1、August 2011Translation by DIN-Sprachendienst.English price group 6No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 7
2、5.160.20!%CLi“2324170www.din.deDDIN 51603-4Liquid fuels Fuel oils Part 4: Fuel oils R, Minimum requirements,English translation of DIN 51603-4:2011-08Flssige Brennstoffe Heizle Teil 4: Heizle R, Mindestanforderungen,Englische bersetzung von DIN 51603-4:2011-08Combustible liquides Huiles combustibles
3、 Partie 4: Huiles combustibles R, Exigences minimales,Traduction anglaise de DIN 51603-4:2011-08SupersedesDIN 51603-4:1998-04, withdrawn2009-06www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 7 pages08.15 DIN 51603-4:2011-08 2 A comma is
4、 used as the decimal marker. Contents Page Foreword .3 1 Scope .4 1 Normative references .4 3 Terms and definitions 5 4 Designation .5 4.1 Designation of a type R-LS fuel oil conforming to this standard (04-R-LS) .5 4.2 Designation of a type R-TS fuel oil conforming to this standard (04-R-TS) .5 5 S
5、ampling 6 6 Requirements and testing .6 6.1 General requirements 6 6.2 Requirements and methods of test for type R fuel oils 7 DIN 51603-4:2011-08 3 Foreword This document has been prepared by Working Committee NA 062-06-34 AA Anforderungen an Heizle und Schifffahrtsbrennstoffe of the Fachausschuss
6、Minerall und Brennstoffnormung (Standardization of Petroleum, Fuels, Lubricants and Related Products Committee (FAM) of the Normenausschuss Material-prfung (Materials Testing Standards Committee). DIN 51603, Liquid fuels Fuel oils consists of: Part 1: Fuel oils EL, specifications Part 2: Types L, T
7、and M fuel oils; requirements and testing (withdrawn) Part 3: Fuel oil S, Minimum requirements Part 4: Fuel oils R, Minimum requirements Part 5: Fuel oils SA, Minimum requirements Part 6: Fuel oils EL A, Minimum requirements (DIN SPEC, in accordance with the prestandard procedure) Amendments This st
8、andard differs from DIN 51603-4:1998-04, withdrawn in June 2009, as follows: a) Types ZT and C fuel oils have been included in DIN EN 14156:2003-11 and have therefore been deleted from this standard. This standard specifies only type R fuel oil products not included in DIN EN 14156:2003-11; b) the n
9、ormative references to the standards specifying the methods of test used to verify compliance with the requirements have been updated. Previous editions DIN 51603-4: 1992-04, 1998-04 DIN 51603-4:2011-08 4 1 Scope This standard specifies requirements and methods of test for types R-LS and R-TS middle
10、 fuel oils derived from re-refining R. Preheating of such fuel oils may be required for the purposes of transport, storage and combustion. This standard does not apply to marine fuel oils. 2 Normative references The following referenced documents are indispensable for the application of this documen
11、t. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. DIN 32645, Chemical analysis Decision limit, detection limit and determination limit under repeatability conditions Terms, methods, evalu
12、ation DIN 51400-3, Testing of mineral oils and fuels Determination of sulfur content (total sulfur) Part 3: Combusting according to Schniger; Thorin-sulfonazo-III-titration DIN 51408-1, Testing of liquid petroleum hydrocarbons Determination of chlorine content Wickbold combustion method DIN 51408-2,
13、 Testing of mineral oil hydrocarbons Determination of chlorine content Part 2: Microcoulo-metric determination, oxidation method DIN 51551-1, Testing of lubricants and liquid fuels Determination of the carbon residue Part 1: Conradson method DIN 51562-1, Viscometry Measurement of kinematic viscosity
14、 by means of the Ubbelohde viscometer Part 1: Viscometer specification and measurement procedure DIN 51750-1, Sampling of petroleum products General information DIN 51750-2, Sampling of liquid petroleum products DIN 51757, Testing of mineral oils and related materials Determination of density DIN 51
15、777-1, Testing of mineral oil hydrocarbons and solvents Determination of water content according to Karl Fischer Part 1: Direct method DIN 51900-1, Testing of solid and liquid fuels Determination of gross calorific value by the bomb calorimeter and calculation of net calorific value Part 1: Principl
16、es, apparatus, methods DIN 51900-2, Testing of solid and liquid fuels Determination of gross calorific value by the bomb calori-meter and calculation of net calorific value Part 2: Method using isoperibol of static jacket calorimeter DIN 51900-3, Testing of solid and liquid fuels Determination of gr
17、oss calorific value by the bomb calori-meter and calculation of net calorific value Part 3: Method using adiabatic jacket DIN EN 12766-1, Petroleum products and used oils Determination of PCBs and related products Part 1: Separation and determination of selected PCB congeners by gas chromatography (
18、GC) using an electron capture detector (ECD) DIN EN 12766-2, Petroleum products and used oils Determination of PCBs and related products Part 2: Calculation of polychlorinated biphenyl (PCB) content DIN EN 24260, Petroleum products and hydrocarbons Determination of sulfur content Wickbold combustion
19、 method DIN 51603-4:2011-08 5 DIN EN ISO 2719, Determination of flash point Pensky-Martens closed cup method DIN EN ISO 3170, Petroleum liquids Manual sampling DIN EN ISO 3735, Crude petroleum and fuel oils Determination of sediment Extraction method DIN EN ISO 4259, Petroleum products Determination
20、 and application of precision data in relation to methods of test DIN EN ISO 6245, Petroleum products Determination of ash DIN EN ISO 8754, Petroleum products Determination of sulfur content Energy-dispersive X-ray fluorescence spectrometry DIN EN ISO 12185, Crude petroleum and petroleum products De
21、termination of density Oscillating U-tube method DIN EN ISO 12937, Petroleum products Determination of water Coulometric Karl Fischer titration method DIN EN ISO 14596, Petroleum products Determination of sulfur content Wavelength-dispersive X-ray fluorescence spectrometry DIN ISO 3016, Petroleum pr
22、oducts Determination of pour point DIN ISO 3733, Petroleum products and bituminous materials Determination of water Distillation method DIN ISO 15597, Petroleum and related products Determination of chlorine and bromine content Wave-length-dispersive X-ray fluorescence spectrometry 3 Terms and defin
23、itions For the purposes of this standard, the following term and definition apply. 3.1 type R fuel oil liquid fuels derived from processed re-refined mineral oil fractions containing aromatics NOTE Depending on the sulfur content, a distinction is made between type LS and type TS fuel oils. 4 Design
24、ation 4.1 Designation of a type R-LS fuel oil conforming to this standard (04-R-LS): Fuel oil DIN 51603 R-LS 04 4.2 Designation of a type R-TS fuel oil conforming to this standard (04-R-TS): Fuel oil DIN 51603 R-TS 04 DIN 51603-4:2011-08 6 5 Sampling Sampling shall be carried out conforming to DIN E
25、N ISO 3170 or in compliance with the specifications given in DIN 51750-1 and DIN 51750-2, or any other regulations governing sampling. 6 Requirements and testing 6.1 General requirements The pollutant content (in particular arsenic, lead, cadmium, cobalt, nickel and their compounds, expressed as ele
26、ments) of re-refined fuel oils shall not exceed the relevant emission limit values within the meaning of the immission control act. The nitrogen content of re-refined fuel oils is to be indicated by the supplier on request. All methods of test mentioned in this standard include precision data. In ca
27、ses of dispute, the procedures specified in DIN EN ISO 4259 are to be followed to settle the dispute. The results are to be interpreted on the basis of the precision data of the methods of test. DIN 51603-4:2011-08 7 6.2 Requirements and methods of test for type R fuel oils The requirements and meth
28、ods of test for type R fuel oils are specified in Table 1. Table 1 Requirements and methods of test for type R fuel oils Properties Requirements Testing as in Type R-LS fuel oil Type R-TS fuel oil Density at 20 C kg/m3To be specified by the supplier To be specified by the supplier DIN 51757 or DIN E
29、N ISO 12185 Flash point determined by the Pensky-Martens closed cup method C 61 61 DIN EN ISO 2719 Kinematic viscosity DIN 51562-1 at 50 C mm2/s 30 at 70 C Mm2/s 15 30 at 90 C mm2/s 15 Conradson carbon residue % (m/m) 0,5 10 DIN 51551-1 Sulfur content % (m/m) 0,5 1,0 DIN 51400-3 or DIN EN 24260, or
30、DIN EN ISO 8754, or DIN EN ISO 14596 Water content % (m/m) 0,2 0,2 DIN ISO 3733 or DIN 51777-1, or DIN EN ISO 12937 Calorific value, HuMJ/kg 42 42 DIN 51900-1 and DIN 51900-2, or DIN 51900-1 and DIN 51900-3 Ash % (m/m) 0,02 0,05 DIN EN ISO 6245 Sediment % 0,05 0,05 DIN EN ISO 3735 Pour point C To be
31、 specified by the supplier To be specified by the supplier DIN ISO 3016 Total halogen, expressed as chlorine mg/kg 300 300 DIN 51408-1 or DIN 51408-2, or DIN ISO 15597 PCB content (PCB = polychlorinated biphenyls) mg/kg Below the limit of detection Below the limit of detection DIN EN 12766-1 and DIN EN 12766-2
