KS M 3331-2009 Testing methods for liquid unsaturated polyester resin《不饱和聚酯树脂试验方法》.pdf

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1、 KSKSKSKS KSKSKSK KSKSKS KSKSK KSKS KSK KS KS M 3331 KS M 3331 :2009 2009 12 25 http:/www.kats.go.krKS M 3331:2009 : ( ) ( ) () ()SK () ( ) : (http:/www.standard.go.kr) : :1976 12 22 :2009 12 25 2009-0878 : : ( 02-509-7300) (http:/www.kats.go.kr). 10 5 , . KS M 3331:2009 Testing methods for liquid u

2、nsaturated polyester resin 1. (, 80 , ) ( ) . . 1 1) . , . . KS M ISO 2114, ( ), () KS M ISO 2535, KS M ISO 2554, KS M ISO 3521, KS M ISO 4615, KS M ISO 14848, 130 ISO 584:1982, PlasticsUnsaturated polyester resinsDetermination of reactivity at 80 (conventional method) 2 . . ( ) . KS A 0001, KS A 51

3、03, KS B 5213, KS C 1602, KS C 1610, 1) . KS M 3331:2009 2 KS C 1615, KS L 2302, KS L 2307, KS L 2317, KS M 0001, KS M 8075, (IV)() KS M 8227, (III) (6)() KS M 8241, () KS M 8275, () KS M 8367, () KS M 8380, () KS M ISO 911:2008, 1: 15 16F KS M ISO 912:2008, 2: 20 KS M ISO 472:2001, KS M ISO 6491:20

4、01, KS M ISO 1652:2008, KS M ISO 1675:2008, KS M ISO 2211:2003, ( ) KS M ISO 2554, KS M ISO 2555:2002, , KS M ISO 3007:2003, KS M ISO 3219:2003, , / KS M ISO 3696:2005, KS M ISO 63532, 2:1 KS M ISO 63533 3:2 KS Q 1003, KS Q 5002, 1: ISO 650:1977, Relative density 60/60 degrees F hydrometers for gene

5、ral purpose ISO 10431:1987, PlasticsSymbolsPart 1:Basic polymers and their special characteristics(KS M ISO 10431 ) ISO 2552:1987, Water for analytical laboratory useSpecification and test methods ISO 3675:1993, Crude petroleum and liquid petroleum productsLaboratory determination of density or rela

6、tive densityHydrometer method ISO 4619:1980, Paints and varnishesDriers for paints and varnishes ISO 4630:1997, Binder for paints and varnishesEstimation of colour of clear liquids by the Gardner colour scales JIS K 8681, p- 1 () JIS K 8842, () EN 605842:1993, ThermocouplesPart 2:Tolerances NFT 5750

7、5:1993, PlasticsThermosetting materials based on unsaturated polyester, obtained by cross linkingDetermination of the active oxygen content of an organic peroxide(perester type) for starting the base resin cross linking 3 1 . . KS M 3331:2009 3 1 , 5.1 , 5.2 5.3 5.4 , 5.5 5.6 80 (80 ) 5.7 130 (130 )

8、 5.8 (25 ) 5.9 (25 ) 5.10 5.11 5.12 4 4.1 , 15 35 , (6520) % . . 4.2 KS Q 1003 . 2 . 4.3 KS Q 5002 . 5 5.1 5.1.1 . 23 , kg/m 3 (g/mL). 5.1.2 KS M 3331:2009 4 . a) . . . . b) 1) , KS M ISO 6491 KS B 5213 . . 2) 0.2 . 3) 25 mm . 25 mm . ISO . 5 mm . 4) 0.2 . c) 15 , 20 , 23 25 . . d) 1) , . 2) . 3) .

9、. 2 . 4) . 1/2 . 5) 2 . . . . 6) 1/5 1/10 . . 6.1) (ISO) . 1 . 6.2) . KS M 3331:2009 5 1 (ISO) 7) 2 (ISO) . . (ISO) . . 8) 1/2 . 0.5 0.5 . 2 (ISO) e) . 1) 2) 3) 4) KS , , 5) 6) 7) 5.1.3 a) 23 . . . KS M 3331:2009 6 b) 1) 2 D(mm) V(mL) KS L 2317 ( 3) . 50 mm . 2 V mL D mm 100 131 50 111 3 2) . 3) 0.2

10、 . 4) 0.2 mg . c) 23 , . d) . . (230.2) 1 . . , . . 23 (g) . e) 23 23 (23/23 ) (1) . a 0 1 23 V m m(1) m 1 :23 (g) m 0 :23 (g) a :23 0.001 2 g/mL( ) V :23 (mL) 50 mm KS M 3331:2009 7 23 V . V (2) . 3 966 . 0 0 2 a e 0 2 m m m m V (2) m 2 :23 (g) e :23 0.997 5 g/mL . 25 . a :25 0.001 2 g/mL( ) e :25

11、0.997 0 g/mL 1 KS Q 5002 . f) . 1) 2) 3) 4) KS , , 5) 6) 7) 5.2 , . 5.2.1 . a) (0 500) . b) 1) 23 mm 100 mm 2) . 2) KS M 8075 2.49 g 2.10 g KS M ISO 62533(R55) 2.00 g KS M ISO 62532(R13) 200 mL 2 000 mL . 3 . . 6 . 2) 50 250 mm . 100 mm . 50 mL 100 mL . KS M 3331:2009 8 3 mL mL mL mL 0 0 100 90 18 8

12、2 5 1 99 100 20 80 10 2 98 125 25 75 15 3 97 150 30 70 20 4 96 175 35 65 25 5 95 200 40 60 30 6 94 250 50 50 35 7 93 300 60 40 40 8 92 350 70 30 50 10 90 400 80 20 60 12 88 450 90 10 70 14 86 500 100 0 80 16 84 c) . . 3) . d) . 1) 2) 3) 4) KS , , 5) 6) 5.2.2 . a) (1 18) . b) 1) KS L 2302 (10.650.025

13、) mm, 12.5 mm, 114 mm 2) 3) . . , KS M 3331:2009 9 2.1) 18 . KS M 8075 4 KS M ISO 63532(R13) 0.1 mol/L 1 000 mL . 91 8 . KS M 8227 5 () KS M ISO 63532(R13) 1.2 () . KS M ISO 63533(R55) 1 () 2 %(m/m) 3 () . 2 % 4 . 100 mL . 4 g 2 mL mL 2 %(m/m) mL 1 0.550 2 0.865 3 1.330 4 2.080 5 3.035 6 4.225 7 6.4

14、00 8 7.900 9 3.8 3.0 93.2 10 5.1 3.6 91.3 11 7.5 5.3 87.2 12 10.8 7.6 81.6 13 16.6 10.0 73.4 14 22.2 13.3 64.5 15 29.4 17.6 53.0 16 37.8 22.8 39.4 17 51.3 25.6 23.1 18 100.0 2.2) 5 18 . KS M 3331:2009 10 5 a X Y % ()% 1 0.317 7 0.330 3 80 7 2 0.323 3 0.335 2 79 7 3 0.332 9 0.345 2 76 6 4 0.343 7 0.3

15、64 4 75 5 5 0.355 8 0.384 0 74 4 6 0.376 7 0.406 1 71 4 7 0.404 4 0.435 2 67 4 8 0.420 7 0.449 8 64 4 9 0.434 3 0.464 0 61 4 10 0.450 3 0.476 0 57 4 11 0.484 2 0.481 8 45 4 12 0.507 7 0.463 8 36 5 13 0.539 2 0.445 8 30 6 14 0.564 6 0.427 0 22 6 15 0.585 7 0.408 9 16 2 16 0.604 7 0.392 1 11 1 17 0.62

16、9 0 0.370 1 6 1 18 0.647 7 0.352 1 4 1 a CIE No.15() . c) . . . d) . 1) 2) 3) 4) KS , , 5) 6) 5.3 5.3.1 a) 1 g mg . KOH mg/g . b) KS M 3331:2009 11 c) 5.3.2 a) . . 1 g mg . b) . 20 . . 1 g mg . 5.3.3 a) 0.3% . b) 0.2% . c) 99.8% . d) 0.005% . e) 0.05% . f) 0.01% . g) ISO 3696 3 KS M 0001 . h) KS M I

17、SO 63532(R24) . i) JIS K 8842 . j) KS M 8275 . k) 1) d) 2 b) 1 . 2) 2.1) d) 2 b) 1 . 2.2) d) 7 b) 3 . l) e) 400 mL, f) 750 mL g) 50 mL . m) 1) b) c) 0.1 mol/L 2) h) 7 g g) 5 mL b) 1 L . . 25 mL g) 50 mL 0.1 mol/L KS M ISO 63532(R13) . . n) 1) 0.1 % b) 2) 1 % b) 3) 1) 0.10 g 2) 0.10 g g) 20 mL 0.1 mo

18、l/L m) 2) g) 200 mL . 5.3.4 KS M 3331:2009 12 . a) 250 mL, 100 mL . b) 25 mL, 0.05 mL . c) d) 25 mL, 50 mL, 60 mL . e) 1 mg 0.2 mg . f) 5.3.5 a) 1) 1.1) 2 . 1 0.5 3.0 g . 1.2) 250 mL 1 mg ( m 1 ). 5.3.3 k) 1) 50 mL . . 5 5.3.3 k) 1) 50 mL 25 mL . 1.3) 5.3.3 m) 1) . (V 1 , mL) . . (V 2 , mL) . 2) 2.1) 13 g 5.3.3 k) 2) 2.1) 5 . 20 30 5.3.3 m) 1) . (V 1 , mL) . 5.3.3 k) 2) 2.1) 50 mL 5.3.3 a) 25 mL . () . (V 2 , mL) . 2.2) 13 g 5.3.3 k) 2) 2.2) 10 30 mL 5.3.3 n) 3) 0.1 mol/L 5.3.3 m) 2) . . . b) 1) 1

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