1、AEROSPACE MATERIAL SPECIFICATIONAMS 3054BIssuedRevisedSuperseding AMS 3054AOil, Lubricating, Low TemperatureFor -55 C (-67 F) Service1. SCOPE:1.1 Form: This specification covers a petroleum-base lubricating oil.1.2 Application: This lubricant has been used typically for general purpose, low-temperat
2、ure lubrication applications where low evaporation and rust-preventive characteristics are desired, but usage is not limited to such applications.1.3 Safety - Hazardous Materials: While the materials, methods, applications, and processes described or referenced in this specification may involve the
3、use of hazardous materials, this specification does not address the hazards which may be involved in such use. It is the sole responsibility of the user to ensure familiarity with the safe and proper use of any hazardous materials and to take necessary precautionary measures to ensure the health and
4、 safety of all personnel involved.2. APPLICABLE DOCUMENTS: The issue of the following documents in effect on the date of the purchase order forms a part of this specification to the extent specified herein. The supplier may work to a subsequent revision of a document unless a specific document issue
5、 is specified. When the referenced document has been canceled and no superseding document has been specified, the last published issue of that document shall apply.Reaffirmed 1983-072001-052010-05SAE Technical Standards Board Rules provide that: “This report is published by SAE to advance the state
6、of technical and engineering sciences. The use of this report is entirely voluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole responsibility of the user.” SAE reviews each technical report at least every five years
7、 at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions. Copyright 2010 SAE International All rights reserved. No part of this publication may be reproduced, stored in a retrieval system or transmitted, in any form or by any means, electronic, me
8、chanical, photocopying, recording, or otherwise, without the prior written permission of SAE. TO PLACE A DOCUMENT ORDER: Tel: 877-606-7323 (inside USA and Canada) Tel: +1 724-776-4970 (outside USA) Fax: 724-776-0790 Email: CustomerServicesae.org SAE WEB ADDRESS: http:/www.sae.org SAE values your inp
9、ut. To provide feedback on this Technical Report, please visit http:/www.sae.org/technical/standards/AMS3054B Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-AMS 3054B SAE AMS 3054B- 2 -2.1 SAE Publi
10、cations: Available from SAE, 400 Commonwealth Drive, Warrendale, PA 15096-0001.AMS 2759/2 Heat Treatment, of Low-Alloy Steel Parts, Minimum Tensile Strength 220 ksi (1515 MPa) and HigherAMS 4037 Aluminum Alloy Sheet and Plate, 4.4Cu - 1.5Mg - 0.60Mn, (2024; T3 Flat Sheet, -T351 Plate), Solution Heat
11、 TreatedAMS 4377 Magnesium Alloy Sheet and Plate, 3.0Al - 1.0Zn, 0.20Mn (AZ31B-H24), Cold Rolled and Partially AnnealedAMS 4500 Copper Sheet, Strip, and Plate, Soft AnnealedAMS 4507 Copper Alloy (Brass) Sheet, Strip, and Plate, 70Cu - 30Zn, Half Hard (H02)AMS 5040 Steel Sheet and Strip, 0.15 max Car
12、bon, Deep Forming GradeAMS 6440 Steel Bars, Forgings, and Tubing, 1.45Cr (0.98 - 1.10C), (SAE 52100), For Bearing Applications2.2 ASTM Publications: Available from ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959.ASTM D 91 Precipitation Number of Lubricating OilsASTM D 92 Flash and Fire
13、 Points by Cleveland Open CupASTM D 97 Pour Point of Petroleum ProductsASTM D 130 Detection of Copper Corrosion from Petroleum Products by the Copper Strip Tarnish TestASTM D 445 Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)ASTM D 664 Acid Number of Pet
14、roleum Products by Potentiometric TitrationASTM D 972 Evaporation Loss of Lubricating Greases and OilsASTM D 1500 ASTM Color of Petroleum Products (ASTM Color Scale)ASTM D 1748 Rust Protection by Metal Preservatives in the Humidity Cabinet2.3 ANSI Publications: Available from ANSI, 1430 Broadway, Ne
15、w York, NY 10018.ASME B46.1 Surface Texture3. TECHNICAL REQUIREMENTS: 3.1 Material:The oil shall be a fraction of refined crude petroleum, containing additives imparting corrosion protective and oxidation resisting properties, meeting the requirements of 3.2.Copyright SAE International Provided by I
16、HS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-AMS 3054B SAE AMS 3054B- 3 -3.2 Properties:The oil shall conform to the following requirements, determined in accordance with specified test methods, insofar as practicable: 3.2.1 Color and Ap
17、pearance: The oil shall be clear, transparent, and uniform in appearance and not darker than No. 5 (ASTM Color Scale), determined in accordance with ASTM D 1500.3.2.2 Kinematic Viscosity: Shall conform to the values shown in Table 1, determined in accordance with ASTM D 445:3.2.3 Flash Point: Shall
18、be not lower than 130 C (266 F), determined in accordance with ASTM D 92 on the preproduction sample. Tests on subsequent lots for acceptance testing shall not differ from the preproduction flash point value by more than 6 C (10 F) degrees.3.2.4 Pour Point: Shall be -57 C (-71 F) or below, determine
19、d in accordance with ASTM D 97.3.2.5 Precipitation Number: Shall be 0.00, determined in accordance with ASTM D 91.3.2.6 Corrosion: Shall be not greater than Class 1, determined in accordance with ASTM D 130 at 100 C 1 (212 F 2) for 3 hours 0.1.3.2.7 Evaporation: Weight loss shall not exceed 22%, det
20、ermined in accordance with ASTM D 972.3.2.8 Humidity Resistance: Not more than one panel out of five, covered with a film of the lubricating oil and subjected to humidity testing in accordance with ASTM D 1748 for 100 hours 0.25, using the same steel and thickness of test panel as in 4.5.1.2, shall
21、exhibit either a dot of rust larger than 2 mm in diameter or two or more dots of rust larger than 1 mm in diameter on the significant area of the panel.3.2.9 Corrosion and Oxidation Stability: The oil shall comply with the following requirements, determined in accordance with 4.5.1:3.2.9.1 Corrosion
22、: The change in weight of metal test specimens shall not exceed 0.2 mg/cm2of surface for each specimen. There shall be no pitting, etching, or visible corrosion on the surfaces of any of the metals when examined at approximately 20X magnification. Slight discoloration of surfaces of the copper and c
23、admium specimens is permissible.TABLE 1 - Kinematic ViscosityTemperature, 1 C (2 F) Value, centistokes (mm2/s), max38 C (100 F) 10-40 C (-40 F) 4000Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-AMS
24、 3054B SAE AMS 3054B- 4 -3.2.9.2 Viscosity Change Due to Oxidation: The viscosity of the oil shall be within -5 to +20% of the original viscosity, determined in accordance with ASTM D 445 at 38 C 1 (100 F 2).3.2.9.3 Acid Number Change Due to Oxidation: After the oxidation-corrosion test, the increas
25、e in the acid number shall be not greater than 0.20 and there shall be no evidence of separation of insoluble materials or gumming of the oil.3.2.10 Low-Temperature Stability: There shall be no indication of low-temperature instability evidenced by gelling or separation of solid or liquid phases in
26、the oil after completion of the test in 4.5.2. The presence of cloudiness, which does not settle out, is acceptable.3.2.11 Corrosivity Test: Two of the three test assemblies shall show no signs of corrosion or pitting, and the third disc shall exhibit not more than three spots of corrosion within th
27、e area covered by the brass clip, determined in accordance with 4.5.3.3.3 Quality:Oil, as received by purchaser, shall be free of undissolved water, sediment, suspended matter, and other foreign materials detrimental to usage of the oil.4. QUALITY ASSURANCE PROVISIONS: 4.1 Responsibility for Inspect
28、ion: The vendor of oil shall supply all samples for vendors tests and shall be responsible for the performance of all required tests. Purchaser reserves the right to sample and perform any confirmatory testing deemed necessary to ensure that the oil conforms to the specified requirements.4.2 Classif
29、ication of Tests: 4.2.1 Acceptance Tests: The following requirements shown in Table 2 are acceptance tests and shall be performed on each lot:TABLE 2Requirement Paragraph ReferenceColor 3.2.1Kinematic Viscosity 3.2.2Flash Point 3.2.3Pour Point 3.2.4Precipitation Number 3.2.5Corrosion, Copper Strip 3
30、.2.6Evaporation 3.2.7Corrosion and Oxidation Stability 3.2.9Copyright SAE International Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-AMS 3054B SAE AMS 3054B- 5 -4.2.2 Preproduction Tests: All technical requirements are prepr
31、oduction tests and shall be performed prior to or on the initial shipment of oil to a purchaser, when a change in material and/or processing requires reapproval as in 4.4.2, and when purchaser deems confirmatory testing to be required.4.3 Sampling:Sufficient oil shall be taken at random from each lo
32、t to perform all required tests. The number of determinations for each requirement shall be as specified in the applicable test procedure or, if not specified therein, not less than three. 4.3.1 A lot shall be all oil produced in a single production run from the same batches of raw materials under t
33、he same fixed conditions and presented for vendors inspection at one time and shall not exceed 10,000 gallons (37,854 L).4.3.2 When a statistical sampling plan and acceptance quality level (AQL) have been agreed upon by purchaser and vendor, sampling shall be in accordance with such plan in lieu of
34、sampling as in 4.3 and the report of 4.6 shall state that such plan was used.4.4 Approval:4.4.1 Sample oil shall be approved by purchaser before oil for production use is supplied, unless such approval be waived by purchaser. Results of tests on production oil shall be essentially equivalent to thos
35、e on the approved sample.4.4.2 Vendor shall use ingredients, manufacturing procedures, and methods of inspection on production oil which are essentially the same as those used on the approval sample oil. If necessary to make any change in ingredients or in manufacturing procedures, vendor shall subm
36、it for reapproval a statement of the proposed changes in ingredients and/or processing and, when requested, sample oil. Production oil made by the revised procedure shall not be shipped prior to receipt of reapproval.4.5 Test Methods: 4.5.1 Corrosiveness and Oxidation Stability: 4.5.1.1 Test Apparat
37、us: Shall consist of the following:4.5.1.1.1 Test tube of standard-wall with 50 mm 3 OD and 500 mm 10 long, with open end formed as a male ground-glass joint.4.5.1.1.2 Allihn type condenser 40 mm, minimum, OD by 300 mm 20 long jacket, with the lower end formed as a female ground-glass joint to mate
38、with the test tube.4.5.1.1.3 Air tube of Pyrex, standard wall, 6 to 8 mm OD and length at least 50 mm longer than the combined length of the assembled test tube and condenser described above. The tube shall have one end drawn to an outside diameter of 0.063 inch 0.016 (1.60 mm 0.41).Copyright SAE In
39、ternational Provided by IHS under license with SAENot for ResaleNo reproduction or networking permitted without license from IHS-,-,-AMS 3054B SAE AMS 3054B- 6 -4.5.1.1.4 Constant temperature bath capable of maintaining a temperature 150 C 1 (302 F 2).4.5.1.2 Preparation of Specimens: Metal specimen
40、s, one each, nominally 0.032 inch (0.81 mm) thick by 1 inch (25 mm) square, with two holes (Figure 1) cut from the following materials: AMS 4500 copper, AMS 4037 aluminum alloy, AMS 4377 magnesium alloy, AMS 5040 low carbon steel, and cadmium anode material. Remove burrs from the edges of the specim
41、ens and from around drilled holes. Remove surface defects from both surfaces and all edges using progressively finer grades of abrasive paper. After this operation, all subsequent handling of the specimens shall be carried out with clean filter paper or tongs. Use a 240 grit (60 m) silicon carbide p
42、aper for the final sanding operation, making sure all marks produced by previous abrasive papers are removed. Clean the specimens and store separately immersed in acetone. Remove the specimens from the acetone and polish both flat surfaces and edges, using 150 mesh (100 m) silicon carbide grains app
43、lied with an acetone moistened pad. Wipe the specimens with clean absorbent cotton pads, changing pads until the pad no longer exhibits a soil when the specimen is wiped. Wash the specimens in a warm (approximately 55 C (131 F) suitable solvent and allow them to air dry. Weigh and record the weight
44、of each specimen to an accuracy of 0.1 milligram.4.5.1.3 Test Procedure: Determine the neutralization number of the oil sample in accordance with ASTM D 664. Determine the viscosity of the oil in accordance with ASTM D 445 at 38 C 1 (100 F 2). Arrange the prepared metal specimens in a wooden or plas
45、tic fixture in the pattern shown in Figure 1, making sure the magnesium and copper specimens do not touch. Tie the squares together using a clean light-weight cotton or nylon cord. Wear latex surgical gloves or nylon gloves when handling the cord and tying the knots. Using forceps, place the assembl
46、ed specimens in the bottom of the test tube with the squares positioned vertically (so the air tube can be inserted to the bottom of the test tube). Weigh the test tube with metal specimens and the air tube together to the nearest 0.1 gram. Add 100 mL 1 of the sample oil to the test tube containing
47、the metal specimens, reweigh the air tube, test tube, and contents together to the nearest 0.1 gram and determine the weight of the oil sample added. Assemble the test tube and condenser and mount the assembly so that 300 mm 50 of the test tube is submerged in the constant temperature bath previousl
48、y stabilized at 150 C 1 (302 F 2). Start the flow of cooling water through the condenser jacket. Insert the air tube, orifice end down, through the condenser and into the oil sample, and support it so the orifice is within 0.125 inch (3.18 mm) of the bottom of the test tube. Connect the air tube to
49、a supply of low pressure, filtered, dry air, and adjust the flow through the tube to 5 liters/hour 0.5. Continue the test for 68 hours 1. At the end of the test period, stop the flow of air, remove the air tube, and separate the condenser from the test tube containing the specimens. Remove the test tube from the constant temperature bath, allow to cool to room t
