EN 1895-2001 en Adhesives for Paper and Board Packaging and Disposable Sanitary Products - 180 Degrees - T Peel Test for a Flexible-to-Flexible Assembly (Incorporating corrigendu.pdf

1、BRITISH STANDARD BS EN 1895:2001 Incorporating corrigendum no. 1 Adhesives for paper and board, packaging and disposable sanitary products 180 -T peel test for a flexible-to-flexible assembly The European Standard EN 1895:2001 has the status of a British Standard ICS 83.180 BS EN 1895:2001 This Brit

2、ish Standard was published under the authority of the Standards Policy and Strategy Committee on 22 March 2002 BSI 2007 ISBN 978 0 580 59409 0 National foreword This British Standard is the UK implementation of EN 1895:2001, incorporating corrigendum June 2007. The start and finish of text introduce

3、d or altered by corrigendum is indicated in the text by tags . Text altered by CEN corrigendum June 2007 is indicated in the text by . The UK participation in its preparation was entrusted to Technical Committee PRI/52, Adhesives. A list of organizations represented on this committee can be obtained

4、 on request to its secretary. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publication Amd. No. Dat

5、e Comments 17265 Corrigendum No. 1 31 August 2007 See national forewordEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM EN1895 October2001 ICS83.180 Englishversion Adhesivesforpaperandboard,packaginganddisposable sanitaryproducts180”T”peeltestforaflexibletoflexible assembly Adhsifspourpapieretcarton,e

6、mballageetproduits sanitairesjetablesEssaidepelageen“T”180pourun assemblageflexiblesurflexible KlebstoffefrPapier,VerpackungundHygieneprodukte 180”T”Schlprfungfrflexibel/flexibelgeklebteProben ThisEuropeanStandardwasapprovedbyCENon30September2001. CENmembersareboundtocomplywiththeCEN/CENELECInternal

7、RegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember. ThisEuropeanStandardexistsinthreeofficialve

8、rsions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheManagementCentrehasthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,CzechRepublic,Denmark,Finland,France,German

9、y,Greece, Iceland,Ireland,Italy,Luxembourg,Netherlands,Norway,Portugal,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2001CEN Allrightsofexploitationinanyformandbyany

10、meansreserved worldwideforCENnationalMembers. Ref.No.EN1895:2001E IncorporatingcorrigendumJune2007EN1895:2001(E) 2 Contents page Foreword3 Introduction .4 1 Scope 4 2 Normativereferences 4 3 Termsanddefinitions . 4 4 Principle5 5 Safety5 6 Apparatusandmaterial .5 7 Testspecimens 5 8 Conditioningandt

11、estatmosphere 8 9 Procedure.8 10 Expressionofresults 8 11 Testreport 9EN1895:2001(E) 3 Foreword ThisEuropeanStandardhasbeenpreparedbyTechnicalCommitteeCEN/TC193“Adhesives“,thesecretariatof whichisheldbyAENOR. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationofanidentic

12、altextor byendorsement,atthelatestbyApril2002,andconflictingnationalstandardsshallbewithdrawnatthelatestby April2002. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsofthefollowing countriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,CzechRepublic,Denmark,Fi

13、nland, France,Germany,Greece,Iceland,Ireland,Italy,Luxembourg,Netherlands,Norway,Portugal,Spain,Sweden, SwitzerlandandtheUnitedKingdom.EN1895:2001(E) 4 Introduction Peeltestingforadhesivebondsiswidelyusedforassessingtheperformanceofadhesivesand,becauseofthe widediversityoftheflexibilityofsubstratesw

14、hichcanbeused,nosinglepeeltestwillfulfiltherequirementsofall cases. ThisEuropeanStandardisintendedtotestanassemblyconsistingoftwoflexibleadherends. “T”peeltestcanalsobemadeincompliancewith EN285101,AdhesivesPeeltestforaflexiblebondedtorigidtestspecimenassemblyPart1:90peel(ISO 85101:1990). EN285102,A

15、dhesivesPeeltestforaflexiblebondedtorigidtestspecimenassemblyPart1:180peel(ISO 85102:1990). 1 Scope ThisEuropeanstandardspecifiesa180“T“peeltestforthedetermination,underspecifiedconditions,ofthe peelresistanceofabondedassemblyoftwoflexibleadherendswhichmayhaveanequalordifferentflexural modulus. 2 No

16、rmativereferences ThisEuropeanStandardincorporatesbydatedorundatedreference,provisionsfromotherpublications.These normativereferencesarecitedattheappropriateplacesinthetext,andthepublicationsarelistedhereafter.For datedreferences,subsequentamendmentstoorrevisionsofanyofthesepublicationsapplytothisEu

17、ropean Standardonlywhenincorporatedinitbyamendmentorrevision.Forundatedreferencesthelatesteditionofthe publicationreferredtoapplies(includingamendments). EN923 AdhesivesTermsanddefinitions. ENISO15605 EN1067 AdhesivesExaminationandpreparationofsamplesfortesting. ENISO10365 AdhesivesDesignationofmain

18、failurepatterns(ISO 10365:1992). ISO554 Standardatmospheresforconditioningand/ortesting Specifications. 3 Termsanddefinitions ForthepurposesofthisEuropeanStandard,thetermsanddefinitionsgiveninEN923andthefollowingapply. 3.1 peelforce forcerequiredtoseparateprogressivelythetwopartsofabondedtestspecime

19、nofspecifieddimensionsoverthe adherendsurfacesunderthespecifiedconditionsoftestexpressedinnewtons AdhesivesSampling(ISO15605:2000). EN1895:2001(E) 5 3.2 peelstrength forceperunitswidthnecessarytobringanadhesivejointtothepointoffailureortomaintainarateoffailureby meansofastressappliedinthepeelingmode

20、 NOTE thepeelstrengthcanbeexpressedasforceperunitpeelwidth. EN923:1998,2.7.16 4P r i n c i p l e Adherendsareseparatedatacontrolledratefromanopenedgeofapreparedbondlinesothattheseparation occursprogressivelyalongthebondline. Forthe“T“peeltestforaflexibletoflexibleassembly,theforceisappliedtotheunbon

21、dedendsofthetest specimen. Theangleofthebondlinetothedirectionoftheappliedforceisuncontrolled. 5 Safety Personsusingthisstandardshallbefamiliarwithnormallaboratorypractice. Thisstandarddoesnotpurporttoaddressallsafetyproblems,ifany,associatedwithitsuse. Itistheresponsibilityoftheusertoestablishsafet

22、yandhealthpracticesandtoensurecompliancewithany Europeanandnationalregulatoryconditions. 6 Apparatusandmaterial 6.1 Tensiletestingmachine, capableofsupplyingatensileforcewithaconstantrateofgripseparation.The machineshallbeequippedwithaforcemeasuringsystemcompletewithanindicatorand/orarecorder. Thein

23、dicatedforceshallnotdifferfromthetrueappliedforcebymorethan2%.Theresponsetimeofthemachine shallbeshortenoughnottoaffecttheaccuracywithwhichtheforceappliedatthetimeofrupturecanbe measured. Theforceofruptureofthespecimenshalllieintherangebetween20%and80%ofthefullscalereading. 7 Testspecimens 7.1 Sampl

24、ing 7.2Adherends NOTE Thethickness,theflexibilityandothersurfacecharacteristicsoftheadherendshaveanimpactonthepeelstrength value. Theadherendsshalleachbeofuniformthickness,preferablynotmorethan3mm. 7.3Preparationoftestspecimens Testspecimensshouldbecapableofwithstandingtheexpectedtensileforceandshou

25、ldbecapableofbeingbent throughthepeelinganglewithoutgrossirreversibledimensionalchange. testinginaccordancewithEN1067. Takeasampleoftheadhesivetobetestedinaccordancewith ENISO15605 . Examineandprepareitfor EN1895:2001(E) 6 Applytheadhesivesfollowingthemethodrecommendedbytheadhesivemanufacturer. Thea

26、pplicationtemperatureoftheadhesiveandthepressureusedtocombinetheadherendsshallbespecifiedin thetestreport. Thecoatingprocedure,thecoatingmassoftheadhesiveandthebondingconditionsshouldcomplywiththe manufacturerrecommendationsandshallbereported. Unlessotherwisespecified,25mmwidthtestspecimens,arecutfr

27、omthebondedadherends. Thechoiceofthetypeofbond:fullcoating(lamination)orbead/lineapplicationdependsonthenatureofthe adherends(e.g.softness,flexibility),onthetypeofadhesiveandonthefinalapplication(e.g.ifsubstratesfailure isexpected,bead/linebondingcanbeused,ifcohesivefailureisexpectedfullcoatingisrec

28、ommended). Dimensionsinmillimetres Key 1 Flexibleadherend 2 Adhesive 3 Testpanel 4Bonded 5 Testpiece 6Unbonded 7 Directionofpull Figure1FullcoatingEN1895:2001(E) 7 Dimensionsinmillimetres Key 1 Testpanel 2 Directionofpull 3Bonded 4 Testpiece Thistestisappropriateforhotmeltadhesives Figure2Beadline I

29、fapressisusedtomakethetestspecimens,itshallbecapableofapplyinganevenpressureovertheentire bondedareaandshouldpreferablybefittedwithatimereleasemechanism.Inordertogiveauniformdistribution ofpressureoverthebondedareatheplatensofthepressshallbeparallel.Wherethisisimpracticable,oneplaten shallbecoveredw

30、itharesilientpad. Thepreparationprocedureshallbesuchastominimizevariationsandtheuseofapneumaticorhydraulicpress, handorpoweroperated,whichcanapplyapressureupto1N/mm 2 ,isrecommended. 7.4Numberoftestspecimens Thenumberoftestspecimensshallberecordedinthetestreportandshallnotbelessthanfive.EN1895:2001(

31、E) 8 8 Conditioningandtestatmosphere Adherendsshallbeprepared,storedandbondedandtheassembliesconditionedandtestedinastandard atmosphere(23/50)accordingtoISO554unlessotherwisespecified. Theminimumconditioningtimeshallbe2h. 9 Procedure Bendbacktheunbondedportionsoftheadherendsandclamptheminthegrips,ta

32、kingcarethatthetestspecimen isaccuratelyaligned,sothatthetensionappliedisdistributeduniformlyacrossitswidth. Unlessotherwisespecified,setthetensiletestingmachine(6.1)inmotionatarateofgripseparationof(30010) mm/min(orotherspecifiedspeeds). Type1:continuethetestuntilatleast125mmofthebondedlengthissepa

33、rated(seeFigures1and3). Type2:Thetestisfinishedwhentheadherendsarecompletelyseparated(seeFigures2and4). NotethetypeoffailureaccordingtoENISO10365. 10 Expressionofresults Type1:taketheaverageforceasthepeelingforce(seeFigure3). Key 1 Forceinnewtons(N) 2 Peelinglengthinmillimetres(mm) 3 Estimatedaverag

34、evalueforpeelingforce Figure3 NOTEPeelstrengthfortestspecimenstype1andtype2aredifferentevenforthesameadhesive,duetothegeometric differencesandthemethodofevaluation. Type2:Recordthemaximumforce(seeFigure4).EN1895:2001(E) 9 Key 1Forceinnewton(N) 2Peelinglengthinmillimetres(mm) Figure4 Peelstrengthisth

35、earithmeticmeanofallthetestspecimens. Calculatethearithmeticmeanoftheaveragepeelingforcesforalltestspecimens. 11 Testreport Thereportshallstatethefollowing: a) areferencetothisEuropeanStandard; b) adesignationoftheadhesive,givingallinformationrequiredforthecompleteidentificationofthesample; c) adesc

36、riptionoftheadherendsincludingmaterialthicknessandsurfacepreparation; d) adescriptionofthebondingprocess,includingthemethodofapplicationoftheadhesive,dryingor precuringconditions(whereapplicable)andcuringtime,temperatureandpressure; e) theaverageofdrycoatingweightorthickness(aspreciselyaspossible)of

37、theadhesivelayerafter formationofthebond; f) acompletedescriptionofthetestpiece(type1ortype2),includingdimensions,andthenumberoftest specimens; g) theconditioningprocedurepriortotestingandthetestatmosphere; h) therateofseparationofthegrips; i) themethodofdeterminingtheaveragepeelforce(manualorautoma

38、tic); j) Thepeelforceinnewtonsforeachpieceandtheaveragepeelforceinnewtonaswellasthepeelstrength in newtonper millimetreofspecimenwidth ; k) thetypeoffailureforeachtestspecimen; l) Dateoftesting. BS EN 1895:2001 BSI 389 Chiswick High Road London W4 4AL BSI British Standards Institution BSI is the ind

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