1、Designation: D2065 03 (Reapproved 2017)Standard Test Method forDetermination of Edge Performance of Composite WoodProducts Under Surfactant Accelerated Moisture Stress1This standard is issued under the fixed designation D2065; the number immediately following the designation indicates the year ofori
2、ginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method is intended to serve as a means formeasuremen
3、t of swelling and cracking of the coated oruncoated edge of a composite wood substrate that has beensubjected to wetting by a test solution containing surface activeagent.1.2 The values stated in SI units are to be regarded as thestandard. The values given in parentheses are for informationonly.1.3
4、This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.1.4 This internatio
5、nal standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade (TBT) Commit
6、tee.2. Referenced Documents2.1 ASTM Standards:2D661 Test Method for Evaluating Degree of Cracking ofExterior PaintsE177 Practice for Use of the Terms Precision and Bias inASTM Test MethodsE691 Practice for Conducting an Interlaboratory Study toDetermine the Precision of a Test Method3. Terminology3.
7、1 Definitions of Terms Specific to This Standard:3.1.1 crack rating, na numerical value on a scale from 1to 10, with 10 representing no evidence of cracking of the edge(see Test Method D661).3.1.2 composite wood products, nboards or other struc-tural or decorative materials manufactured from wood fi
8、bers,flakes or strands and various resin binders consolidated underheat, or pressure, or both.4. Summary of Test Method4.1 A surfactant solution is placed in a tray that contains asponge. A preweighed and calipered panel with a coated edgeis placed with the edge in contact with the surfactant satura
9、tedsponge for 2 h. The exposed panel is blotted dry, reweighed,recalipered, and inspected for edge cracking. Percentageweight and thickness changes are calculated and recorded.Edge cracking is rated in accordance with Test Method D661and recorded.5. Significance and Use5.1 This test method provides
10、a measure of the dimensionalstability and integrity of the coated edge of various compositewood products under accelerated moisture stress. It is widelyused as an indicator or predictor of the anticipated performanceof composite wood products during exterior exposure. It maybe used for developmental
11、 evaluation of coatings, substrates, orboth. It may also be useful for quality control or monitoring ofthe production of coated or uncoated composite wood prod-ucts.6. Apparatus6.1 Wide Flat Tray or Pan, suitable to contain the requirednumber of sponges and test boards. The sides must be highenough
12、to safely contain at least 6 mm (14 in.) of solution.6.2 Rack or Holder, suitable to support the required numberof test boards at the nominal 60 angle.6.3 Micrometer or Vernier Caliper, of sufficient capacity forthe board thickness to be measured and capable of 0.1 mmaccuracy.6.4 Balance, with suffi
13、cient capacity (typically 400 g) and0.01 g accuracy.6.5 Suitable Saw, for cutting of samples.1This test method is under the jurisdiction of ASTM Committee D01 on Paintand Related Coatings, Materials, and Applications and is the direct responsibility ofSubcommittee D01.52 on Factory Coated Wood Produ
14、cts.Current edition approved July 1, 2017. Published July 2017. Originally approvedin 1991. Last previous edition approved in 2011 as D2065 03 (2011). DOI:10.1520/D2065-03R17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For
15、 Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationa
16、lly recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.16.6 Common Household Cellulose Sponges, cut to suitable
17、size.7. Materials7.1 A sufficient supply of test solution.7.2 Appropriately identified test boards cut to proper size.8. Hazards8.1 When using saws, wear goggles, dust mask, and useproper machine safeguards to prevent injury.9. Procedure9.1 See Fig. 1.9.2 Make the required test solution.3Pour soluti
18、on into thetray to saturate all sponges, and allow to reach room tempera-ture. A 6-mm (14 -in.) depth of solution in the tray works well.9.3 Cut board specimens to a suitable size.A10.2-cm (4-in.)by 12.7-cm (5-in.) size has been found to be convenient. The10.2-cm (4-in.) dimension should be the coat
19、ed edge. Prepa-ration of triplicate specimens is recommended.9.4 Measure thickness of the samples along the edge to betested. Three measurements at 2.54-cm (1-in.) intervals (Fig. 2)are recommended for a 10.2-cm (4-in.) specimen. Recordresults.9.5 Weigh the samples to the nearest 0.01 g and record.9
20、.6 Place boards in the tray on sponges as noted in Fig. 1.Ifcoated edges are to be tested, note that the sponges must benarrower than the length (nominally 10.2 cm or 4 in.) of thecontacting coated edges to prevent contact of the solution withthe uncoated edges of the samples. Sponges 9.0-cm (3.5-in
21、.)wide have been used successfully. For the same reason, thecoated face of the board must rest against the sponge at a 60angle to prevent contact of the solution with the uncoated backof the board.9.7 The test duration is 2 h.After 2 h, remove the boards andblot the edges dry with paper towels.9.8 O
22、bserve and record changes as follows:9.8.1 Visually inspect the edges for cracks and record thecrack rating in accordance with Test Method D661. Repeat theobservation 48 h later.9.8.2 Remeasure the thickness of the boards at the samespots measured in 4.4. Record the percent change at each spot,9.8.3
23、 Reweigh the boards and record the weight gain andpercent weight gain, and9.8.4 Calculate averages and standard deviations for thepercent thickness change and percent weight gain.10. Precision and Bias10.1 PrecisionAn interlaboratory study of CompositeWood Product surfactant accelerated moisture str
24、ess was con-ducted in accordance with Practice E691 in seven laboratories3Common test solutions such as 1.0 % of an ethoxylated alkylphenol, nonionicwith hydrophile lipophile balance (HLB) of 13.5 is made using warm, (over 120F(49C), distilled, or deionized water. Historically, Triton X-100 has been
25、 used, butwith this revision Turgitol 15-S-9 was used. Refer to McCutcheons Emulsifiers andDetergents, 1996, McCutcheon Publishing Co., 175 Rock Rd., Glen Rock, NJ07452.FIG. 1 Test Apparatus Side ViewFIG. 2 Specimen DimensionsD2065 03 (2017)2with five materials, with each laboratory obtaining six te
26、stresults for each material (see Table 1).10.1.1 The terms repeatability limit and reproducibilitylimit in Table 1 are used as specified in Practice E177.10.2 BiasSince there is no accepted reference material,method, or laboratory suitable for determining the bias for theprocedure in this test metho
27、d, no statement on bias is beingmade.11. Keywords11.1 accelerated moisture stress; detergent test; wood orcomposite-woodASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are express
28、ly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,
29、either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may att
30、end. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States.
31、Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secu
32、red from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Interlaboratory StudyMaterial AverageRepeatablility,StandardDeviation, SrReproducibility,StandardDeviation, SRRepeatabilityLimit, YReproducibilityLimit, RA 12.8886 2.0878 5.8050 5.8458 16.2540B 9.7200 0.6498 3.5835 1.8195 10.0338C 16.8257 2.1491 7.4174 6.0175 20.7688D 9.1943 2.0814 6.2392 5.8279 17.4696E 14.3286 2.0616 5.4152 5.7724 15.1626F 11.8229 3.7899 6.3353 10.6117 17.7389D2065 03 (2017)3
