FORD FLTM BO 131-03-2014 INTERIOR ODOR TEST.pdf

1、 FORD LABORATORY TEST METHOD BO 131-03 Date Action Revisions Rev. 6 2014 04 10 Revised See summary of revisions, added 80 C for China only D. Stark, NA 2013 10 25 Editorial See summary of revisions D. Stark, NA 2007 06 07 Activated J.Williams FOE Controlled document at www.MATS Copyright 2014, Ford

2、Global Technologies, LLC Page 1 of 7 INTERIOR ODOR TEST Application This test method is used to determine the odor originating from interior trim materials/components/assemblies in the passenger or luggage compartment or from parts or ducting that convey air into the passenger compartment as dictate

3、d by the Material and/or Performance Specifications. Customer Clinics have indicated that the customer expects a new vehicle to have a neutral or new car smell. This test is designed to establish whether parts and materials used in a vehicle have an inappropriate or disturbing odor. Apparatus and Ma

4、terials Required Mechanical Convection Ovens Capable of maintaining the specified test temperatures. 3-Litre Odorless Preserving Jar with Lid Dimensions of jar: approximately 250 mm high x 125 mm diameter; neck 100 mm diameter. The jar and any seals it may employ must be odorless. A suitable odorles

5、s material for the jar seals is polyethylene closed cell foam, 3 mm thick of 45 kg/m3 density. Suitable suppliers for jars of this type are: O French Flint and Ormco Ltd. Item Number: 13433248 Product Name/Code: Kiln3000 Suitable supplier of material for making jar seals is: RS Components Ltd UFP

6、Technologies http:/uk.rs- Stock Number: 733 6696 Stock Number: LD45 Plastazote Stainless Steel Wire Ring/Support Frame The above material is available from any reputable laboratory equipment supply house. Distilled or Deionized Water 20 micro ohms/cm at 25 C maximum conductivity (ASTM D1125). Sampl

7、e Preparation The area or weight and number of samples is determined using Table 1 below. The choice of variants A, B, C or D is based upon the area or weight content of each material used in the vehicle interior. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Technologies, LLC Pa

8、ge 2 of 7 TABLE 1 Variant Application Specimen Weight/Size* A Clips, plugs, covers, foils and other small parts Sum of total, similar parts. Equal to or greater than 100 g or 100 cm2 B Armrests, ashtrays, door handles, shift lever gaiters, sun visors, steering wheels, door/window seals and other med

9、ium size parts 1 each of 90 x 200 mm. If the component is less than 90 x 200 mm, test the actual part, i.e. door handles. For steering wheels, door/window seals or similar parts cut the component into a 200 mm length size C Seat Trim/roof covers, sound-deadeners, foils, foam materials, carpets, duct

10、ing and other large surface materials 3 each of 90 x 200 mm (in same jar) D* Sealers, adhesives, liquid applied sound deadeners and antiflutter mastics Panel dimensions: 200 x 100 x 0.8 mm Substrate: -Paint shop applied materials-HDG with EC -Body shop applied materials-HDG substrate (cleaned and de

11、greased) Materials dimensions: -Paint shop sealer-150 x 85 x 1 mm bead* -Body Shop sealer -100 x 6 mm bead* Curing conditions: FLTM BV 150-05 at minimum, nominal and maximum Age sample for 14-28 days after manufacture at room temperature prior to bagging to allow for curing * Do not test components

12、less than 100 g or 100 cm2. *Unless otherwise noted in the material specification. Note: For material testing, select variant per intended part application. For materials used in several applications, test to the largest application variant. If the material thickness of a homogeneous material is mor

13、e than 20 mm, then the sample is to be prepared for a 20 mm thickness. Sandwich materials must be tested in their compound state. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Technologies, LLC Page 3 of 7 Conditioning of Materials and Test Conditions All test values indicated he

14、rein are based on material conditioned in a controlled atmosphere of 23 2 C and 50 5% relative humidity, for not less than 24 hours prior to testing, and tested under the same conditions unless otherwise specified. All parts or samples should be wrapped/bagged 14 - 28 days after part manufacture wit

15、h one of the following: heat sealed polyethylene (PE) bags, clean plastic wrap foil (PE or PP), PE coated aluminum bags or aluminum foil. Parts that are only to be used in the China market and regionally sourced should be wrapped/bagged 7-14 days after part manufacture. Parts for testing must be lab

16、eled with the following information: supplier, date of manufacture, part number, part name, plant and location, and shipping date. Procedure 1. Clean the jars, lids (using laboratory washing machines) and seals (hand or machine wash) before each use. They must be clean and odorless. 2. A blank test

17、jar may be employed, as a control, to ensure that the jars are odorless and the water quality does not create an odor. 3. The jars containing the specimen(s) (or blank) should be conditioned and assessed per Table 2 below. TABLE 2: Summary of Test Conditions Use a separate specimen and jar for each

18、condition. Condition Temperature Test Time 1 23 2 C 24 h 1 h 2 40 2 C 24 h 1 h 3 65 2 C 2 h 10 min 4 (China Only)* 80 2 C 2 h 10 min *Applies to parts that are for the China market and regionally sourced only. Condition 1: Add 50 5 ml of distilled or deionized water to the jar(s). Take a stainless s

19、teel wire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). The specimens are to be placed in the jar(s) in such a way to prevent direct contact with the water and to avoid wetting the specimen(s). Close the jar(s) and allow the specimen(s) to condition for 24 h 1 hr a

20、t 23 2 C. Immediately evaluate the odor. Condition 2: Pre-heat an oven to 40 2 C. Add 50 5 ml of distilled or deionized water to the jar(s). Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). The specimen(s) are to be placed in the jar(s) in

21、such a way to prevent direct contact with the water and to avoid wetting the specimen(s). FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Technologies, LLC Page 4 of 7 Close the jar(s) and place in the pre-heated oven for 24 h 1 hr at 40 2 C. Remove jar(s) from the pre-heated oven

22、and immediately evaluate the odor. Return the jar(s) to the pre-heated oven at 40 2 C for 15 2 minutes between odor assessments. Condition 3: Pre-heat oven to 65 2 C. Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested in the jar(s). Close the jar(s) and pla

23、ce in the pre-heated oven for 2 h 10 min at 65 2 C. Remove the jar(s) from the pre-heated oven and immediately evaluate the odor. Three assessors (maximum) are permitted to evaluate the odor at one time. One minute, maximum total time, is allowed for the three assessors to evaluate the odor prior to

24、 returning the jars to the pre-heated 65 2 C oven*. Return the jar(s) to the pre-heated oven at 65 2 C for 15 mintues (minimum) between odor assessments. Condition 4 for CHINA ONLY: Pre-heat oven to 80 2 C. Take a stainless steel wire ring or support and suspend or stand the specimen(s) to be tested

25、 in the jar(s). Close the jar(s) and place in the pre-heated oven for 2 h 10 min at 80 2 C. Remove the jar(s) from the 80 2 C pre-heated oven then transfer the jar(s) to a second pre-heated oven at 65 2 C for 15 minutes (minimum). Remove the jar(s) from the 65 2 C pre-heated oven and immediately eva

26、luate the odor. Three assessors (maximum) are permitted to evaluate the odor at one time. One minute, maximum total, is allowed for the three assessors to evaluate the odor prior to returning the jars to the pre-heated 80 2 C oven*. Between odor assessments return the jars to the 80 2 C pre-heated o

27、ven for 30 5minutes. Then place the jar(s) in the 65 2 C pre-heated oven for 15 minutes (minimum) prior to the evaluation. * No more than three assessors are allowed per group. 4. Evaluating the Odor: The assessors should be selected from staff who do not work in the production facility. Heavy smoke

28、rs, users of strong perfumes, or people with sinus problems are not suitable. All assessors must be aware of any risk assessment documents and Toxicology reports of all submitted components, which should be readily available, if requested. Acceptance tests shall be made by a minimum of five assessor

29、s. If the rating of individual tests differs by more than two points, three additional assessors shall be used to retest the sample. The test must be conducted in an environment free from drafts and contaminant odors. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Technologies, LL

30、C Page 5 of 7 The lid should be removed and the assessors nose should be positioned about 5 cm over the edge of the jar. The air from the jar should be wafted towards the assessors nose. The assessor should slowly inhale through the nose. The lid should not be off the jar longer than 5 seconds. Reco

31、rd the appropriate rating (refer to “Rating Scale“). If the assessor gives a rating which would be classed as a failure, a description of the odor must be included in the report. The person conducting the Odor Test should not allow the assessors to view any previous ratings or comments in any way. 5

32、. Repeat Step 4 for each assessor and each sample. 6. The odor rating is indicated by the arithmetic mean of all the assessors individual ratings, the value being rounded up to the nearest half point. To ensure that odor differentiation can be established by the assessors, all conditions being teste

33、d shall be conducted in the same time frame. For all the variants and conditions, the odor evaluation uses the rating of 1 to 6, with half-point ratings, as follows: Rating Scale Rating 1 not perceptible Rating 1.5 slightly perceptible Rating 2 perceptible, not disturbing Rating 2.5 clearly percepti

34、ble but not disturbing Rating 3 very perceptible but not disturbing Rating 3.5 intense enough to be slightly disturbing Rating 4 disturbing Rating 4.5 intense and disturbing Rating 5 strongly disturbing Rating 5.5 very intense, disturbing Rating 6 extremely disturbing The definition of a disturbing

35、odor is one that would be considered inappropriate for a new car smell. The smell of a component/ material is defined as disturbing, not when it is more concentrated, but rather when it transitions from one acceptable odor to another unacceptable odor upon conditioning. The concentrated odor of hot

36、plastic, hot rubber, hot leather, etc. would not qualify as a disturbing odor. A disturbing odor or inappropriate smell is also one that is identifiable as smells that are not normally associated with the interior of a new car, (i.e. sour milk, fish, perfume, burnt, musky, asphalt, rotten meat). The

37、 assessors should be encouraged to use the half point ratings to improve differentiation between samples. 7. The test report shall include: A reference to this standard. All necessary details for identifying the test samples. Material variant classification (A, B, C or D) from Table 1. Test conditio

38、n(s) (1, 2, 3, and/or 4) from Table 2. Identification of assessor by name or number. Individual and average odor rating. Samples defined as unacceptable should include an odor description. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Technologies, LLC Page 6 of 7 Special charact

39、eristics of the test samples and their condition. Date of manufacture of the samples and the date of the test. Example of the test result designation: Designation Test Method Test Variant Test Condition Rating Odor Test FLTM BO131-03 B 2 3 average (2, 2.5, 2.5, 3, 3, 3) Odor Test FLTM BO131-03 C 3 4

40、 average (3, 3, 4, 4, 5) Fish like smell Chemicals, materials, parts, and equipment referenced in this document must be used and handled properly. Each party is responsible for determining proper use and handling in its facilities. FORD LABORATORY TEST METHOD BO 131-03 Copyright 2014, Ford Global Te

41、chnologies, LLC Page 7 of 7 Summary of Revisions 2014/04/10 Added Condition 4 for the China market only. Condition 4 will be re-evaluated in 6 - 12 months Added 7-14 day conditioning period for the China market only. Updated equipment supplier information Added test size note for Variant A Changed n

42、umber of assessors from 3-5 to a minimum of five, changed assessment to be a mean instead of average Add descriptions for the half point scale Editorial changes for clarification 2013/10/25 Editorial Corrected odor average for first odor example 2013/04/15 Modified the test temperature for Condition

43、 3 from 80 C to 65 C 2012/05/01 Added North America source for jar seal 2011/12/22 Updated application paragraph Variant A allowed usage of actual part if less than 30 g Deleted statement that if part size is weights less than 30 g multiple parts should be tested together to achieve 30 g minimum. Ad

44、ded option to use blank jar as a reference Added optional pre-heating for condition 3 Modified Evaluating the Odor section Added definition of a disturbing odor and examples Modified test report out section Added an example of a failed Test Result Designation 5/27/2011 Modified sample bagging materi

45、al and when the component should be bagged Re-formatted testing procedure Added individual rating to be reported in the test report Modified size of Variant B from weight to area Clarified Condition 3 6/11/2010 Added variant D for sealers and adhesives Modified condition 3 method of reaching temperature Removed odor rating acceptance