1、Manual de Estndares de Medicin de Petrleo Captulo 8.5 Prctica Estndar para Muestreo de Cilindros de Pistn Manual para Productos de Petrleo Crudo Voltiles, Condensados y Productos Derivados del Petrleo Lquido PRIMERA EDICIN, DICIEMBRE DE 2015 Notas Especiales /DVSXEOLFDFLRQHVGHO$3,VRORVHUHHUHQDSUREOH
2、PDVGHQDWXUDOHDJHQHUDO(QFDVRGHFLUFXQVWDQFLDVSDUWLFXODUHVVHGHEHUtDQUHYLVDUODVOHHVUHJXODFLRQHVORFDOHVHVWDWDOHVIHGHUDOHV1LHO$3,QLQLQJXQRGHVXVHPSOHDGRVVXEFRQWUDWLVWDVFRQVXOWRUHVFRPLWpVXRWURVDSRGHUDGRVJDUDQWLDQRUHSUHVHQWDQGHPDQHUDHSUHVDRLPSOtFLWDFRQUHODFLyQDODSUHFLVLyQLQWHJULGDGRXWLOLGDGGHODLQIRUPDFLyQDTX
3、tFRQWHQLGDQLDVXPHQQLQJXQDREOLJDFLyQRUHVSRQVDELOLGDGSDUDQLQJQXVRRORVUHVXOWDGRVGHWDOXVRGHODLQIRUPDFLyQRORVSURFHVRVUHYHODGRVHQHVWDSXEOLFDFLyQ1LHO$3,QLQLQJXQRGHORVHPSOHDGRVVXEFRQWUDWLVWDVFRQVXOWRUHVXRWURVDSRGHUDGRVDUPDQTXHHOXVRGHHVWDSXEOLFDFLyQQRLQIULQJLUiQLQJQGHUHFKRSULYDGR/DVSXEOLFDFLRQHVGHO$3,SXHGHQV
4、HUXWLOLDGDVSRUFXDOTXLHUDTXHGHVHHKDFHUOR(O,QVWLWXWRKDUHDOLDGRWRGRHOHVIXHURSRVLEOHSDUDDVHJXUDUODSUHFLVLyQODYHUDFLGDGGHORVGDWRVFRQWHQLGRVHQGLFKDVSXEOLFDFLRQHVVLQHPEDUJRQRKDFHQLQJXQDGHFODUDFLyQQLRWRUJDQLQJXQDJDUDQWtDHQUHODFLyQFRQHVWDSXEOLFDFLyQSRUHVWHPHGLRHSUHVDPHQWHGHVFRQRFHFXDOTXLHUREOLJDFLyQRUHVSRQVD
5、ELOLGDGSRUSpUGLGDRGDxRFRPRUHVXOWDGRGHVXXVRRSRUODYLRODFLyQGHFXDOTXLHUDXWRULGDGDSURSLDGDFRQMXULVGLFFLyQFRQODFXDOHVWDSXEOLFDFLyQSXHGDHVWDUHQFRQLFWR/DVSXEOLFDFLRQHVGHO$3,VHSXEOLFDQSDUDIDFLOLWDUODDPSOLDGLVSRQLELOLGDGGHSUiFWLFDVSUREDGDVGHLQJHQLHUtDGHVRQLGRSUiFWLFDVGHIXQFLRQDPLHQWR(VWDVSXEOLFDFLRQHVQRHVWiQ
6、SHQVDGDVSDUDREYLDUODQHFHVLGDGGHDSOLFDUHOEXHQMXLFLRHQUHODFLyQFRQHOPRPHQWRHOOXJDUHQORVTXHVHGHEHUtDQXWLOLDUHVWDVSXEOLFDFLRQHV/DIRUPXODFLyQODSXEOLFDFLyQGHODVSXEOLFDFLRQHVGHO$3,QRWLHQHQSRUREMHWRLQKLELUGHQLQJXQDPDQHUDDQLQJXQDSHUVRQDTXHGHVHHXWLOLDURWUDVSUiFWLFDV/RVXVXDULRVGHHVWHHVWiQGDUQRGHEHUtDQGHSHQGHUHF
7、OXVLYDPHQWHGHODLQIRUPDFLyQLQFOXLGDHQHVWHGRFXPHQWR3DUDHOHPSOHRGHODLQIRUPDFLyQLQFOXLGDHQHVWHGRFXPHQWRVHGHEHUtDXWLOLDUHOVHQWLGRFRPQHQFXDQWRDODVSHFWRFRPHUFLDOFLHQWtFRGHLQJHQLHUtDGHVHJXULGDG(O$3,QRVHFRPSURPHWHDFXPSOLUODVREOLJDFLRQHVGHORVHPSOHDGRUHVIDEULFDQWHVRSURYHHGRUHVUHODFLRQDGDVFRQDGYHUWLUHQWUHQDUFRU
8、UHFWDPHQWHHTXLSDUDVXVHPSOHDGRVDFXDOTXLHUSHUVRQDHSXHVWDHQORFRQFHUQLHQWHDULHVJRVGHVDOXGVHJXULGDGQLVHFRPSURPHWHDFXPSOLUHVDVREOLJDFLRQHVFRQIRUPHDODVOHHVORFDOHVHVWDWDOHVRIHGHUDOHV/RVVLWLRVGHWUDEDMRODVRSHUDFLRQHVGHORVHTXLSRVSXHGHQYDULDU/RVXVXDULRVVRQUHVSRQVDEOHVQLFDPHQWHGHHYDOXDUVXVHTXLSRVHLQVWDODFLRQHVHV
9、SHFtFRVSDUDGHWHUPLQDUVLFRUUHVSRQGHDSOLFDUHOHVWiQGDU(QWRGRPRPHQWRDOXVDUHVWHHVWiQGDUORVXVXDULRVGHEHUtDQHPSOHDUVXVHQWLGRFRPQHQFXDQWRDODVSHFWRFRPHUFLDOFLHQWtFRGHLQJHQLHUtDGHVHJXULGDG/RVHMHPSORVHQHVWHGRFXPHQWRVHLQFOXHQVRORFRQQHVLOXVWUDWLYRV , proporciona instrucciones sobre la WUDQVIHUHQFLDHQWUHHO033527U
10、DQVIHUHQFLDGHXQ03PXHVWUDODFRQJXUDFLyQHOSURFHGLPLHQWRGHWUDQVIHUHQFLD; SDUDSHUPLWLUODHSXOVLyQGHDLUHDPHGLGDTXHVHIXHUDHOSLVWyQKDFLDHOHWUHPRGHOFLOLQGUR/DSUHVLyQGHODIXHQWHGHDJXDRJDVLQHUWHGHEHVHUXQPDRUTXHODSUHVLyQGHODPXHVWUDGHO03XVDQGRODVWXEHUtDVODYiOYXODORVDFFHVRULRVGHOYROXPHQPXHUWREDMR;$%5$ODYiOYXODGHYDF
11、tR 9 ODYiOYXODGHO)3 3HUPLWDTXHIXQFLRQHODSUHVLyQGHYDFtRGXUDQWHPLQXWRV N3D SDUDHOLPLQDUHODLUHUHVLGXDOGHODOtQHDGHWUDQVIHUHQFLDHOYROXPHQPXHUWRGHOFLOLQGUR$; ;HVFRQHFWHODERPEDGHYDFtRGHODYiOYXODGHYDFtR 9 ;0LHQWUDVFRPSULPHHOSLVWyQGHO030LHQWUDVFRPSULPHHOSLVWyQGHO03 SDUDSHUPLWLUTXHODPXHVWUDOOHQHHOYROXPHQPXHUW
12、RGHO)3 0LHQWUDV FRPSULPH HO SLVWyQ GHO 03%;)LMHHOUHJXODGRUGHFRQWUDSUHVLyQ %35 DOSRUHQFLPDGHODSUHVLyQGHODPXHVWUDGHO03 0LHQWUDV FRPSULPH HO SLVWyQ GHO 03 ODYiOYXODGHODPXHVWUDGHO039(17,/(ODSUHVLyQUHVWDQWHGHOYROXPHQPXHUWRGHODOtQHDGHWUDQVIHUHQFLDDWUDYpVGHODYiOYXODGHYDFtR 9 ;6LJDODVLQVWUXFFLRQHVGHOIDEULFD
13、QWHGHOLQVWUXPHQWRSDUDODFDUJDODLQHFFLyQGHODPXHVWUD;7UDQVIHUHQFLDGHXQ03;PXHVWUDQODSUHSDUDFLyQHOSURFHGLPLHQWRGHWUDQVIHUHQFLD127$;(OGHVSODDPLHQWRGHDJXDQRHVDGHFXDGRFXDQGRHODJXD11D8009 15 WDPELpQHVXQFRPSRQHQWHLPSRUWDQWHRFXDQGRSXHGHDIHFWDUORVUHVXOWDGRVGHODSUXHED;Preparacin del CVCLa )LJ;PXHVWUDHOPpWRGRGHSU
14、HSDUDFLyQXVDGR(OFLOLQGURGHEHSHUPDQHFHUYHUWLFDOGXUDQWHODSUHSDUDFLyQ;,QVWDOHXQDFFHVRULRFRQUHEDEDSDUDPDQJXHUDGH1LQHQODYiOYXOD;/OHQHHOUHVHUYRULRGHDJXDFRQXQYROXPHQVXFLHQWHSDUDOOHQDUHOFLOLQGURVLQYDFLDUHOUHVHUYRULRGHOWRGR 6HUHFRPLHQGDXQYROXPHQGH P/ 5HJLVWUHHOYROXPHQLQLFLDO$;$%5$ODYiOYXODGHOFLOLQGUR ;$%5$OD
15、YiOYXODGHVDOLGDGHOUHVHUYRULRSDUDFRPHQDUDOOHQDUHOFLOLQGURFRQDJXD;$%5$ODYiOYXODGHOFLOLQGUR ; YHQWLODQGRHODLUHVLJDOOHQDQGRKDVWDTXHVDOJDDJXDGHODYiOYXOD;DFRQWLQXDFLyQLQPHGLDWDPHQWH%;1ROOHQHHO(OYROXPHQGHOOHQDGRVHUiODGLIHUHQFLDHQWUHORVYROPHQHVLQLFLDOQDO(VWHYROXPHQVHXVDUiGXUDQWHODWUDQVIHUHQFLDGHODPXHVWUD;7U
16、DQVIHUHQFLD GH OD 0XHVWUD GH XQ 03PXHVWUDODWUDQVIHUHQFLDGHXQ03XVDQGRODVWXEHUtDVODYiOYXODORVDFFHVRULRVGHOYROXPHQPXHUWREDMR;$%5$ODYiOYXODGHYDFtR 9 SHUPLWDTXHIXQFLRQHGXUDQWHPLQXWRV N3D SDUDHOLPLQDUHODLUHUHVLGXDOGHODOtQHDGHWUDQVIHUHQFLDHOYROXPHQPXHUWRGHODOtQHDGHWUDQVIHUHQFLD$;HVFRQHFWHODERPEDGHYDFtRGHOD
17、YiOYXODGHYDFtR 9 ; 0LHQWUDV FRPSULPH HO SLVWyQ GHO 03 0LHQWUDV FRPSULPH HO SLVWyQ GHO 03 SDUDSHUPLWLUTXHODPXHVWUDHQWUHHQFRQWDFWRFRQHODJXDGHGHVSODDPLHQWRGHQWURGHO% ;),-(HOUHJXODGRUGHFRQWUDSUHVLyQ %35 DOSRUHQFLPDGHODSUHVLyQGHODPXHVWUDGHO037UDQVIHUHQFLDGHO03 0LHQWUDV FRPSULPH HO SLVWyQ GHO 03 ODYiOYXOD
18、GHODPXHVWUDGHO039(17,/(ODSUHVLyQUHVWDQWHGHOYROXPHQPXHUWRGHODOtQHDGHWUDQVIHUHQFLDDWUDYpVGHODYiOYXODGHYDFtR 9 ;7UDQVIHUHQFLDGHXQPXHVWUDODFRQJXUDFLyQ(OFLOLQGURGHODPXHVWUDHOFLOLQGURGHVHSDUDFLyQGHEHQSHUPDQHFHUYHUWLFDOHVGXUDQWHWRGDODWUDQVIHUHQFLDGHODPXHVWUDDOLQVWUXPHQWR; 35(3$5( XQ VHJXQGR FLOLQGUR GH SUH
19、SDUDFLyQ VHJQ;SHURVROROOpQHORKDVWDHOGHOYROXPHQWRWDOGHOFLOLQGURFRQWURODQGRHOYROXPHQGHDJXDTXHVHXVySDUDOOHQDUOR;$-867(ODSUHVLyQGHJDVLQHUWHDOSRUHQFLPDGHODSUHVLyQGHOFLOLQGURGHODPXHVWUD;$%5$ OD YiOYXOD GHO FLOLQGUR GH VHSDUDFLyQ * SDUDSUHVXULDUHOFLOLQGURGHVHSDUDFLyQ;$%5$ODYiOYXODGHOFLOLQGURGHVHSDUDFLyQ : ODYiOYXODGHOFLOLQGURGHODPXHVWUD SDUDLJXDODUODSUHVLyQHQWUHDPERVFLOLQGURV; DOLQVWUXPHQWR;$%5$ODYiOYXODGHOFLOLQGURGHODPXHVWUD ; SDUDFRPHQDUDOOHQDUODOtQHDGHWUDQVIHUHQFLDHO
