1、中华人民共和国国家标准蒸锢酒及配制酒卫生标准的分析方法也1etbodfor analysis of byglenic standard 。fdistilled wlnes and mlxed wlnes 1 主题内容与适用范围GB/T 5009.48-1996 代替GB5009. 48-85 本标准规定了以含糖或淀粉的物质为原料，经糖化发酵蒸馆而制得的白酒及以发酵酒或蒸馆酒作酒基，经添加可食用的辅料制成的配制酒中各项卫生指标的分析方法。本标准适用于蒸饱酒和配制酒中各项卫生指标的分析.2 引用标准GB 2757 蒸馆酒和配制酒卫生标准GB 5009.2 食品中相对密度的测定方法GB/T 5009
2、. 11 食品中总呻的测定方法GB/T 5009.12 食品中铅的测定方法GB/T 5009.35 食品中着色剂的测定方法GI:I/T 5009. 36 粮食卫生标准的分析方法GB 12396 食品中铁、镜的原子吸收测定方法3 感官检查3. 1 量取30时，样品，倒入50mL清洁干燥无色玻璃烧杯中，观察其颜色，应透明，无沉淀或杂质。3. 2 尝其味应有该种酒特有的芳香昧和滋味，不应有霉昧、酸味、异味。应符合GB2757的规定。4 理化检验4. 1 乙醇浓度比重计法4. 1. 1 原理同GB5009.2的原理。4.1.2 仪器酒精比重汁。4. 1. 3 分析步骤吸取100mL样品于250mL或5
3、00mL全玻璃蒸馆器中，加50mL水，再加入玻璃珠数粒，蒸筒，用100mL容量瓶收集馆出液100mL。将蒸馆后的样品倒入量筒中，将洗净擦干的酒精计缓缓沉入量筒中，静止后再轻轻按下少许，待其上升静止后，从水平位置观察其与液面相交处的刻度，为乙醇浓度，同时测定温度，按测定的温度与浓度，查酒精计温度浓度换算表).换算成温度为20C时的乙醇浓度(%)。4.2 甲醇中华人民共和国卫生部1996-06-19批准1996-09-01实施603 GB!T 5009.48-1996 4.2.1 原理甲醇经氧化成甲醒后，与品红亚硫酸作用生成蓝紫色化合物，与标准系列比较定量。最低检出量为0.02 g!100 mL
4、4.2.2 试剂4. 2. 2. 1 高健酸饵磷酸溶液2称取3g高锺酸饵，加入15mL磷酸(85%)与70mL水的混合液中，溶解后加水至100mL.贮于棕色瓶内，防止氧化力下降，保存时间不宜过长.4.2.2.2 草酸硫酸溶液2称取5g无水草酸(H，C，O.)或7g含2分子结晶水草酸(H，C，O. 2H,O) , 溶于硫酸(1+1)中至100mL。4.2.2.3 品红亚硫酸溶液s称取O.1 g碱性品红研细后，分次加入共60mL 80C的水，边加入水边研磨使其溶解，用滴管吸取上层溶液滤于100mL容量瓶中，冷却后加10mL亚硫酸销溶液(100g/L) , 1 mL盐酸，再加水至刻度，充分混匀，放置
5、过夜，如溶液有颜色，可加少量活性炭搅拌后过滤，贮于棕色瓶中，置暗处保存，溶液呈红色时应弃去重新配制。4.2.2.4 甲醇标准溶液z称取1.000 g甲醇，置于100mL容量瓶中，加水稀释至J度.此溶液每毫升相当于10mg甲醇。置低温保存。4.2.2.5 甲醇标准使用液z吸取10.0mL甲醇标准溶液，置于100mL容量瓶中，加水稀释至J度.再取10.0mL稀释液置于50mL容量瓶中，加水至刻度，该溶液每毫升相当0.50mg甲醇，4.2. 2.6 无甲醇的乙醇溶液z取0.3mL按操作方法检查，不应显色.如显色需进行处理。取300mL乙醇(95%)，加高锺酸侨少许，蒸饵，收集馆出液。在馆出液中加入硝
6、酸银溶液取1g硝酸银溶于少量水中和氢氧化纳榕液(取.5g氢氧化纳溶于少量水中)，摇匀，取上清液蒸馆，弃去最初50mL馆出液，收集中间馆出液约200mL，用酒精比重计测其浓度，然后加水配成无甲醇的乙醉(60%4.2. 2.7 亚硫酸销溶液(100g!L)。4.2.3仪器分光光度计。4.2.4 分析步骤根据样品中乙醇浓度适当取样(乙醇浓度30%，取1.0 mL;40%，取0.8mL , 50%，取0.6mL , 60% ，取0.5mL).置于25mL具塞比色管中.着色或混浊的蒸馆酒和配制酒按4. 3方法处理后再按上述取样体积取祥。吸取0，0.10，0.20，0.40 ,0.60 ,0. 80 ,
7、00 mL甲醇标准使用液(相当0，0.05，0.10，0.20，0.30.0.40.0.50mg甲醇分别置于25mL具塞比色管中，并用元甲醇的乙醇稀释至1.0mL. 于样品管及标准管中各加水至5mL .再依次各加2mL高锺酸饵磷酸溶液，混匀，放置10min , 各加2mL草酸-硫酸溶液，混匀使之褪色，再各加5mL品红-亚硫酸溶液，混匀，于20C以上静置。.5 h.用2cm比色杯，以零管调节零点，于波长590nm处测吸光度，绘制标准曲线比较，或与标准色列目测比较。4.2.5 计算x m1 2芷lT = X 100 . ( 1 ) 式中，X，-一样品中甲醇的含量.g!100mL，m，-一测定样品中
8、甲醇的质量，mgJV，-一样品体积.mL。结果的表述z报告算术平均值的二位有效数.604 GB/T 5009.48-1996 酒精计温度浓度换算表酒精计刁亏值溶液70.0 69.5 69 68.5 68 67.5 67 66.5 66 65. 5 温度温度+20C;时用容量百分数表示乙醇浓度35 65.0 64.5 64.0 63.4 62.9 62.4 61. 9 61. 4 60.9 60.4 34 65.3 64.8 64.3 63.8 63.2 62.7 62.2 61. 7 61. 2 60.7 33 65.7 65. 2 64.6 64. 1 63.6 63. 1 62.6 62.
9、 1 61. 6 61. 1 32 66.0 65.5 65.0 64.4 63.9 63.4 62.9 62.4 61. 9 61. 4 31 66.4 65.9 65.4 64.8 64.3 63.8 63.3 62.8 62.3 61. 8 30 66.7 66.2 65.7 65.2 64.6 64.1 63.6 63. 1 62.6 62. 1 29 67.0 66.5 66.0 65.5 65.0 64.5 64.0 63.4 62.9 62.4 28 67.4 66.8 66.3 65.8 65.3 64.8 64.3 63.8 63.3 62.8 27 67.7 67.2 66
10、.7 66.2 65.7 65.2 64.6 64.1 63.6 63. 1 26 68.0 67.5 67.0 66.5 66.0 65.5 65.0 64.5 64.0 63.5 25 68.4 67.8 67.3 66.8 66.3 65.8 65.3 64.8 64.3 63.8 24 68.7 68.2 67.7 67.2 66.7 66.2 65.6 65. 1 64.6 64. 1 23 69.0 68.5 68.0 67.5 67.0 66.5 66.0 65.5 65.0 64.5 22 69.3 68.8 68.3 67.8 67.3 66.8 爸6.3 65.8 65.3
11、 64.8 21 69.7 69.2 68.7 68.2 67.7 67.2 66.7 66.2 65. 7 65.2 20 70.0 69.5 69.0 68.5 68.0 67.5 67.0 66.5 66.0 65. 5 19 70.3 69.8 69.3 68.8 68.3 67.8 67.3 66.8 66.3 65.8 18 70.6 70.2 69.6 69.2 68.7 68.2 67.7 67.2 66.7 66.2 17 71. 0 70.5 70.0 69.5 69.0 68.5 68.0 67.5 67.0 66.5 16 71. 3 70.8 70.3 69.8 69
12、.3 68.8 68.3 67.8 67.3 66.8 15 71. 6 71. 1 70.6 70.1 69.6 69. 1 68.6 68.2 67.7 67.2 14 72.0 71. 4 71. 0 70.5 70.0 69.5 69.0 68.5 68.0 67.5 13 72.3 71. 8 71. 3 70.8 70.3 69.8 69.3 68.8 68.3 67.8 12 72.6 72.1 71. 6 71. 1 70.6 70.1 69.6 69.2 68.7 68.2 11 72.9 72.4 71. 9 71. 4 71. 0 70.5 70.0 69.5 69.0
13、68.5 10 73. 2 72.7 72.2 71. 8 71. 3 70.8 70.3 69.8 69.3 68.8 605 GB/T 5009. 48-1996 续表酒精it 刁亏值溶液温度65 64. 5 64 63.5 63 62. 5 62 61. 5 61 60.5 温度斗20.C时用容量百分数表示乙醇浓度35 59.9 59.4 58.9 58.4 57.8 57.2 56.7 56.2 55.8 55.2 34 60叼259. 7 59.2 58.6 58.1 57.6 57. 1 56.6 56. 1 55. 6 33 60.6 60. 1 59.6 59.0 58.5 5
14、8.0 57.4 57.0 56.5 55 , 9 32 60 , 9 60, 4 59.9 59.4 58. 8 58.3 57.8 57 , 3 56.8 56.2 31 61. 3 60.8 60.3 59.8 59.2 58.6 58.1 57.6 57.2 56.6 30 61. 6 61. 1 60, 6 60.0 59. 5 59.0 58.5 58.0 57 , 5 57.0 29 61. 9 61. 4 60.9 60.4 59.9 59.4 58.8 58.3 57.8 57.3 28 62 , 3 61. 8 61. 2 60.7 60, 2 59 , 7 59.2 58
15、.7 58.2 57.7 27 62.6 62. 1 61. 6 61. 1 60 , 6 60. 1 59.6 59 , 0 58. 5 58.0 26 63.0 62.4 61. 9 61. 4 60.9 60, 4 59 , 9 59 , 4 58 , 9 58.4 25 63.3 62.8 62.3 61. 8 61. 3 60, 8 60.3 59.8 59.2 58.7 24 63.6 63. 1 62.6 62, 1 61 , 6 61. 1 60, 6 60 , 1 59 , 6 59 , 1 23 64.0 63. 5 63.0 62.5 62 , 0 61. 5 61. 0
16、 60.4 60, 0 59 , 4 22 64 , 3 63.8 63.3 62 , 8 62, 3 61. 8 61. 3 60, 8 60 , 3 59 , 8 21 64.6 64.2 63.6 63.2 62.6 62.2 61. 6 61. 2 60.6 60.1 20 65.0 64. 5 64 , 0 63.5 63 , 0 62, 5 62.0 61. 5 61. 0 60.5 19 65.3 64.8 64.3 63 , 8 63.3 62 , 8 62 , 3 61. 8 61. 3 60.8 18 65.7 65.2 64.7 64.2 63.7 63.2 62.7 6
17、2. 2 61. 7 61. 2 17 66.0 65 , 5 65 , 0 64.5 64.0 63.5 63.0 62.5 62.0 61. 5 16 66.3 65.8 65.4 64.8 64.4 63.9 63.4 62.9 62.4 61. 9 15 66.7 66 , 2 65 , 7 65 , 2 64 , 7 64.2 63.7 63.2 62 , 7 62.2 14 67.0 66.5 , I 66. 0 65.5 65.0 64.6 64. 1 63.6 63. 1 62.6 13 67 , 4 66.8 66 , 4 65. 9 65 , 4 64, 9 64 , 4
18、63 , 9 63 , 4 62 , 9 12 67.7 67.2 66. 7 66 , 2 65.7 65.2 64.7 64 , 2 63.8 63 , 3 II 68 , 0 67 , 5 67, 0 66 , 5 66 , 0 65. 6 65 , 1 64 , 6 64 , 1 63 , 6 10 68.3 67. 8 67.4 66.9 66.4 65 , 9 65 , 4 64.9 64 , 4 63.9 606 GB/T 5009.48-1996 续表酒精计刁飞值榕液温度60 5. 5 5 58.5 58 57.5 57 56.5 56 55.5 温度+20C时用容量百分数表示
19、乙醇浓度35 54.6 54. 1 53.6 53. 1 52.6 52. 1 51. 6 51. 0 50.5 50.0 34 55.0 54.5 54.0 53.5 53.0 52.4 51. 9 51. 4 50.8 50.3 33 55.3 54.8 54. 3 53.8 53.3 52.8 52.3 51. 8 51. 2 50. 7 32 55.7 55.2 54.7 54.2 53.7 53.2 52.7 52.2 51. 6 51. 1 31 56.1 55.5 55.0 54.5 54.0 53.5 53.0 52.4 51. 9 51. 4 30 56.4 55.9 55.
20、4 54.9 54.4 53.9 53.4 52. 9 52.3 51. 8 29 56.8 56.3 55.8 55.3 54.8 54.2 53.7 53.2 52.7 52.2 28 57.2 56.6 56. 1 55.6 55. 1 54.6 54. 1 53.6 53. 1 52. 6 27 57.5 57.0 56.5 56.0 55.5 55.0 54.5 54.0 53. 4 52.9 26 57.9 57.4 56.9 56.4 55. 8 55. 3 54.8 54.3 53.8 53. 3 25 58.2 57.7 57.2 56.7 56.2 55.7 55.2 54
21、.7 54.2 53.7 24 58.6 58. 1 57.6 57. 1 56. 6 56. 1 55.6 55. 0 54. 5 54.0 23 58.9 58.4 57.9 57.4 56. 9 56.4 55.9 55.4 54.9 54.4 22 59.3 58.8 58.3 57.8 57.3 56.8 56.3 55. 8 55. 3 54.8 21 59. 6 59.1 58.6 58. 1 57. 6 57. 1 56.6 56. 1 55.6 55. 1 20 60.0 59.5 59.0 58.5 58. 0 57.5 57.0 56.5 56.0 55.5 19 60.
22、4 59.8 59.4 58.8 58.4 57.8 57.4 56. 9 56.4 55.9 18 60.7 60.2 59.7 59.2 58. 7 58.2 57.7 57.2 56.7 56.2 17 61. 0 60.5 60.0 59.6 59. 1 58.6 58. 1 57.6 57. 1 56.6 16 61. 4 60.9 60.4 59.9 59.4 58.9 58.4 57.9 57.4 56. 9 15 61. 7 61. 2 60.8 60.2 59.8 59.3 58.8 58.3 57.8 57.3 14 62町I61. 6 61. 1 60.6 60. 1 5
23、9.6 59. 1 58.6 58.2 57. 7 13 62.4 61. 9 61.4 61. 1 60.5 60.0 59.5 59.0 58.5 58.0 12 62.8 62.3 61. 8 61. 3 60.8 60.3 59.8 59.4 58.9 58.4 II 63. 1 62.6 62. 1 61. 6 61. 2 60. 7 60.2 59.7 59.2 58. 7 10 63.5 63.0 62.5 62.0 61. 5 61. 0 60.5 60.0 59.6 59. 1 607 GB/T 5009.48-1996 续表酒精计刁飞值溶液54.5 54 53.5 53 5
24、2.5 52 51. 5 51 50.5 55 温度温度+20C时用容量百分数表示乙醇浓度35 49.5 49.0 48.5 48.0 47.4 46.8 46.3 45.8 45.3 44.8 34 49.8 49.3 48.8 48.3 47.8 47.2 46.7 46.2 45.7 45.2 33 50.2 49.7 49.2 48.7 48.2 47.6 47.1 46.6 46.1 45.6 32 50.6 50. 1 49.6 49.0 48.5 48.0 47.4 46.9 46.4 45.9 31 50.9 50.4 49.9 49.4 48.9 48.4 47.8 47.3
25、 46.8 46.3 30 51. 3 50.8 50.3 49.8 49.3 48.8 48.2 47.7 47.2 46.7 29 51. 7 51.2 50.7 50.2 49.6 49. 1 48.6 48. 1 47.6 47. 1 28 52. 1 51. 5 51. 0 50.5 50.0 49.5 49.0 48.5 48.0 47.5 27 52.4 51. 9 51. 4 50.9 50. 4 49.9 49.4 48.8 48.3 47.8 26 52.8 52.3 51. 8 51. 3 50.8 50.2 49.7 49.2 48.7 48.2 25 53.2 52.
26、6 52.2 51. 6 51. 1 50.6 50.1 49.6 49.1 48.6 24 53.5 53.0 52.5 52.0 51. 5 51. 0 50.5 50.0 49.5 49.0 23 53.9 53.4 52.9 52.4 51. 9 51. 4 50.9 50.4 49.9 49.4 22 54.3 53.8 53.3 52.8 52.2 51. 8 51. 2 50.7 50.2 49.7 21 54.6 54.1 53.6 53. 1 52. 6 52.1 51. 6 51. 1 50.6 50.1 20 55.0 54.5 54.0 53.5 53.0 52.5 5
27、2.0 51. 5 51.0 50.5 19 55.4 54.9 54.4 53.9 53.4 52.9 52.4 51. 9 51. 4 50.9 18 55.7 55.2 54.7 54.2 53.7 53.2 52.7 52.2 51.7 51. 2 17 56.1 55.6 55. 1 54.6 54.1 53.6 53.1 52.6 52.1 51. 6 16 56.4 56.0 55.5 55.0 54.5 54.0 53.5 53.0 52.5 52.0 15 56.8 56.3 55.8 55.3 54.8 54.4 53.9 53.4 52.9 52.4 14 57.2 56
28、.7 56.2 55.7 55.2 54.7 54.2 53.7 53.2 52.7 13 57.5 57.0 56.5 56.0 55.6 55.1 54.6 54.1 53.6 53. 1 12 57.9 57.4 56.9 56.4 55.9 55.4 55.0 54.5 54.0 53.5 11 58.2 57.7 57.2 56.8 56.3 55.8 55.3 54.8 54.3 53.8 10 58.6 58.1 57.6 57. 1 56.6 56.2 55.7 55.2 54.7 54.2 L一608 GB/T 5009.48一1996续表酒精计习飞值溶液50 4日.5 49
29、 48.5 48 47.5 47 46.5 46 45. 5 温度温度+20(;时用容量百分数表示乙醇浓度35 44.3 43.8 43.3 42.8 42.3 41. 8 41. 2 40.7 40.2 39.6 34 44.7 44.2 43.7 43.2 42.7 42. I 41. 5 41. 0 40.5 40.0 33 45.0 44.6 44. I 43.6 43. I 42.5 41. 9 41. 4 40.9 40.4 32 45.4 44.9 44.4 43.9 43.4 42.8 42.3 41.8 41. 3 40.8 31 45.8 45.3 44.8 44.3 43
30、.8 43.2 42.7 42.2 41.7 41. 2 30 46.2 45.7 45.2 44.7 44.2 43.6 43.1 42.6 42.1 41. 6 29 46.6 46.1 45.6 45.0 44.5 44.0 43.5 43.0 42.5 42.0 28 47.0 46.4 45.9 45.4 44.9 44.4 43.9 43.4 42.9 42.4 27 47.3 46.8 46.3 45.8 45.3 44.8 44.3 43.8 43.3 42.8 26 47.7 47.2 46.7 46.2 45.7 45.2 44.7 44.2 43.7 43.2 25 48
31、.1 47.6 47. I 46.6 46.1 45.6 45.1 44.6 44.1 43.6 24 48.5 48.0 47.5 47.0 46.4 46.0 45.4 44.9 44.4 43.9 23 48.9 48.4 47.8 47.3 46.8 46.3 45.8 45.3 44.8 44.3 22 49.2 48.7 48.2 47.7 47.2 46.7 46.2 45.7 45.2 44.7 21 49.6 49. 1 48.6 48. I 47.6 47.1 46.6 46. 1 45.6 45. I 20 50.0 49.5 49.0 48.5 48.0 47.5 41
32、.0 46.5 46.0 45.5 19 50.4 49.9 49.4 48.9 48.4 47.9 47.4 46.9 46.4 45.9 18 50.7 50.2 49.8 49.3 48.8 48.3 47.8 47.3 46.8 46.3 17 51. 1 50.6 50.1 49.6 49.2 48.7 48.2 47.7 47.2 46.7 16 51. 5 51.0 50.5 50.0 49.5 49.0 48.6 48.0 47.6 47.1 15 51. 9 51. 4 50.9 50.4 49. 9 49.4 48.9 48.4 47.9 47.4 14 52.2 51.
33、8 51. 3 50.8 50.3 49.8 49.3 48.8 48.3 47.8 13 52.6 52. 1 51. 6 51. 2 50.7 50.2 49.7 4日Z 48.7 48.2 12 53.0 52.5 52.0 51. 6 51. 0 50.6 50.1 49.6 49.1 48.6 11 53.4 52.9 52.4 51. 9 51. 4 50.9 50.4 50.0 49.5 49.0 10 53.7 53.2 52.8 52.3 51. 8 51. 3 50.8 50.3 49.8 49.4 609 GB/T 5009.48-1996 续表酒精计E飞值溶液45 44
34、.5 44 43.5 43 42.5 42 41.5 41 40.5 温度温度十20C时用容量百分数表示乙醇浓度35 39.0 38.6 38 , 1 37 , 6 37 , 0 36.5 36.0 35.5 35.0 34 , 5 34 39.5 39 , 0 38.5 38.0 37.4 36 , 9 36.4 35.9 35 , 4 34.9 33 39.9 39.4 38.9 38.4 37.8 37.3 36 , 8 36.3 35.8 35. 3 32 40.3 39.8 39 , 3 38.8 38.2 37.7 37 , 2 36.7 36.2 35 , 7 、31 40.7
35、40.2 39.7 39.2 38.6 38.1 37 , 6 37.1 36.6 36. 1 30 41. 0 40 , 6 40.1 39.5 39.0 38.5 38 , 0 37.5 37.0 36.5 29 41. 5 41. 0 40.4 39.9 39.4 38.9 38.4 37.9 37.4 36 , 9 28 41. 9 41. 4 40.8 40.3 39.8 39.3 38.8 38.3 37.8 37 , 3 27 42.3 41. 8 41. 2 40.7 40, 2 39 , 7 39.2 38.7 38.2 37.7 26 42.7 42 , 2 41. 6 4
36、1. 1 40.6 40.1 39.6 39.1 38 , 6 38. 1 25 43 , 0 42 , 5 42.0 41. 5 41.0 40.5 40.0 39.5 39.0 38.5 24 43.4 42.9 42.4 41. 9 41. 4 40.9 40.4 39.9 39.4 38.9 23 43.8 43. 3 42.8 42.3 41. 8 41. 3 40.8 40.3 39 , 8 39.3 22 44.2 43.7 43.2 42 , 7 42.2 41. 7 41. 2 40.7 40.2 39 , 7 21 44 , 6 44.1 43.6 43.1 42.6 42
37、.1 41. 6 41.1 40.6 40 , 1 20 45.0 44.5 44.0 43.5 43.0 42.5 42.0 41. 5 41. 0 40.5 19 45.4 44.9 44.4 43.9 43.4 42.9 42.4 41. 9 41. 4 40 , 9 18 45.8 45.3 44.8 44.3 43.8 43.3 42.8 42 , 3 41. 8 41. 3 17 46.2 45.7 45.2 44.7 44.2 43.7 43.2 42.7 42.2 41. 7 16 46 , 6 46. 1 45.6 45.1 44.6 44.1 43, 6 43.1 42 ,
38、 6 42. 1 15 47 , 0 46.4 46.0 45.5 45.0 44.5 44 , 0 43.5 43 , 0 42.5 14 47.3 46.8 46.4 45 , 8 45.4 44.9 44 , 4 43.9 43 , 4 42.9 13 47.7 47.2 46.7 46.2 45.8 45.3 44.8 44.3 43.8 43 , 3 12 48.1 47.6 47. 1 46.6 46. 1 45.6 45.2 44 , 7 44.2 43 , 7 11 48.5 48.0 47.5 47 , 0 46.5 46.0 45.6 45.1 44.6 44. 1 10
39、48.9 48.4 47.9 47 , 4 46.9 46.4 46.0 45 , 5 45.0 44.5 610 G/T 5009.48-1996 续表洒精计刁亏值熔液39.5 39 38.5 38 37.5 37 36.5 36 35.5 40 温度温度+20t;时用容量百分数表示乙醇浓度35 34.0 33.5 33.0 32.5 32.0 31. 5 31.0 30.5 30.0 29.4 34 34.4 33.9 33.4 32.9 32.4 31. 9 31. 4 30.9 30.4 29.8 33 34.8 34.3 33.8 33.3 32.8 32.3 31. 8 31. 3
40、 30.8 30.2 32 35. 2 34.7 34.2 33.7 33.2 32.7 32.2 &1. 7 31. 2 30.6 31 35.6 35. 1 34.6 34. 1 33.6 33. 1 32.6 32.1 31. 6 31. 0 30 36.0 35.5 35.0 34.5 34.0 33.5 33.0 32.4 32.0 31. 4 29 36.4 35.9 35.4 34.9 34.4 33.9 33.4 32.8 32.3 31. 8 28 36.8 36.3 35.8 35.3 34.8 34.3 33.8 33.2 32.8 32.2 27 37. 2 36.7
41、36.2 35.7 35.2 34.7 34.2 33.7 33.2 32.7 26 37.6 37. 1 36. 6 36. 1 35. 6 35. 1 34.6 34. 1 33.6 33. 1 25 38.0 37.5 37.0 36.5 36.0 35.5 35.0 34.5 34.0 33.5 24 38.4 37.9 37.4 36.9 36.4 35.9 35.4 34.9 34.4 33.9 23 38.8 38.3 37.8 37.3 36.8 36.3 35.8 35.3 34.8 34.3 22 49.2 38.7 38.2 37.7 37.2 36.7 36.2 35.
42、7 35.2 34.7 21 49.6 39. 1 38.6 38.1 37.6 37. 1 36.6 36.1 35.6 35. 1 20 40.0 39.5 39.0 38.5 38.0 37.5 37.0 36.5 36.0 35.5 19 40.4 39.9 39.4 38.9 38.4 37.9 37.4 36.9 36.4 35. 9 18 40.8 40.3 39.8 39.3 38.8 38.3 37.8 37.3 36.8 36.3 17 41. 2 40.7 40.2 39.7 39.2 38.7 38.2 37.7 37.2 36.7 16 41. 6 41. 1 40.
43、6 40.1 39.6 39. 1 38.6 38.1 37.6 37.1 15 42.0 41. 5 41. 0 40.5 40.0 39.5 39.0 38.5 38.0 37.5 14 42.4 41. 9 41. 4 40.9 40.4 39.9 39.4 38.9 38.4 37.9 13 42.8 42.3 41. 8 41. 3 40.8 40.3 39.8 39.3 38.8 38.3 12 43.2 42.7 42.2 4 1. 7 41.2 40.7 40.2 39.7 39.2 38.7 11 43.6 43. 1 42.6 42.1 41. 6 41. 1 40.6 4
44、0.2 39.6 39.2 10 44.0 43.5 43.0 42.5 42.0 41. 6 41. 0 40.6 40.1 39.6 611 GB/T 5009.48-1996 续表1洒精计刁飞值溶液温度35 34.5 34 33.5 33 32.5 32 31. 5 31 30.5 温度+20C时用容量百分数表示乙醇浓度35 28.8 28.3 27.8 27.3 26.8 26.4 26.0 25.5 25.0 24.6 34 29.3 28.8 28.3 27.8 27.3 26.8 26.4 25.9 25.4 25.0 33 29.7 29.2 28.7 28.2 27.7 27
45、.2 26.8 26.3 25.8 25. 4 32 30. 1 29.6 29. J 28.6 28. 1 27.6 27.2 26.7 26.2 31 30.5 30.0 29.5 29.0 28.5 28.0 27.6 27.1 26.6 25.2 30 30.9 30.4 29.9 29.4 28.9 28.4 28.0 27.5 27.0 26.5 29 31. 3 30.8 30.3 29.8 29.4 28.8 28.4 27.9 27.4 26.9 28 31. 7 31. 2 30.7 30.2 29.7 29.2 28.8 28.3 27.8 27 32.2 31. 6 3
46、1. 2 30.6 30.2 29.6 29.2 28.7 28.2 27.7 26 32.6 32.0 31. 6 31.0 30.6 30.0 29.6 29. 1 28.6 28.1 25 33.0 32.5 32.0 31. 5 31. 0 30.5 30.0 29.5 29.0 28.5 24 33.4 32.9 32.4 31. 9 31. 4 30.9 30.4 29.9 29.4 23 33.8 33.3 32.8 32.3 31. 8 31.3 30.8 30.3 29.8 29.3 22 34.2 33.7 33.2 32.7 32.2 31. 7 31.2 30.7 30
47、.2 29.7 21 34.6 34. 1 33.5 33.1 32.5 32.0 31.6 31. 1 30.6 30. 1 20 35.0 34.5 34.0 33.5 33.0 32.5 32.0 31. 5 31. 0 30.5 19 35.4 34.9 34.4 33.9 33.4 32.9 32.4 31.9 31. 4 30. 9 18 35.8 35.3 34.8 34.3 33.8 33.3 32.8 32.3 31. 8 31. 3 17 36.2 35.7 35.2 34.7 34.2 33.7 33.2 32.7 32.2 31. 7 16 36.6 36. 1 35.
48、6 35.1 34.6 34. 1 33.6 33.1 32.6 15 37.0 36.5 36.0 35.5 35.0 34.5 34.0 33.5 33.0 32.5 14 37.4 36.9 36.4 35.9 35.4 35.0 34.4 34.0 33.5 33.0 13 37.8 37.3 36.8 36.4 35.9 35.4 34.9 34.4 33.9 33.4 12 38.2 37.8 37.3 36.8 36.3 35.8 35.3 34.8 34.3 33.8 1J 38.7 38.2 37.7 37.2 36.7 36.2 35.7 35.2 34.7 34.2 10
49、 39. 1 38.6 38.1 37.6 37. 1 36.6 36.1 35.6 35.1 34.6 612 GB/T 5009. 48-1996 续表酒精计部值溶液温度30 29.5 29 28.5 28 21.5 21 26.5 26 25.5 温度+20-C时用容量百分数表示乙醇浓度35 24.2 23.1 23.2 22.8 22.3 21.8 21.3 20.8 20.4 20.0 34 24.5 24.0 23.5 23.1 22.1 22.2 21.1 21. 2 20.8 20.4 33 24.9 24.4 23.9 23.5 23. 1 22.6 22.0 21.6 21. 2 20.8 32 25.3 24.8 24.3 23.8 23.4 22.9 22.4 22.0 21. 6 21. 2 31 25.1 25.2 24.1 24.2 23.8 23.3 22.8 22.4 21.9 21. 4 30 26.1 25.6 25.1 24.6 24.2 23.7 23.2 22.8 22.3 21. 9 29 26.4 26.0 25.5 25.0 24.6 24.1 23.6
