NAVY MIL-K-17073-1952 KIT PACKAGED CHEMICALS PHOTOGRAPHIC NAVY RE-EXPOSURE REVERSAL PROCESS FOR 16MM UNIVERSAL FILM IN HOUSTON K-3A MACHINES《用于休斯顿16MM普通电影和海军重复暴光逆转过程的成相集成化学工具》.pdf

1、Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l7073(Aer) 16 March 1952 O-S-603 O-S-606 o-s-609 OS-616 Sodium Hydroxide, Photographic Sodium Sulfite, Anhydrous, (for). Photography Sodium Sulfate, Photographic (Anhydrous) Sodium Thiosulfate, An

2、hydrous, . Photographic Grade Navy iJepar-nen, Specification General Specifications for Inspectian of Material 22 OTHEH PUBLICATIONS,- The following other publications, of the issue in effect on date of invitation for bids, form a part of this speci- fication, Military Standard MIL -STD - 129 Harkin

3、g of Shipments American Standards 233 8 e 106 238.8,.153 Paraformaldehyde 238 8 , 105 Sodium Acid Sulfate 28% Acetio Acid 238 .?3.231 Sodium Me taborate Z38,8,101 Sulfuric Acid (Concentrated) 2.3 AVAILABILITY OF SPECIFICATIONS AND OTIIER PUBLICATIONS - 2a3.1 General.- When requesting specifications

4、and other 213.2 Government Specifications,- Copies of this specification publications, refer to both title and number, and applicable Government Specifications may be obtained upon application to the Commanding Offioer, U.S. Naval Air Station, JohnsviLle, Pennsylvania, Attention: Technical Records D

5、ivision. 2e3e3 ASA Standards.- Copies of American Standards may be obtained from the American Standards Association, Inc., 70 East 45th Street, New York 17, New York. 3 REQUIIIEMENTS 3.1 MATERIALS.- All chemicals in the kit shall conform to the specifications and standards designated. When materials

6、 are used which are not specifically designated, they shall be of the. highest photographic quality and suitable for the purpose. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l7073(Aer) 16 March 1952 3.2 FORM.- Each powdered chemical shall b

7、e dry, free-flowing, 3.3 WEIGHT TOLERANCE.- The weight of each chemical shall be without lumps OP clusters, and in such form as to dissolve easily. accurate to within two percent of the specified weight. The weight of the contents of each container shall be accurate to within three percent of the sp

8、ecified weight. and seven separate. packages of chemicals as follows: 3.4 COMPONENTS.- The kit shall consist of an instruction sheet 1 package of Prehardener, Formula UH-1 1 package of.Birst Developer, Formula EW-1 2 packages of Bleach, Formula RB-1 or RB-2 1 package of Clearing Bath, Formula RC-1 1

9、 package of Second Developer, Formula “-1 1 package of Fixing Bath, Formula RF-2 or alternate 3.5 CONTAINERS.- Inner containers shall be used to package chemicals of a formula which must be kept separated until use. Each main container shall enclose one.package of a formula, including any necessary

10、inner containers. The seven main containers shall be packaged with an instruction sheet in an outside container. 3.5.1 Container Haterial. - 3.5.1.1 Outside Container.- The outside container shall be a single rectangular-shaped carton made of Y-Board, of such size as to snugly enclose the contents o

11、f the kit, and of such strength as to withstand normal handling and shipment without tearing or breaking. 3.5.1.2 Main Containers.- The main containers shall be of tinplate or terneplate conforming to the requirements of Federal Specification O-P-16 and shall preclude the possibility of interaction

12、between the containers and the chemicals with which they come in contact. The containers may be round, square or rectangular in cross section. The containers shall be hermetically sealed and shall be equipped with suitable means for openins, such as key- type, rip-strip opening. 3.5.1.3 Inner Contai

13、n=.- The inner containers shall be of such material as to preclude the possibility of interaction between the container and the chemicals with which t comes in contact. The inner containers shall be so constructed as to eliminate the possibility of the contents sfting or leaking. 3 -5 1 e4 Glass Btt

14、1es.- Inner containers made of glass shall conform to the requirements of Federal Specification O-P-16 and may be round, oblong, or rounded square with sloping shoulders. Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l7073(Aer) 16 March 1952

15、3.6 LABELING - 31611 Kit Label.- The following information shall be plainly marked with waterproof stencil or labels on the outside container of the kit: KIT, PACIUGED CHEMICALS, PBOTOGHAPBIC, NAVY RE-EXPOSUHE lIEVEli5AL PTLOCESS Poli 16FiM UNIVEIISAL FILM IN IIOUSTON Ei-3A MACHINES Specification No

16、. Navy Stock No, Contract No , Date of Manufacture Manufacturers Name or Trademark U, S. PROPERTY 3.6.2 Main Container LaBel.- Each main container shall have the Type matter type matter printed directly on the surface by lithographic or other suitable process which will pass the test specified in pa

17、ragraph 4.5.3, shall be lacquered or otherwise protected against abrasion, shall be legible and not less than 6-point in size. all applicable Federal and State laws, containers, Labels shall conform to all applicable Federal and State laws. the prehardener shall be in accordance with Table I. Type m

18、atter Labels shall conform to 3,613 Inner Container Label,- Paper labels may be used on inner Type matter shall be legible and not less than 6-point in size, 3.7 PHEHAWENER FORMULA, UH-1 , - The chemical composition of TABLE I PmtIARDENER, FORMULA UH-1 Quantity for 3 Specification Part gallons (11,3

19、5 or liters) of work- Standard ing solution GRAMS Sodium Hexametaphosphate a 5.7 - (Calgon) Sodium Bisulfite a 34.1 O-S-579 Sodium Sulfate, Anhydrous a 567.8 O-S-609 6-Nitrobenzimidazole Nitrate a 0.3 O -N -376 Total net weight, part a 607.9 Sodium Carbonat,e, Mbnohydrated b 56.5 O-S-581 araf o rmal

20、 de hsde C 45 .4 238 . 8 . 153 Total net weight, prehardener 7U9,8 Packaging of Prehardener,- The prehardener shall be %- 3*7*1 psokaged By placing Parta chemioals in the main container and Parts b and c ohemicals in individual inner containers. Inner containers b and c shall then be plaoed in the m

21、ain oontainer, Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-ow(A) 16 March 19.52 3.7.2 .- The preliardener containers shall e 3.7.2.1 Main Container Label. - Prehardener Formula UH-1 for KaVy marked with the tion. He-Exposure Reversal Proces

22、s Kit, 3 gallon size, (11.35 liters) net weight, grams. Directions: 1, Remove the inner containers, Parts b and c, from tho maih container. 2. Dissolve the cliemjcals from the main container, Part a, in 2 gallons of water at IoC-OOF. 3. Add and dissolve the contents of Part h inner container. 4. Add

23、 and dissolve the conteiifs of Part c inner container. 5. Add water to make a total or. 3 gallons, 6. Adjust temperature of solution to 65-70F. 3.7.2.2 Part h Label.- Prehardener U$-1, Part b, 3 g3llon size. 3.7.2.3 Part c Label.- Prehardener UII-1, Part c, 3 gallon size. 3.5 FIRST DEVELOPER, FORMUL

24、A RV-1.- The chemical composition of the first developer shall be in accordance wifh Table II, TLE Ir FIRST IIEmIOPER, FOFiFULA RN-1 - . Quantity for 6 Part gallons (22.7 SpecitTcation liters) of work- or .- jing solution Standard - Monome thy1 Paraminophenol a 13.6 Grams O-M-571 Hydro quinone if 45

25、4.2 Grams O-H-886 Sulfate (Elon) Total net weight, Part a 4678 Grams Sodium Hexametaphospha.te b 11.4 Grams - Sodznni Sulfite (Anhydrous) .b 1135.5 Grams O -S -606 Potassium Bromide b 181.7 Grams o-P-u51 (Calgon) Sodium Thiocyanate b 56.8 Grams - Total net weight, Fart b 1385.4 Grams Sodium Hyiiroxi

26、.de C 450.2 Grams 0-3-603 Total net weight, first developer 2307.4 Grams - - 3 e8 e1 Packazihff of First Developer. - ThO f+rst developer shall be packaged by placing Part h chemicals into the main container, Part a chemicals in an individual inner conainer and Part c, in a sealed glass bottle, Plac

27、e the bottle containing Part c in the pot?dered chemtcals in the niain container and then place the inner container nf Part a over the hottle. . 3, 5 P : .$ -$ Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-17073 67 9999906 0150LI78 7 m MIL-K-

28、l7073(Aer) 16 March 1952 3.8.2 First Developer Labels.- The first developer containers 3o8,2.1 Main Container.Labe1.- First Developer RN-1 for Navy Re- shall be marked with the following information, Exposure Reversal Process Kit, 6 gallon size (22,7 liters), net weight grams . Di re c tions : 1, Re

29、move the inmr containers, Parts a and c (bottle) from the main container. 2. Dissolve the contents of Part a, inner container in 3 gallons of water at 1l5-121i0F. 3. Add and dissolve the chemicals in the main container, Part b. 4, Add and dissolve the contents of the bottle, Part C. 5. Add water to

30、make a total of 6 gallons. 6. Adjust temperature of solution to 65-7OoF. NOTE: 3.a.2.2 Part a Label,- First Developer HN-l, Part a, 6 gallon size, 3.8.2.3 Part c Label.- First Developer IN-1, Part c, 6 gallon size. 3.9 BLEACH,- Each kit shall have two main containers of bleach, For Ansco Hypan, Ansc

31、o Triple-S and DuPont 314 add 113.4 grams sodium thiocyanate to the six gallons of first developer “-1. The blesch shall have the czhemical composition of Formulas RE-1 or RB-2 in aooordsnce with Tables IIIa or IIIb, respectively, TABLE IIIa BmACH, FOREIITLA RB-1 Quantity for 3 gal- Part lons (11.35

32、 liters) of working sol- ution Potassium Dichromate a 125,O grams Sulfurio Acid, Concentrated b 204.4 ml. TABLE: IIIb BmACH, FORMULA RB-2 Po tas sium Dichroma te Sodium Acid Sulfate, Fused t Total net weight, Bleach RB-2 cation or Standard O-P-556 Quantity for 3 gal- Specifi- of working sol- Standar

33、d ution Part lone (11.35 liters) cation or GRAMS a 125.0 O-P-556 a 920 , o 238 8 105 1045 *O Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l7073(Aer) 16 March 1952 . 3.9.1 Packaging of Formula RB-1; - The bleach Formula RB-1 shall be packaged

34、 by placing Part a in an individual inner container and Part b in an individual sealed, glassktoppered, glass bottle. Place sufficient Filtercel, OP equivalent inert absorbent material, to properly pack the bottle containing Part b in the main container and then place Part a con- tainer over the bot

35、tle. bottle and closure of materidl which is inert to the action of concentrated sulfuric acid may be used. and the inner containers shall be printed in red, with the word ltPOISONtt prominent on each label. of the inner container labels. In addition, the bleach labels shall be marked with the follo

36、wing information. Exposure Reversal Process Kit, 3 gallon size, (11.35 liters) net weight- grams. Directions: 1. 2. Slowly add the sulfuricacid while stirring. 3. Add water to make a total of 3 gallons. 4. Adjust temperature of solution to 65-7OOF. 3.9.1.1 In. lieu of the glass-stoppered glass bottl

37、e for Part b, a 3.9.1.2 Formula RB-1 Labels.- The labels for the main container Proper antidotes shall also be described on each 3.9.1.2.1 Main Container Label.- Bleach Formula RB-1 for Navy Re- Dissolve Part a in 2 gallons of water at 60-70F. Sulfuric acid should always be added slowly to the potas

38、sium dichromate solution. Never add water or water solutions to sulfuric acid! Bleach RB-1 is a powerful corrosive mixture and should be handled with care. Mixing should be done in a stainless steel bucket or an earthenware crock. B1each.m-1 should not be allowed to stand in stainless steel buckets

39、for long periods because of tendency to corrode. 3.9.1.2.2 Part a Label.- Bleach RB-1, Part a, 3 gallon size. 3.9.1,2.3 Part b Label.- Bleach RB-1, Part b, 3 gallon size. 2.9.2 Packaging of Formula RB-2.- Place the powdered chemicals in a main container. 3*9*2*1 Formula RB-2 Labels.- The label for t

40、he main container shall be printed in red, with the word “POISON“ prominent. Proper antidotes shall also be described on the label. In addition the label shall be marked with the following information: Bleach Formula RB-2 for Navy Re-Exposure Reversal Process Kit, 3 gallon size, (11.35 liters), net

41、weight grams. f- 7 Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-L7073 b7 77779Ob OL5OqO 5 W MIL-K-l7073(Aer) 16 March 1952 -=, Provided by IHSNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l7073(Aer)

42、 i6 March 1952 TABLE V - SECOND DEVELOPER, FORMULA Rp-1 Quantity for 3 Specification liters) of work- Standard inn solution GRAMS Part gallons (11.35 or Monomethyl Paraminophenol Sulfate a 11.4 O-M-571 Hydroquinone a 227.1 0-H-886 (Elon) Total net weight, Part a 238.5 ,Sodium Hexametaphosphate b 5.7

43、 - ( Ca i gon ) Sodium Sulfite (Anhydrous) b 567.8 O-S-606 Potassium Bromide b 56.8 O-P-551 Total net weight, Part b 630.3 Sodium Hydroxide C 170.3 O-S-603 Total weight, Second Developer 1039.1 3.11.1 Packaging of Second Developer.- The second developer shall be packaged by placing Part b chemicals

44、in the main container, Part a in an inner container, and Part c in a glass bottle. Place Part c in the powdered chemicals in the main container and then place Part a on top of the bottle. . 3.11.2 Second Developer Labels.- The second developer containers 3.11.2.1 Main Container Label.- Second Develo

45、per Formuia Rp-1 for shall be marked with the following information. Navy Re-Exposure Reversal Process Kit, 3 gallon size (11.35 liters), net weight Directions: 1. .Remove the inner containrs, Part a and c (bottle) from 2. 3. 4. Add and dissolve the contents of the bottle, Part c. 5. Add water to ma

46、ke 3 gallons. 6. Adjust temperature of solution to 65-700F. he main container. Disso1,ve the contents of Part a inner container in 24 gallons of water at 115-125OF: Add and-dissolve the chernicals in the main container, Part b. 3.11.2.2 Part aiLabel.- Second Developer Rp-1, Part a, 3 gallon size. 3.

47、11.2.3 Part b Label.- Second Developer RP-1, Part c, 3 gallon size. 3.12 FIXING BATH.- The fixing bath shall have the chemical com- position of Formula RF-2 in accordance with Table VI, or shall meet the requirements for the Alternate Fixing- Bath in acc0rdanc.e with paragraph 3.12.1 Provided by IHS

48、Not for ResaleNo reproduction or networking permitted without license from IHS-,-,-MIL-K-l?073(Aer) 16 March 1952 :Sodium Thiosulfate. Anhydrohs I a I 2315.0 grams 1 043-616 I 726, mis. 238.8 . 3.08 28d Acetic Acid b Soclium Metaborate C 227,l grams Z38,8.231 Aluminum Potassium Sulfate C 227;l grams

49、 0-A-421 Total net weight, Part c 454.2 grams 3,12,1 Alternate Fixing Bath.- A drv Dackaged fixer which is which shall show no tendency to lowering of ttwashabilTtyt of the SensitizGii material, and which has substantially the same photographic characteristics, shall also be acceptable, 3e12e2 Packaging of Fixing Bath. Formula RF-2.- Formula FU?-2 P