1、Designation: A1099/A1099M 17Standard Specification forModified Alloy Steel Forgings, Forged Bar, and Rolled BarCommonly Used in Oil and Gas Pressure Vessels1This standard is issued under the fixed designation A1099/A1099M; the number immediately following the designation indicates theyear of origina
2、l adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of lastreapproval. A superscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This specification covers modified high-strength alloysteel forgin
3、gs and rolled and forged bar for oil and gas pressurevessels and oilfield equipment. See Appendix X1. Oil and gasproduct specifications for which this material is intendedinclude, but are not limited to, the following:1.1.1 API 6A Specification for Wellhead and ChristmasTree Equipment and Errata,1.1
4、.2 API RP 6AR Recommended Practice for Repair andRemanufacture of Wellhead and Christmas Tree Equipment,1.1.3 API 16A Specification for Drill-Through Equipment,1.1.4 API 16R Specification for Marine Drilling RiserCouplings,1.1.5 API 17D Specification for Subsea Wellhead and TreeEquipment and Errata,
5、1.1.6 API 8C Specification for Drilling and ProductionHoisting Equipment.1.2 Supplementary requirements are provided for use whenadditional testing or inspection is desired. These shall applyonly when specified individually by the purchaser in the order.1.3 In the case of conflict between a requirem
6、ent of thisspecification and a requirement of referenced generalspecifications, this specification takes precedence. In the caseof conflict between a requirement of the product specificationor a requirement of this specification and a more stringentrequirement of the purchase order or contract, the
7、purchaseorder or contract take precedence. The purchase order orcontract requirements shall not take precedence if they, in anyway, violate the requirements of the product specification orthis specification, for example, by the waiving of a testrequirement or by making a test requirement less string
8、ent. Inthe case of conflict in terminology between API standards andTerminology A941, Terminology A941 definitions shall beapplied.1.4 UnitsThe values stated in either SI units or inch-pound units are to be regarded separately as standard. Thevalues stated in each system may not be exact equivalents
9、;therefore, each system shall be used independently of the other.Combining values from the two systems may result in noncon-formance with the standard.1.5 This specification is expressed in both inch-pound unitsand in SI units; however, unless the purchase order or contractspecifies the applicable M
10、 specification designation (SI units),the inch-pound units shall apply.1.6 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine th
11、e applica-bility of regulatory limitations prior to use.1.7 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards, Guides and Recom-mendations iss
12、ued by the World Trade Organization TechnicalBarriers to Trade (TBT) Committee.2. Referenced Documents2.1 ASTM Standards:2A370 Test Methods and Definitions for Mechanical Testingof Steel ProductsA388/A388M Practice for Ultrasonic Examination of SteelForgingsA534 Specification for Carburizing Steels
13、for Anti-FrictionBearingsA700 Guide for Packaging, Marking, and Loading Methodsfor Steel Products for ShipmentA788/A788M Specification for Steel Forgings, General Re-quirementsA941 Terminology Relating to Steel, Stainless Steel, RelatedAlloys, and FerroalloysA961/A961M Specification for Common Requi
14、rements for1This specification is under the jurisdiction of ASTM Committee A01 on Steel,Stainless Steel and Related Alloys and is the direct responsibility of SubcommitteeA01.22 on Steel Forgings and Wrought Fittings for Piping Applications and BoltingMaterials for Piping and Special Purpose Applica
15、tions.Current edition approved May 15, 2017. Published May 2017. DOI: 10.1520/A1099_A1099M-17.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document
16、 Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Princ
17、iples for theDevelopment of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.1Steel Flanges, Forged Fittings, Valves, and Parts forPiping ApplicationsA991/A991M Test Method for Conducting TemperatureUniformity Surv
18、eys of Furnaces Used to Heat Treat SteelProductsA1058 Test Methods for Mechanical Testing of SteelProductsMetricE10 Test Method for Brinell Hardness of Metallic MaterialsE21 Test Methods for Elevated Temperature Tension Tests ofMetallic MaterialsE45 Test Methods for Determining the Inclusion Content
19、 ofSteelE110 Test Method for Rockwell and Brinell Hardness ofMetallic Materials by Portable Hardness TestersE112 Test Methods for Determining Average Grain SizeE165/E165M Practice for Liquid Penetrant Examination forGeneral IndustryE381 Method of Macroetch Testing Steel Bars, Billets,Blooms, and For
20、gingsE1444/E1444M Practice for Magnetic Particle TestingE1820 Test Method for Measurement of Fracture Toughness2.2 API Standards:3API 6A Specification for Wellhead and Christmas TreeEquipmentAPI RP 6AR Recommended Practice for Repair and Re-manufacture of Wellhead and Christmas Tree EquipmentAPI 8C
21、Specification for Drilling and Production HoistingEquipmentAPI 16A Specification for Drill-Through EquipmentAPI 16R Specification for Marine Drilling Riser CouplingsAPI 17D Specification for Subsea Wellhead and Tree Equip-mentAPI RP 6HT Heat Treatment and Testing of Large Cross-Section and Critical
22、Section Components2.3 ASNT Standard:4ANST SNT-TC-1A Topical Outlines for Qualification ofNondestructive Testing Personnel2.4 SAE Standards:5AMS 2750 PyrometryAMS-H-6875 Process for Heat Treatment of Steel2.5 ISO Standard:6ISO 6506 Metallic MaterialsBrinell Hardness TestPart1: Test Method2.6 Norsok S
23、tandard:7Norsok M-650 Qualification of Manufacturers of SpecialMaterials2.7 British Standard:8BS 7448-1 Method for Determination of KIc, Critical CTODand Critical J Values of Metallic Materials3. Ordering Information and General Requirements3.1 General:3.1.1 Quantity (mass), length, or number of pie
24、ces;3.1.2 Name of material (forgings or rolled or forged bar);3.1.3 ASTM International specification designation andyear date to which the product is to be furnished and certifiedas meeting or as capable of meeting;3.1.4 Condition (as forged, as rolled, annealed, normalized,normalized, re-austenitiz
25、ed, liquid quenched and tempered,austenitized, and liquid quenched and tempered);3.1.5 Grade, class, and type designations;3.1.6 Dimensions;3.1.7 Shape and finish characteristics;3.1.8 Test location, a drawing or sketch may be used toshow test locations, when applicable;3.1.9 American Petroleum Inst
26、itute (API) productspecification, when applicable; and3.1.10 Any supplementary requirements.3.2 Material supplied to this specification shall conform tothe requirements of Specifications A961/A961M or A788/A788M, which outline additional ordering information, manu-facturing requirements, testing and
27、 retesting methods andprocedures, marking, certification, product analysis variations,and additional supplementary requirements. SpecificationA961/A961M shall apply to bar and forged bar as defined inSpecification A961/A961M and Specification A788/A788Mshall apply to forgings and forged bar unless o
28、therwise stated.4. Melting4.1 In addition to the melting and forging requirements ofSpecifications A961/A961M and A788/A788M, which may besupplemented by supplementary requirements, the followingconditions apply:4.1.1 Material shall be produced by electric arc furnace orinduction melting, followed b
29、y a secondary process includingladle refining and degassing, for example, argon oxygendecarburization (AOD), vacuum oxygen decarburization(VOD) or vacuum arc degassing (VAD), vacuum tankdegassing, and RH (Ruhstahl Heraeus) or DH (Dortmund-Horde) degassing. Material may be secondarily remelted byvacu
30、um arc remelting (VAR) or electroslag remelting (ESR).4.1.2 Material shall be fully killed.4.1.3 Material shall meet the fine austenitic grain sizerequirements as stated in 9.1.1.1.5. Hot Working5.1 The total hot work reduction ratio shall be 4:1 mini-mum.5.1.1 Total hot work reduction ratio for bar
31、s:5.1.1.1 The cross-sectional area of the original ingot orstrand divided by the cross-sectional area of the finished bar.3Available from American Petroleum Institute (API), 1220 L. St., NW,Washington, DC 20005-4070, http:/www.api.org.4Available fromAmerican Society for Nondestructive Testing (ASNT)
32、, P.O. Box28518, 1711 Arlingate Ln., Columbus, OH 43228-0518, http:/www.asnt.org.5Available from SAE International (SAE), 400 Commonwealth Dr., Warrendale,PA 15096, http:/www.sae.org.6Available from International Organization for Standardization (ISO), ISOCentral Secretariat, BIBC II, Chemin de Blan
33、donnet 8, CP 401, 1214 Vernier,Geneva, Switzerland, http:/www.iso.org.7Available from the Norsk Sokkels Konkuranseposisjon, www.standard.no.8Available from British Standards Institution (BSI), 389 Chiswick High Rd.,London W4 4AL, U.K., http:/.A1099/A1099M 1725.1.1.2 The cross-section resulting in th
34、e lowest hot workreduction ratio shall be used.5.1.2 Total hot work ratio for forgings (forging reductionratio):5.1.2.1 The product of the reduction ratios for each hot workoperation including the original starting material reduction andeach subsequent hot work operation. When the cross section ofth
35、e starting material or forged part varies, the cross sectionresulting in the lowest calculated hot work reduction ratio shallbe used.5.2 Forgings shall have a surface finish adequate for in-tended inspection as stated in Specification A788/A788M.6. Heat Treatment6.1 When a heat-treated condition is
36、not specified, any heattreatment shall be at the option of the manufacturer.6.2 When the heat-treated condition is specified, the follow-ing apply:6.2.1 Forgings and bars shall be normalized, re-austenitizedfollowed by liquid quench and temper or alternatively,austenitized, followed by liquid quench
37、 and tempered.6.2.2 Forgings and bars shall be allowed to cool down to atemperature below 200C 400F before commencing anyoperation of heat treatment cycle. This includes before anormalizing cycle.6.2.3 Forgings shall be near net shape before quenching.The rough machine dimensions (or near net shape
38、forgingdimensions) before quenching shall comply with the purchas-ers near net shape drawings. When drawings are not available,the forging supplier shall adhere as close as possible to therecommended practices of API RP 6HT. When no drawings orinstructions are provided by the purchaser, it is the re
39、sponsi-bility of the manufacturer to meet the required mechanicalproperties.6.3 Heat treatment equipment calibration and furnace sur-veys shall be in accordance with API 6A Annex M or API 16AAnnex A. Alternatively, heat treatment equipment survey andcalibration may be performed in accordance with an
40、 interna-tionally recognized industry standard such as SAE AMS 2750,SAE-H-AMS 6875, Test Method A991/A991M (uniformitysurvey), or Norsok M650 provided that the supplier demon-strates that the requirements of API 6A or API 16A have beenexceeded. Induction heating equipment survey and calibrationshall
41、 be in accordance with the manufacturers written proce-dures.6.4 Heat treatment of bars, forgings, and forged bars shall beperformed in a furnace meeting the requirements of 6.3. SeeAPI RP 6HT for additional guidance.6.5 The heat treatment temperatures shall be in accordancewith Table 1.TABLE 1 Heat
42、 Treatment TemperaturesMaterial NormalizingAAustenitizingAQuench Media Tempering MinimumBF22OF Class 75 16751750F900950C16501725F900950CWater/polymer/oil 1225F650CF22OF Class 80 16751750F900950C16501725F900950CWater/polymer/oil 1200F650CF22OF Class 85 16751750F900950C16501725F900950CWater/polymer/oi
43、l 1175F625CF22OFA Class 105 16751750F900950C16501725F900950CWater/polymer/oil 1100F600C4130OF Class 60 16001700F875925C15751650F850900CWater/polymer/oil 1250F675C4130OF Class 75 16001700F875925C15751650F850900CWater/polymer/oil 1200F650C4130OF Class 80 16001700F875925C15751650F850900CWater/polymer/o
44、il 1200F650C4130OF Class 95 16001700F875925C15751650F850900CWater/polymer/oil 1125F600C4130OF Class 110 16001700F875925C15751650F850900CWater/polymer/oil 1075F575C4130OF Class 125 16001700F875925C15751650F850900CWater/polymer/oil 1050F575C8630OF Class 75 16001700F875925C15751650F850900CWater/polymer
45、/oil 1225F650C8630OF Class 80 16001700F875925C15751650F850900CWater/polymer/oil 1200F650C8630OF Class 85 16001700F875925C15751650F850900CWater/polymer/oil 1200F650C8630OF Class 95 16001700F875925C15751650F850900CWater/polymer/oil 1075F575C8630OF Class 100 16001700F875925C15751650F850900CWater/polyme
46、r/oil 1075F575C8630OF Class 110 16001700F875925C15751650F850900CWater/polymer/oil 1050F575C8630OF Class 120 16001700F875925C15751650F850900CWater/polymer/oil 1050F575C8630OF Class 135 16001700F875925C15751650F857.2898.8CWater/polymer/oil 1025F550CATemperature uniformity shall be 25F 14C for normaliz
47、ing and austenitizing.BTemperature uniformity shall be 15F 8C for tempering.A1099/A1099M 1737. Chemical Composition7.1 Heat AnalysisThe heat analysis as determined by thesteel producer as being representative of a heat of steel (seeTerminology A941) meeting the composition of a grade shownin Table 2
48、. Additions of nonspecified elements are not allowed.7.2 Product AnalysisThe manufacturer shall perform aproduct analysis in accordance with Specifications A961/A961M or A788/A788M from a bar, forged bar, or forgingrepresenting each heat. The permissible variations shall meetthose in Specifications A961/A961M or A788/A788M,asapplicable.7.3 For multiple-heat ingots, either individual heat analysesor a weighted average may be taken. The results of the methodused shall conform to the requirements of the product specifi-cation. Annex A2 in
