1、BRITISH STANDARD BS EN ISO 4613-2:1995 Incorporating Amendment No. 1 Plastics Ethylene/vinyl acetate (E/VAC) moulding and extrusion materials Part 2: Preparation of test specimens and determination of properties The European Standard EN ISO 4613-2:1995, with the incorporation of amendment A1:2004, h
2、as the status of a British Standard ICS 83.080.20 BS EN ISO 4613-2:1995 This British Standard, having been prepared under the direction of the Sector Board for Materials and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 February 1996 BSI 11 October 2
3、004 ISBN 0 580 25159 4 National foreword This British Standard has been prepared by Technical Committee PRI/32, and is the official English language version of EN 4613-2:1995, Plastics Ethylene/vinyl acetate (E/VAC) moulding and extrusion materials Part 2: Preparation of test specimens and determina
4、tion of properties, including amendment A1:2004, published by the European Committee for Standardization (CEN). EN 4613-2:1995 was produced as a result of international discussions in which the United Kingdom took an active part. EN 4613-2:1995 has been approved by CEN member bodies under the weight
5、ed voting procedures introduced in 1988 to coincide with the introduction of “New Approach” Directives from the Commission of the European Community. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Cat
6、alogue under the section entitled “International Standards Correspondence index”, or by using the “Search” facility of the BSI Standards Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its co
7、rrect application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, pages 2 to 7 and a back cover. The BSI copyright notice displayed in this document in
8、dicates when the document was last issued. Amendments issued since publication Amd. No. Date Comments 15371 11 October 2004 Change to Clause 2, subclause 3.2 and Clause 4EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 4613-2 August 1995 + A1 June 2004 ICS 83.080.20 English version Plastics
9、Ethylene/vinyl acetate (E/VAC) moulding and extrusion materials Part 2: Preparation of test specimens and determination of properties (includes amendment A1:2004) Plastiques Ethylne/actate de vinyle (E/VAC) pour moulage et extrusion Partie 2: Prparation des prouvettes et dtermination des proprits (i
10、nclut lamendement A1:2004) Kunststoffe Ethylen-Vinylacetat (E/VAC) Formmassen Teil 2: Herstellung von Probekrpern und Bestimmung von Eigenschaften (enthlt nderung A1:2004) This European Standard was approved by CEN on 1995-07-07; and amendment A1 was approved by CEN on 1 June 2004. CEN members are b
11、ound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the
12、 Central Secretarial or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same statu
13、s as the official versions. CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia
14、, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1995 All rights of reproduction and communication in any form and by any means reserved i
15、n all countries to CEN and its members. Ref. No. EN ISO 4613-2:1995 + A1:2004 EXXXXX NE:YYYY B SI 5 Ocebotr Foreword The text of the International Standard ISO 4613-2:1995 has been prepared by Technical Committee ISO/TC 61, Plastics, in collaboration with CEN/TC 249, Plastics. This European Standard
16、 shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 1996, and conflicting national standards shall be withdrawn at the latest by February 1996. According to the CEN/CENELEC Internal Regulations, the following coun
17、tries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Foreword to amendment A1 This document (EN ISO 4613-2:1995/A1:2004)
18、 has been prepared by Technical Committee ISO/TC 61, Plastics, in collaboration with Technical Committee CEN/TC 249, Plastics, the Secretariat of which is held by IBN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsemen
19、t, at the latest by December 2004, and conflicting national standards shall be withdrawn at the latest by December 2004. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium,
20、 Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 4613-2
21、:1995/Amd 1:2004 has been approved by CEN as EN ISO 4613-2:1995/A1:2004 without any modifications. Page2 ENISO46132:1995LANOITANRETNI DRADNATS 0 OSI OSI )E(5991:2=3164 Plastics - Ethylene/vinyl acetate (E/VAC) moulding and extrusion materials - Part 2: Preparation of test specimens and determination
22、 of properties 1 Scope This part of ISO 4613 specifies the methods of prep- aration of test specimens and the test methods to be used in determining the properties of E/VAC moulding and extrusion materials. Requirements for handling test material and for conditioning both the test ma- terial before
23、moulding and the specimens before testing are given here. Procedures and conditions for the preparation of test specimens and procedures for measuring properties of the materials from which these specimens are made are given. Properties and test methods which are suitable and necessary to characteri
24、ze E/VAC moulding and extrusion materials are listed. The properties have been selected from the general test methods in ISO 10350. Other test methods in wide use for or of particular significance to these moulding and extrusion materials are also included in this part of ISO 4613, as are the design
25、atory proper- ties specified in part 1. In Order to obtain reproducible and comparable test results, it is necessary to use the methods of prep- aration and conditioning, the specimen dimensions and the test procedures specified herein Values de- termined will not necessarily be identical to those o
26、btained using specimens of different dimensions or prepared using different procedures. 2 Normative references The following Standards contain provisions which, through reference in this text, constitute provisions of this part of ISO 4613. At the time of publication, the editions indicated were val
27、id. All Standards are subject to revision, and Parties to agreements based on this part of ISO 4613 are encouraged to investigate the possibility of applying the most recent editions of the Standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standard
28、s. ISO 62:1980, Plastics - Determination of water ab- sorp tion. ISO 75-1: 1993, Plastics - Determination of tempera- ture of deflection under load - Part 1: General test method. ISO 75-2: 1993, Plastics - Determination of tempera- ture of deflection under load - Part 2: Plastics and ebonite. ISO 17
29、8: 1993, Plastics - Determination of flexural properties. ISO 179: 1993, Plastics - Determination of Charpy impact strength. ISO 29111977, Plastics - Standard atmospheres for gninoitidnoc dna .gnitset ISO 293:1986, Plastics - Compression moulding test specimens of thermopfastic materiak. Page3 ENISO
30、46132:1995OSI )E(5991:2=3164 0 OSI ISO 527-1 :1993, Plastics - Determination of tensile properties - Part 1: General principles. ISO 527-2: 1993, Plastics - Determination of tensile properties - Part 2: Test conditions for moulding and extrusion plas tics. ISO 527-4: -l 1, Plas tics - Determination
31、of tensile properties - Part 4: Test conditions for isotropic and ortho tropic fibre-rein forced plas tic composites. ISO 899-1: 1993, Plastics - Determination of creep behaviour - Part 1: Tensile creep. ISO 1133:1991, Plastics - Determination of the melt mass-flow rate (MFR) and the melt volume-flo
32、w rate (M VR) of thermoplas tics. ISO 1183:1987, Plastics - Me thods for determining the density and relative density of non-cellular plas tics. ISO 1210:1992, Plastics - Determination of the burning behaviour of horizontal and vertical specimens in contact with a small-flame ignition Source. ISO 16
33、28-3:1991, Plastics - Determination of vis- cosity number and limiting viscosity number - Part 3: Polyethylenes and polypropylenes. ISO 2818:1994, Plastics - Prepara tion of test speci- mens by machining. ISO 3146:1985, Plastics - Determination of melting behaviour (melting temperature or melting ra
34、nge) of semi-crystalline polymers. ISO 3167:1993, Plastics - Multipurpose test speci- mens. ISO 4589-2: -l 1, Plas tics - Determination of burning behaviour by Oxygen index - Part 2: Ambient- temperature test. ISO 4613-1: 1993, Plastics - Ethylene/vinyl acetate (E/vAC) moulding and extrusion materia
35、ls - Part 7: Designa tion and specifica tion. ISO 8256: 1990, Plastics - Determination of tensile- Impact strength. ISO 8985: 1989, Plastics - Ethylene/vinyl acetate copolymer (E/vAC) thermoplas tics - Determination of Vinyl acetate content. ISO 10350: 1993, Plastics - Acquisition and presen- ta tio
36、n of comparable Single-poin t da ta. IEC 93:1980, Methods of test for volume resistivity and surface resistivity of solid electrical insulating ma terials. IEC 112: 1979, Method for determining the compara- tive and the proof tracking indices of solid insulating ma terials under moist conditions. IE
37、C 243-1: 1988, Methods of test for electric strength o f solid insula ting ma terials - Part 1: Tests at po wer frequencies. IEC 250: 1969, Recommended methods for the deter- mination of the permittivity and dielectric dissipation factor of electrical insulating materials at power, audio and radio f
38、requencies including metre wavelengths. IEC 296: 1982, Specification for unused mineral insu- lating oils for transformers and switchgear. 3 Preparation of test specimens Test specimens shall be prepared by compression moulding. lt is essential that the specimens are always prepared by the same proc
39、edure using the Same processing conditions. The material shall be kept in moisture-proof until it is required for use. Containers Moisture content of filled or reinforced materials shall be expressed as a percentage of the total mass of the compound. 3.1 Treatment of the material before moulding Bef
40、ore processing, no pretreatment Sample is normally necessary. 3.2 Compression moulding of the material Compression-moulded sheets shall be prepared in accordance with ISO 293, using the conditions speci- fied in table 1. The test specimens required for the determination of the properties shall be ma
41、chined from the compression-moulded sheets in accordance with ISO 2818 or stamped. 1) To be published. 2 SITIRBDRADNATS H SB EN OSI -31545991:2 W h e n u s i n g a p o s i t i v e ( t y p e 2 ) m o u l d , a p r e s s u r e o f a b o u t 5 MPa to 10 MPa shall be applies to the material. Test psceemi
42、ns slahoc eb lidnoitden ofr ael tast 81 32 ta h C 2 C. Theresi no rqeurime tneofr ihts ot beod en a taraptiucralr elaitevmuh idyti. ISB XX XXXXX 4002 Page4 ENISO46132:19950 OSI A type 1 (frame) mould may be used, but it is necessary to Start cooling whilst simultaneously ap- plying the full pressure
43、. This avoids the melt being pressed out of the frame and avoids sink marks. For thicker sheet (- 4 mm), a type 2 (positive) mould has been found to work satisfactorily. The preheating time depends on the type of mould and the energy input (steam, electricity). For frame moulds, 5 min is usually suf
44、ficient, but for positive moulds, due to the bigger mass, a preheating time of 5 min to 15 min tan be necessary, especially if electric heating is used. 4 Conditioning of test specimens Test snemiceps llahs eb denoitidnoc ni ecnadrocca with OSI 192 rof ta tsael 04 h ta 32 “C + 2 “C dna - (50 k 5) %
45、relative humidity. ISO 461302:1995(E) 5 Determination of properties In the determination of properties and the presen- tation of data, the Standards, supplementary in- structions and notes given in ISO 10350 shall be applied. All tests shall be carried out in the Standard atmosphere of 23 “C + 2 “C
46、and (50 t: 5) % relative humidity unless specifically stated otherwise in tables 2 and 3. Table 2 is compiled from ISO 10350, and the proper- ties listed are those which are appropriate to E/VAC moulding and extrusion materials. These properties are those considered useful for comparisons of data ge
47、nerated for different thermoplastics. Table3 contains those properties, not found specifi- cally in table 2, which are in wide use or of particular significance in the practical characterization of E/VAC moulding and extrusion materials. Table 1 - Conditions for compression moulding of test specimen
48、s Material 6 10 % Vinyl acetate IO % Vinyl acetate Moulding Average Full- cooling Demoulding Full pressure Preheating temperature Preheating rate temperature pressure time pressure time “C “C/min “C MPa min MPa min 155 15 40 20 5+1 - Contact 5to15 125 15 40 IO 5+1 - Contact 5to15 3 SITIRBDRADNATS H SB EN OSI -31545991:2 When using a positive (type 2) mould, a pressure of baout 5 PMot a M 01Pa slahb le palpsei ot eht tamerila. Test psceemins slahoc eb lidnoitden ofr ael tast 81 32 ta h C 2 C. Theresi no rqeurime tneofr ihts ot beod en a taraptiucralr elaitevmuh idyti. ISB XX XXXXX 2004 ITIS
