 5 107.58 1.046 5 120.65 1.051 5 133.82 1.056 5 146.85 1.041 6 107.85 1.046 6 120.93 1.051 6 134.09 1.056 6 147.13 1.041 7 108.12 1.046 7 121.20 1.051 7 134.37 1.056 7 147.41 1.041 8 108.40 1.046 8 121.47 1.051
26、 8 134.59 1.056 8 147.69 1.041 9 108.67 1.046 9 121.75 1.051 9 134.81 1.056 9 147.91 1.042 0 108.95 1.047 0 122.02 1.052 0 135.04 1.057 0 148.13 1.042 1 109.22 1.047 1 122.29 1.052 1 135.26 1.057 1 148.36 1.042 2 109.50 1.047 2 122.56 1.052 2 135.48 1.057 2 148.58 1.042 3 109.77 1.047 3 122.83 1.052
27、 3 135.76 1.057 3 148.80 1.042 4 110.05 1.047 4 123.11 1.052 4 136.03 1.057 4 149.08 1.042 5 110.32 1.047 5 123.38 1.052 5 136.31 1.057 5 149.36 1.042 6 110.59 1.047 6 123.60 1.052 6 136.58 1.057 6 149.64 1.042 7 110.86 1.047 7 123.82 1.052 7 136.86 1.057 7 149.92 1.042 8 111.12 1.047 8 124.04 1.052
28、 8 137.14 1.057 8 150.20 1.042 9 111.39 1.047 9 124.26 1.052 9 137.41 1.057 9 150.48 1.043 0 111.66 1.048 0 124.48 1.053 0 137.69 1.058 0 150.75 1.043 1 111.93 1.048 1 124.76 1.053 1 137.97 1.058 1 151.03 1.043 2 112.20 1.048 2 125.03 1.053 2 138.24 1.058 2 151.29 1.043 3 112.47 1.048 3 125.31 1.053
29、 3 138.52 1.058 3 151.55 1.043 4 112.71 1.048 4 125.58 1.053 4 138.79 1.058 4 151.81 1.043 5 112.95 1.048 5 125.85 1.053 5 139.01 1.058 5 152.07 1.043 6 113.20 1.048 6 126.13 1.053 6 139.24 1.058 6 152.36 1.043 7 113.44 1.048 7 126.40 1.053 7 139.46 1.058 7 152.65 1.043 8 113.68 1.048 8 126.67 1.053
30、 8 139.69 1.058 8 152.94 1.043 9 113.92 1.048 9 126.95 1.053 9 139.91 1.058 9 153.23 1.044 0 114.17 1.049 0 127.22 1.054 0 140.19 1.059 0 153.46 1.044 1 114.41 1.049 1 127.50 1.054 1 140.47 1.059 1 153.69 1.044 2 114.65 1.049 2 127.77 1.054 2 140.74 1.059 2 153.93 1.044 3 114.92 1.049 3 128.04 1.054
31、 3 141.02 1.059 3 154.16 1.044 4 115.20 1.049 4 128.32 1.054 4 141.30 1.059 4 154.39 1.044 5 115.47 1.049 5 128.59 1.054 5 141.58 1.059 5 154.67 1.044 6 115.74 1.049 6 128.87 1.054 6 141.85 1.059 6 154.95 1.044 7 116.02 1.049 7 129.09 1.054 7 142.13 1.059 7 155.23 1.044 8 116.30 1.049 8 129.31 1.054
32、 8 142.41 1.059 8 155.51 1.044 9 116.57 1.049 9 129.52 1.054 9 142.69 1.059 9 155.73 - 续 表 A1 - 比 重 浸出物 比 重 浸出物 比 重 浸出物 比 重浸出物 (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) (20/20) (g/L) - 1.060 0 155.96 1.065 0 169.02 1.070 0 182.10 1.075 0 195.29 1.060 1 156.18 1.065 1 169.31 1.070 1 182.38 1.075 1 19
33、5.52 1.060 2 156.41 1.065 2 169.59 1.070 2 182.67 1.075 2 195.75 1.060 3 156.63 1.065 3 169.88 1.070 3 182.96 1.075 3 195.98 1.060 4 156.91 1.065 4 170.16 1.070 4 183.24 1.075 4 196.21 1.060 5 157.19 1.065 5 170.39 1.070 5 183.53 1.075 5 196.44 1.060 6 157.47 1.065 6 170.61 1.070 6 183.81 1.075 6 19
34、6.73 1.060 7 157.75 1.065 7 170.84 1.070 7 184.04 1.075 7 197.01 1.060 8 158.03 1.065 8 171.06 1.070 8 184.27 1.075 8 197.30 1.060 9 158.31 1.065 9 171.29 1.070 9 184.49 1.075 9 197.59 1.061 0 158.59 1.066 0 171.57 1.071 0 184.72 1.076 0 197.88 1.061 1 158.87 1.066 1 171.86 1.071 1 184.95 1.076 1 19
35、8.17 1.061 2 159.15 1.066 2 172.14 1.071 2 185.24 1.076 2 198.46 1.061 3 159.43 1.066 3 172.42 1.071 3 185.53 1.076 3 198.75 1.061 4 159.71 1.066 4 172.71 1.071 4 185.81 1.076 4 198.98 1.061 5 159.99 1.066 5 172.99 1.071 5 186.10 1.076 5 199.21 1.061 6 160.22 1.066 6 173.28 1.071 6 186.38 1.076 6 19
36、9.44 1.061 7 160.44 1.066 7 173.56 1.071 7 186.67 1.076 7 199.67 1.061 8 160.67 1.066 8 173.79 1.071 8 186.95 1.076 8 199.90 1.061 9 160.89 1.066 9 174.01 1.071 9 187.24 1.076 9 200.19 1.062 0 161.12 1.067 0 174.24 1.072 0 187.47 1.077 0 200.48 1.062 1 161.43 1.067 1 174.46 1.072 1 187.70 1.077 1 20
37、0.77 1.062 2 161.74 1.067 2 174.69 1.072 2 187.93 1.077 2 201.06 1.062 3 162.04 1.067 3 174.97 1.072 3 188.16 1.077 3 201.29 1.062 4 162.35 1.067 4 175.26 1.072 4 188.39 1.077 4 201.52 1.062 5 162.61 1.067 5 175.54 1.072 5 188.68 1.077 5 201.76 1.062 6 162.87 1.067 6 175.83 1.072 6 188.97 1.077 6 20
38、1.99 1.062 7 163.12 1.067 7 176.11 1.072 7 189.25 1.077 7 202.22 1.062 8 163.38 1.067 8 176.40 1.072 8 189.54 1.077 8 202.51 1.062 9 163.60 1.067 9 176.68 1.072 9 189.77 1.077 9 202.80 1.063 0 163.82 1.068 0 176.96 1.073 0 190.00 1.078 0 203.09 1.063 1 164.05 1.068 1 177.25 1.073 1 190.23 1.078 1 20
39、3.38 1.063 2 164.27 1.068 2 177.53 1.073 2 190.46 1.078 2 203.67 1.063 3 164.49 1.068 3 177.82 1.073 3 190.69 1.078 3 203.96 1.063 4 164.72 1.068 4 178.10 1.073 4 190.98 1.078 4 204.24 1.063 5 164.95 1.068 5 178.33 1.073 5 191.26 1.078 5 204.53 1.063 6 165.17 1.068 6 178.56 1.073 6 191.55 1.078 6 20
40、4.76 1.063 7 165.40 1.068 7 178.78 1.073 7 191.84 1.078 7 205.00 1.063 8 165.63 1.068 8 179.01 1.073 8 192.13 1.078 8 205.23 1.063 9 166.01 1.068 9 179.24 1.073 9 192.42 1.078 9 205.47 1.064 0 166.38 1.069 0 179.53 1.074 0 192.70 1.079 0 205.70 1.064 1 166.76 1.069 1 179.81 1.074 1 192.99 1.079 1 20
41、5.99 1.064 2 166.99 1.069 2 180.10 1.074 2 193.22 1.079 2 206.28 1.064 3 167.21 1.069 3 180.38 1.074 3 193.45 1.079 3 206.57 1.064 4 167.44 1.069 4 180.61 1.074 4 193.67 1.079 4 206.86 1.064 5 167.66 1.069 5 180.84 1.074 5 193.90 1.079 5 207.09 1.064 6 167.89 1.069 6 181.06 1.074 6 194.13 1.079 6 207.32 1.064 7 168.17 1.069 7 181.29 1.074 7 194.42 1.079 7 207.56 1.064 8 168.46 1.069 8 181.52 1.074 8 194.71 1.079 8 207.79 1.064 9 168.74 1.069 9 181.81
