1、 , () INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION (ISC) 32055 2013 2014 320552013 II , 1.092 . 1.2-2009 . , . , , , 1 - , , ( ) , 4 2 3 , ( 25 2013 . 55-) : ( 3166) 00497 ( 3166) 00497 AM BY KZ KG MD RU TJ UZ - 4 STM D 95-10 Standard test method for water in petroleum product
2、s and bituminous materials by distillation ( ). (en). ASTM, , ASTM, , . 1.5 2001 ( 3.6). . 5 (IDT) 14 2013 . 495- 320552013 1 2014 . 6 320552013 III , . () . , , 2014 , 320552013 _ 1 Petroleum products and bituminous materials. Determination of water content by distillation 2014 07 01 1 1.1 0 % . 25
3、 % . , . , . 1.2 , , 1. . ASTM D 244. . ASTM D 4006 (API MPMS Chapter 10.2). ASTM D 1796 (API MPMS Chapter 10.6). 1.3 , . . 1.4 , . , . 2 . ( )1) : ASTM D 244 Test methods and practices for emulsified asphalts ( ) ASTM D 1796 Test method for water and sediment in fuel oils by the centrifuge method (
4、laboratory procedure) ( ) ASTM D 4006 Test method for water in crude oil by distillation ( ) ASTM D 4057 Practice for manual sampling of petroleum and petroleum products ( ) ASTM D 4177 Practice for automatic sampling of petroleum and petroleum products ( ) ASTM D 5854 Practice for mixing and handli
5、ng of liquid samples of petroleum and petroleum products ( ) ASTM E 123 Specification for apparatus for determination of water by distillation ( ) 1) ASTM ASTM website, www.astm.org ASTM serviceastm.org. ASTM . ASTM Website standards Document Summary. 2) . (API), 220L. St.,NW, Washington, DC 20005=4
6、070, http:/www.api.org. 320552013 2 API MPMS Chapter 8.1 Manual sampling of petroleum and petroleum products (ASTM Practice D 4057) (ASTM D 4057)2) API MPMS Chapter 8.2 Automatic sampling of petroleum and petroleum products (ASTM Practice D4177) (ASTM D 4177) 1) API MPMS Chapter 8.3 Mixing and handl
7、ing of liquid samples of petroleum and petroleum products (ASTM Practice D 5854) (ASTM D 5854)1) API MPMS Chapter 10.2 Determination of water in crude oil by the distillation method (ASTM Test Method D 4006) (ASTM D 4006)1) API MPMS Chapter 10.6 Test method for water and sediment in fuel oils by the
8、 centrifuge method (laboratory procedure) (ASTM Test Method D1796) ( ) (ASTM D 1796)1) 3 : 3.1 (bituminous material): , , . 4 4.1 , . , , . 5 5.1 , , . 5.2 , 0,05 % . 0,1 % . , / . 5.3 . 6 6.1 (. 1). 6.1.1 : 6.1.1.1 ( , ). 6.1.1.2 20 % . 80 % . ( , ). 6.1.1.3 , 5 % 125 C (257 F) 20 % 160 C (320 F),
9、( ) 0,8545 15,56/15,56 C (60/60 F). ( . . ). 1) . (API), 220L. St.,NW, Washington, DC 20005=4070, http:/www.api.org. 320552013 3 1 , , , , , , , , , , , 6.1.2 , 5 % 90 C 100 C (194 F 212 F) 90 % 210 C (410 F). . ( . ). 6.1.3 : 6.1.3.1 - 100 C 120 C (212 F 248 F) ( . ). 6.1.3.2 95 % ( . . ). 6.2 , ,
10、10. 11. 7 7.1 , , . , , . . 1-3. , . , . , . 7.2 . 500, 1000 2000 3. 7.3 . . , , . 7.4 , , ASTM 123. , , , 9. 320552013 4 1 ; 2 ; 3 ; 4 1 320552013 5 1 0,05 3; 2 ; 3 2 2 3 320552013 6 1 ; 2 ; 3 ; 4 15 16 . 3 320552013 7 8 8.1 , . , ASTM D 4057 (PI PS Chapter 8.1) ASTM D 4177 (PI PS Chapter 8.2). 8.2 , . . ( , ). 8.3 ASTM D 5854 (PI PS Chapter 8.3) . ASTM D 5854 (PI PS Chapter 8.3). 9 9.1 ,
