1、 545462011 27 2002 . 184- , 1.02004 . 1 - , , ( ) 4, 2 160 3 29 2011 . 630-4 ATM 566809 . (ASTM D 566809 Standard test methods for rubber from synthetic sources Volatile matter). , - , . , - . - 1.52004 ( 3.5). - , -, 5 , - . - () . , , 2013 , - - II 5454620111 12 13 .24 .25 .26 .27 .28 .29 .310 311
2、 .312 313 414 D .415 416 417 4 () - , - 5 .6III 545462011 Synthetic rubber. Determination of volatile matter mass fraction 201307011 1.1 - : , - .1.2 , - .1.3 , .1.4 -, . , .2 : 532282008 . 1. - . 545542011 . , , 45077 . 7452003 . 2533682 . , - 3026396 ( 239394) . , - . - - - , 1 , , . (), - () . ,
3、 - , , .1 545462011 3 3.1 , .3.2 - .4 4.1 54554. , 30263.4.2 1.4.3 54554.5 5.1 . - . :- 30263;- 25336;- 53228.6 6.1 250 0,1 .6.2 (0,50 c177 0,05) -, (100 c177 5) C. 4 , . - 0,1 . 2 . . 4 6 0,1 , . 2 , - 0,1 .7 7.1 ,%, =(A B)/A 100, (1) , ; , .8 B 8.1 8.1.1 , - . (2).2 545462011 B :- , - (100 c177 5
4、) C, 1 50 ;- 53228;- 25336.9 9.1 (250 c177 5) (0,50 c177 0,05) 50 C.9.2 0,1 - , (100 c177 5) C. -, . . 0,1 . - 1,0 % 1 .10 ,%, =( )/ 100, (2) , ; , .11 C 11.1 11.1.1 , - . (3). :- , - (100 c177 5) C, 1 50 ;- 53228;- 25336;- 450;- ;- 745 100 c180 75 c180 8 . ( 0,0004 ), , - , .12 12.1 (250 c177 5) -
5、0,50 c177 0,05) , , 50 C. .12.2 10 , 25 3, ,- 0,0001 , - (100 c177 5) C. , . 1. , , , -3 545462011 . 30 , 0,01 % - . 1,0 % 1 .13 ,%, =( )/ 100, (3) , ; , . . , - 0,95 % 15 % . .14 D 14.1 14.1.1 , , , . .15 15.1 (250 c177 5) (1,40 c177 0,05) 50 C. .15.2 5 7 0,001 .15.3 , -, (150 c177 10) C (5500 c177 275) 3 .15.4 , 3 . .16 ,%, =( )/ 100, (4) , ; , .17 17.1 2 .4 545462011 () , .1 , , 532282008 MOD 76 (1):2006 . 1. . 545542011 MOD 31822007 ., 45077 * 7452003 * 2533682 MOD 1773:1976 . ()MOD 3819:1985 . MOD 4797:1981 . 3026396 IDT 2393:1994 ., . * . - :- IDT ;- MOD .5 545462011
