EN 13003-2-1999 en Para-Aramid Fibre Filament Yarns - Part 2 Methods of Test and General Specifications《聚酰胺纤维丝线 第2部分 试验方法和通用规范》.pdf

1、 STD-BSI BS EN 13003-2-ENGL 3777 O 1b2LibbS 0775083 223 W BRITISH STANDARD Para-aramid fibre filament yarns - Part 2: Methods of test and general specifications The European Standard EN 13003-2:1999 has the status of a British Standard ICs 69.100.30 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMIT

2、TED BY COPYRIGHT LAW BS EN 13003-2:1999 STDmBSI BS EN 13003-2-ENGL 1999 I 1b24bb7 0795082 LbT BS EN 13003-2:1999 been prepared under the direction of the Sector Amd. No. Date Committee for Materials and Chemicals, was published under the authority of the Standards Committee and comes into effect on

3、15 September 1999 O BSI 09-1999 ISBN O 580 32559 8 National foreword Comments This British Standard is the English language version of EN 13003-2: 1999. The UK participation in its preparation was entrusted to Technical Committee PRV42, Fibre reinforced thermosetting plastics and prepregs, which has

4、 the responsibility to: - aid enquirem to understand the tex$ - present to the responsible European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; - monitor related international and European developments and promulgate them in the UK. A l

5、ist of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement intdonal or European publications referred to in this document may be found in the BSI Standards Catalogue under the section entided “Intrnational St

6、anda,rds Correspondence Index“, or by using the “Find“ facility of the BSI Sandards Electronic Catalogue. A British Standard does not purport to include ail the necessary provisions of a conh-act Users of British Standards are responsible for their correct application. Compliance with a British Stan

7、dard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, the EN title page, pages 2 to 11 and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued STD-BSI BS

8、 EN 13003-2-ENGL 1999 B LbZVbbS 0795083 OTL EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13003-2 April 1999 ICs 59.100.30 English version Para-aramid fibre filament yarns - Part 2: Methods of test and general specifications Fils en fibre de para-aramide -Partie 2: Methodes dessai et specific

9、ations gnrales Para-Aramidfaser-Filamentgarne - Teil 2: Prifverfahren und allgemeine technische Lie ferbedingungen This European Standard was approved by CEN on 4 March 1999. CEN members are bound to comply with the CENICENELEC Internal Regulations which stipulate the conditions for giving this Euro

10、pean Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standard exists in three official versions (English

11、, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Centrai Secretariat has the same status as the official versions. CEN members are the national standards bodies of Ausia, Belgium, Czech Republic,

12、 Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europeen de Normalisation Europisches Komitee fir Normung Central Secretariat: rue de Stassa

13、rt 36, B-1050 Brussels O 1999 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 13003-2: 1999 E Page 2 EN 13003-21999 Contents Foreword 1 Scope 2 Normative references 3 Definitions 4 Yam characteristics 4.1 Physical properties 4.2 Vi

14、sual properties 4.3 Other properties 4.3.1 Splices 5 Quality inspection 5.1 5.2 Testing at manufacturer 5.3 Certificate 6 Mode of delivery 6.1 Packaging 6.2 Marking of packages 7 Storage Annex A (normative) Para-aramid fibre filament yams: Determination of the differences in length of multiple-wound

15、 yams A. 1 Scope and field of application A.2 Definition A.3 Principle of the method A.4 Apparatus A.5 Sampling . A.6 Procedure A.7 Calculation and expression of results A.8 Testreport Annex B (informative) Certificate of analysis (sample) for para-aramid fibre filament yarns Sampling and criteria f

16、or acceptance 3 4 4 4 5 5 5 5 5 5 6 7 7 7 .7 8 8 8 8 8 8 8 9 9 10 10 11 8 BSI 09- I999 STD=BSI BS EN 13003-2-ENGL 1999 M lb2Vbb9 0775085 777 Page 3 EN 13003-2:1999 Foreword This European Standard has been prepared by Technical Committee CENITC 249, Plastics, the Secretariat of which is held by IBN.

17、This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 1999, and conflicting national standards shall be withdrawn at the latest by October 1999. According to the CEN/CENELEC Internal Regulations

18、, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United

19、Kingdom. EN 13003 consists of the following parts, under the general title Para-aramidJibrefibment yarns: - Part i: Designation - Part 2: Methods of test and general specifications - Fart 3: Technical specifcations 6 BSI 09-1999 Page 4 EN 13003-2:1999 1 Scope This part 2 of EN 13003 applies to high

20、performance para-aramid fibre filament yarns and defines the methods of test which are to be used for the determination of the properties required for the designation and the specifications which are given respectively in parts 1 and 3. This part 2 defines also the general requirements which apply t

21、o the specifications for para-aramid fibre filament yams as listed in part 3 of the present standard. 2 Normative references This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriate places in the te

22、xt and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication referred to appli

23、es. prEN 12562, Textiles - Para-aramid multifiament yarns - Methods of test. EN 13003-1, Para-aramidjbrefdament yarns - Part I: Designation. EN 13003-3, Para-aramidjbrejlament yarns - Part 3: Technical specifications. EN IS0 1886, Reinforcementfibres - Samplingplans applicable to received batches (I

24、S0 1886: 1990). EN IS0 1889, Reinforcement yarns -Determination ofthe linear density (IS0 1889: 1997). EN IS0 1890, Reinforcement yarns - Determination of twist (IS0 1890: 1997). EN IS0 2062, Textiles - Yarns from packages -Determination of single-end breaking force and elongation at break (IS0 2062

25、: 1993). EN IS0 3344, Reinforcement yarns - Determination of moisture content (IS0 3344: 1997). EN IS0 10548, Carbonfibre - Determination of size content (IS0 10548: 1994). IS0 472, Plastics - Vocabulary. IS0 2859-1, Sampling procedures for inspection by attributes -Part i: Sampling plans indexed by

26、 acceptable quality levels (AQL) for lot-by-lot inspection. IS0 101 19, Carbon$bre - Determination of density. prEN IS0 106 18, Carbonjbre -Determination of tensile properties of resin-impregnated yams (ISODIS 106 18: 1994). 3 Definitions For the purpose of this European Standard, the following defi

27、nitions apply. 3.1 qualification testing evaluation of one or several successive lots of given product to demonstrate that the product meets the requirements of the applicable specification 3.2 acceptance testing evaluation of a received lot of a given product to demonstrate that the lot fulfils the

28、 requirements of the applicable specification 8 BSI 09-1999 Page 5 EN 13003-2:1999 1 No. 1 2 3 4 4 Yarn characteristics Properties Units Test methods Density gcm3 IS0 10119 Linear density dtex EN IS0 1889 Finish content (quantitative) % EN IS0 10548 Twist - EN IS0 1890 4.1 Physical properties Testin

29、g of tensile yam specimens prepared in accordance with EN IS0 2062 and prEN 12562a or prEN IS0 106 1 8b 6 Tensile srength MPa aorb 7 Tensile modulus MPa aorb 8 Elongation at break % aorb EN IS0 2062 and prEN 12562 measured on un-impregnated yarns. I DrEN IS0 I 061 8 measured on imurcmtcd mms. The ph

30、ysical properties of the para-aramid fibre filament yams shall be determined in accordance with the relevant EN material standards which are listed in Table 1 below. Table 1 -Tests 15 I Moisture content 1% I EN IS0 3344 I For assembled aramid fibre filament yams the determination of the differences

31、in length of the individual yarns shall be determined according to the method described in annex A of this standard. 4.2 Visual properties The para-aramid fibre filament yarns shall be free from oil, grease and other contaminants as well as from partial tow breakage and fluffy debris on the surface

32、of or within the bobbin, which are incompatible with required processing conditions. 4.3 Other properties Spikes Distinction shall be made between blown splices and bonded splices. Type and number shall be agreed between the yam manufacturer and the customer. 5 Quality inspection The tests to be per

33、formed on a lot (or batch) of para-aramid fibre filament yarn will be different depending whether they are for a reception lot or a production lot. One production lot is obtained by a fabrication campaign of limited duration in time on basis, for example, on the basis of one given amount of raw mate

34、rial. One reception lot, as received by a customer can be made from one part or the whole of one production lot. It may also originate from several production lots. (See also EN IS0 1886: Definitions.) O BSI 09-1999 STD-BSI BS EN L3003-2-ENGL 1999 II lb24bb9 0795088 b88 Page 6 EN 13003-2:1999 5.1 Sa

35、mpiing and criteria for acceptance In the context of this standard, the sampling method by ATTRIBUTES is proposed, though it is also possible to use sampling by variables. The evaluation of a lot of para-aramid fibre filament yarn is based on the sampling that is described in the standard EN IS0 188

36、6 or IS0 2859-1 and on the acceptance quality level (AQL) of 13 % for the physical properties and 2,5 % for the visual properties. Depending on the circumstances, the control for the evaluation of a lot, may be either with a “normal” inspection level (for the qualification of a product or in the cas

37、e of problems), or with a “reduced” inspection level, when a minimum of three successive controls have given an acceptable result. Tables 2 and 3 show the procedure for inspection by attributes with the normal test plan (Table 2) and the reduced test plan (Table 3). Table 2 - Test plan - normal insp

38、ection ncc. IS0 2859-1 (Level II) 8 BS109- I999 STD-BSI BS EN 13003-2-ENGL 1777 E 1b24bb9 0775087 5/11 Page 7 EN 13003-2:1999 Table 3 - Test plan - reduced inspection acc. IS0 2859-1 (Level II) A: Batch is acceptable if the number of non-caiforming units is equal to or less than the number given. B:

39、 Batch is unacccptabic if the number of nonconforming units is equal to or greater than the number given. NOTE For batches or more than IO o00 elementary units. sampling shall be- the subject of an agreement between the yam manufacturer and lhe customer. 5.2 Ttsing at manufacturer The manufacturer s

40、hall ensure that the shipped product meets a given specification. Therefore he has to define a quality control system which will generally include process control (SPC) and testing of final and semi products with adequate test frequency. On the basis of the knowledge of the process and implementatio

41、n of SPC, possibly combined with the use of automated production equipment, the testing at the manufacturer will generally be done using a reduced sampling compared with that used for the reception of lots, with a trend toward testing of process variables in 5.3 Certificate The supplier may at the r

42、equest of the customer issue a certificate for any shipment. This can be: - a certificate of conformance, which is a document confuming that the material has been controlled and meets the requirements of the specification; - a certificate of analysis, which, besides the statement above also includes

43、 the test result on the applicable material; - a draft of a certificate of analysis is given in annex B of this standard. 6 Mode of delivery 6.1 Packaging Unless otherwise explicitly specified, the para-aramid fibre filament yarns shall be shipped in boxes, adequately supported and protected to prev

44、ent damage during normal transit and storage. O BSI 09-1999 Page 8 EN 13003-2:1999 6.2 Marking of packages Para-aramid fibre filament yams shall be marked in a clearly visible and legible way on each bobbin and on the exterior package with the following information: - on each bobbin: trade designati

45、on; - on the packed unit: - trade designation; - net weight; - name of manufacturer; - manufacturers production and traceability reference, including the lot No. 7 Storage Para-aramid fibre filament yams in their original packaging shall be stored in dry locations at a storage temperature of 23 OC f

46、 5 OC and a relative humidity of 60 % r.h. f 5 % r.h Under these storage conditions the shelf life of the para-aramid fibre filament yarns will be a minimum of 3 years, counted from the production date. The advice of the manufacturer should be sought on the expected shelf life under other storage co

47、nditions. Annex A (normative) Para-aramid fibre filament yarns: Determination of the differences in length of multiple-wound yarns A.l Scope and field of application This test method specifies a procedure for the determination of the differences in length of individual yams in multiple-wound aramid

48、fibre filament yams. A.2 Denition The difference in length is evaluated on the basis of the difference in sagging (a on Figure A. 1) between the maximum and minimum sag of the individual aramid fibre filament yams. This difference in sagging is measured and expressed in mm. This property can also be

49、 identified by the term: “catenary”. A3 Prlncfple of the method 15 m of yam taken from the bobbin under test are arranged horizontally and stressed to 12,7 mN/tex at one end. The differences in yam length are given by the difference between the maximum sag of the individual aramid fibre filament yarns. A.4 Apparatus The test apparatus consists of the following parts to be arranged as shown in Figure A. 1 : - two stands, approx. 1 200 mm high. A rubber-faced clamp is fixed to one stand and a pulley attached to the other; - movable rubbergaced clamp, capable o