GOST 32015-2012 Food products feeds food raw materials Method of determination of anabolic steroids and stylben derivatives by gas chromatography using mass spectrometry《食品 饲料 食品原料.pdf

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6、 , 19,552-9)*;- (), . .;- 13647;- N,N- () (Sigma, , T-5634)*;- () (Sigma, T-4252)*;- , . .;- (Aldrich, , 22,690-4)*;- -, . .;- 24363, . .;- - 6995;- , . .;- , . .;- , . .;- 2603, . .;- C18 40 (Varian, , 12213012)*;- Helix pomatia (Merck, , 1.04114)*;- 4166, . .;- , . . ;- ()-, . . 2 . . 3 . . . 1386

7、7.4.3 :- -d6 99,0 % (RIKILT*, BRS 01)*;- -d2 99,0 % (RIKILT, BRS 02)*;- -d4 98,0 % (RIKILT, BRS 03)*;- -d3 98,0 % (RIKILT, BRS 04)*;- -d3 98,0 % (RIKILT, BRS 05)*;-17c98-d3 98,0 % (RIKILT, BRS 54)*;-17c98-d2 98,0 % (RIKILT, BRS 55);-17c97- 99,0 % (RIKILT, BRS 56)*;-17c97- 99,0 % (RIKILT, BRS 57)*;*

8、. .* , .3 320152012-17c98- 99,0 % (RIKILT, BRS 58)*;-17c98-d2 99,0 % (RIKILT, BRS 59)*;-17c98-d3 99,0 % (RIKILT, BRS 72)*;- 17- 98,0 % (Acros, 225730050)*-17c97- 98,0 % (Sigma, E-4876)*- c98- 98,0 % (Sigma, E-8875)*;-17c98- 99,0 % (Acros, 164410050)*;- 99,0 % (Sigma, P-0130)*;- 19- 99,0 % (Fluka, 74640)*;- 98,0 % (Sigma, D-3253)*;- 99,0 % (Sigma, H-7753)*;- 99,0 % (Sigma, D-4628)*;- *:1) (IRMM*,BCR-411);2) (IRMM, BCR-411);3) 17c97- (IRMM, BCR-474/475).5 5.1 1- 2- 12.1.007, , , 12.1.005.5.2 , , - .5.3 .5.4 12.2.085 - , , , .5.5 - - 12.1.019 .5.6 , -