1、ASD STANDARD NORME ASD ASD NORM prEN 4800-007 Edition P 1 September 2009 PUBLISHED BY THE AEROSPACE AND DEFENCE INDUSTRIES ASSOCIATION OF EUROPE - STANDARDIZATIONAvenue de Tervuren, 270 - B-1150 Brussels - Tel. + 32 2 775 8126 - Fax. + 32 2 775 8131 - www.asd-stan.orgICS: Descriptors: ENGLISH VERSIO
2、N Aerospace series Titanium and titanium alloys Technical specification Part 007: Remelting stock Srie arospatiale Titane et alliages de titane Spcification technique Partie 007 : Produits pour refusion Luft- und Raumfahrt Titan und Titanlegierungen Kneterzeugnisse Technische Lieferbedingungen Teil
3、007: Vormaterial This “Aerospace Series“ Prestandard has been drawn up under the responsibility of ASD-STAN (The AeroSpace and Defence Industries Association of Europe - Standardization). It is published for the needs of the European Aerospace Industry. It has been technically approved by the expert
4、s of the concerned Domain following member comments. Subsequent to the publication of this Prestandard, the technical content shall not be changed to an extent that interchangeability is affected, physically or functionally, without re-identification of the standard. After examination and review by
5、users and formal agreement of ASD-STAN, it will be submitted as a draft European Standard (prEN) to CEN (European Committee for Standardization) for formal vote and transformation to full European Standard (EN). The CEN national members have then to implement the EN at national level by giving the E
6、N the status of a national standard and by withdrawing any national standards conflicting with the EN. Edition approved for publication 30 September 2009 Comments should be sent within six months after the date of publication to ASD-STAN Metallic Material Domain Copyright 2009 by ASD-STAN prEN 4800-
7、007:2009 (E) 2 Contents Page Foreword2 Introduction .3 1 Scope 3 2 Normative references 3 3 Terms and definitions .4 4 Wording of order4 5 Health and safety .5 6 Technical requirements 5 Foreword This standard was reviewed by the Domain Technical Coordinator of ASD-STANs Metallic Material Domain. Af
8、ter inquiries and votes carried out in accordance with the rules of ASD-STAN defined in ASD-STANs General Process Manual, this standard has received approval for Publication. prEN 4800-007:2009 (E) 3 Introduction This standard is part of the series of EN metallic material standards for aerospace app
9、lications. The general organization of this series is described in EN 4258. 1 Scope This standard defines the requirements for the ordering, manufacture, testing, inspection and delivery of titanium and titanium alloy remelting stock. It shall be applied when referred to and in conjunction with the
10、EN material standard unless otherwise specified on the drawing, order or inspection schedule. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edi
11、tion of the referenced document (including any amendments) applies. EN 2002-001, Aerospace series Metallic materials Test methods Part 001: Tensile testing at ambient temperature EN 2002-002, Aerospace series Metallic materials Test methods Part 002: Tensile testing at elevated temperature EN 2002-0
12、05, Aerospace series Test methods for metallic materials Part 005: Uninterrupted creep and stress-rupture testing EN 2032-1, Aerospace series Metallic materials Part 1: Conventional designation. EN 2032-2, Aerospace series Metallic materials Part 2: Coding of metallurgical condition in delivery cond
13、ition. EN 2078, Aerospace series Metallic materials Manufacturing schedule, inspection schedule, inspection and test report Definition, general principles, preparation and approval. EN 2955, Aerospace series Recycling of titanium and titanium alloy scrap EN 3238, Aerospace series Metallic materials
14、Test method Shear test for wires and rivets 1)EN 3976, Aerospace series Titanium and titanium alloys Test method Chemical analysis for the determination of hydrogen content EN 4258, Aerospace series Metallic materials General organization of standardization Links between types of EN standards and th
15、eir use EN 4259, Aerospace series Metallic materials Definition of general terms 1)EN 9100, Aerospace series Quality management systems Requirements (based on ISO 9001:2000) and Quality systems Model for quality assurance in design, development, production, installation and servicing (based on ISO 9
16、001:1994) 1) Published as ASD-STAN Prestandard at the date of publication of this standard. prEN 4800-007:2009 (E) 4 EN 9133, Aerospace series Quality management systems Qualification Procedure for aerospace standard parts TR 2410, Aerospace series Metallic materials Relationship between dimensional
17、 standards and material standards 2)AMS 2750, Pyrometry 3)3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 4259 and the following apply. 3.1 melt a mass of homogeneous liquid metal from a single charge 3.2 remelt solid metal resulting from a single mel
18、t 3.3 parent cast a cast of remelting stock to be used for the production of castings 3.4 remelting stock metal supplied in cast or wrought form, the composition of which has been established by chemical analysis 4 Wording of order The order shall clearly indicate: quantities to be supplied; dates o
19、f delivery; material standard number; delivery condition and metallurgical code of products; dimensions and tolerances or reference to an appropriate dimensional standard; product designation, when required; forwarding address; nature and type of packing, if required; definition and frequency of any
20、 special tests and their retest procedures, if required. 2) Published as ASD-STAN Technical Report at the date of publication of this standard. 3) Published by: American Society for Testing and Materials (ASTM), 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA, 19428-2959 USA. prEN 4800-007
21、:2009 (E) 5 5 Health and safety Products in the delivery condition shall fulfil the health and safety laws of the area of the country when and where it is to be delivered. A product safety data sheet shall be available. 6 Technical requirements 6.1 General The product shall be manufactured in accord
22、ance with the requirements of the relevant material standard and the applicable requirements of this specification. A manufacturing schedule shall be established and applied in accordance with EN 2078. Product shall satisfy the requirements of the material standard and/or order and shall be free fro
23、m irregularities prejudicial to the subsequent manufacture or use of this product. Not with standing previous acceptance complying with this material standard, any product that is found, at a later stage, to contain such defects shall be rejected. Unless otherwise specified, the requirements in Tabl
24、es 1 and 2 shall apply in conjunction with those of the relevant material standard. Table 1 relates to lines 1 to 29 (inclusive) of the material standard and Table 2 relates to lines 30 onwards in which the sub-line format is also used. Lines 2 to 98 may also be opened in line 100 if the material st
25、andard details specific qualification requirements. If a specific line number is not shown in Tables 1 and 2, the requirement is stated in the material standard and/or order. The requirements of the order and/or material standard shall over-ride the requirements of the technical specification. 6.2 Q
26、ualification requirements Qualification requirements when invoked by the material standard and/or order are detailed in Tables 1 and 2. Unless otherwise agreed between the manufacturer and purchaser the qualification phase shall be run on the first 3 batches. 6.3 Release requirements 6.3.1 Release t
27、ests Release testing shall be the responsibility of the manufacturer. The purchaser reserves the right to perform any of the inspections and/or tests required by the material standard and/or order. The test samples shall be representative of the product. When required the manufacturer shall inform t
28、he purchaser of the planned dates for extraction of samples and release testing in order that these operations may be witnessed. Tables 1 and 2 detail the requirements for each line of the material standard. Unless otherwise specifically requested by the purchaser, a particular inspection and/or tes
29、t for release shall be carried out if corresponding acceptance criteria and/or values are stated in the applicable material standard, but see also in 6.3.5. prEN 4800-007:2009 (E) 6 6.3.2 Retests If the test procedure or test piece preparation is faulty, testing shall be re-applied at the original f
30、requency after rectification of the original cause of failure. When failure cannot be attributed to faulty testing, or test piece preparation, further test samples shall be selected at twice the original frequency from the product, one of which shall be that on which the original results were obtain
31、ed unless already withdrawn by the manufacturer after suitable identification of the cause of failure. If all retest results are satisfactory, the batch shall be accepted. If one or more tests are unsatisfactory, the batch shall be: rejected, or 100 % retested and the conforming products accepted, o
32、r partially or fully re-heat treated if heat treatment can rectify the cause of the failure and tested as a completely new batch except for chemical composition, for which redetermination of hydrogen content is required. No product or test sample shall be re-heat treated more than twice. 6.3.3 Rejec
33、tion Any failure to meet the requirements of the material standard shall be cause for rejection. 6.3.4 Special tests Special tests may be required by the purchaser. In such cases, the nature of the test, method, frequency and technical requirements shall be specified on the order or inspection sched
34、ule and shall be mutually agreed by the manufacturer and purchaser. 6.3.5 Capability clause Where capability clause is invoked and where sufficient statistical evidence exists, the test need not be carried out (unless specifically requested by the purchaser). However, this in no way reduces the obli
35、gations of the manufacturer to fulfil the requirements. If subsequent testing indicates that the product does not comply with the requirements, the batch shall be rejected. If sufficient statistical evidence does not exist, the test shall be carried out at a frequency agreed between the manufacturer
36、 and the purchaser. 6.3.6 Statistical process control Reduction in the extent of release testing, other than that defined in 6.3.5 above, may be negotiated with the purchaser on the basis of appropriate statistical process control and/or statistical data. 6.3.7 Inspection and test report The manufac
37、turer shall furnish, with each delivery, a report conforming to the requirements of EN 2078 stating the following: manufacturers name and address and, if appropriate, identification of the plant; order number; material standard number; delivery condition and metallurgical code of the product; quanti
38、ty and dimensions; prEN 4800-007:2009 (E) 7 manufacturing and inspection schedule reference; cast and batch number; batch and/or test samples heat treatment conditions; results of the tests and retests if any. 6.4 Traceability Each product shall be traceable to the cast, production batch and/or heat
39、 treatment batch at all stages of manufacture, testing and delivery. prEN 4800-007:2009 (E) 8 Table 1 Technical requirements for lines 1 to 29, where appropriate Frequency of testing Material standard line reference No Title Requirements Qualification Release 1 Material designation See EN 2032-1. Th
40、e test samples used for chemical analysis shall be representative of the product and shall be taken from each melt or cast. The method of chemical analysis shall be at the discretion of the manufacturer unless otherwise stated in the material standard or order. In cases of dispute, the method of che
41、mical analysis shall be agreed between the manufacturer and purchaser preferably using existing chemical analysis standards. The measured chemical composition shall be stated on the inspection certificate. 2 per cast 2 per cast 2 Chemical composition Specific requirements for hydrogen content: The h
42、ydrogen content shall be determined on each batch in the delivery condition in accordance with EN 3976. 1 per cast 1 per cast 3 Method of meltingMethod of melting shall consist of Cold Hearth (Electron Beam or Plasma Arc) and/or Consumable Electrode Vacuum Arc Melting. An initial non-consumable elec
43、trode melt is allowed provided a water-cooled copper electrode is used. Some of the following requirements depend on whether the melting method includes Cold Hearth. 1 Raw material: Raw materials shall be purchased only from suppliers approved by the manufacturer and registered in his list of approv
44、ed suppliers. Approval of suppliers shall be made in accordance with written procedures contained within the quality assurance system of the manufacturer. Titanium sponge and alloying elements: The requirements shall be specified by the manufacturer who shall also establish the following procedures
45、for the evaluation and acceptance testing of each batch. titanium sponge: manufacturing method, level of impurities, particle size, freedom from surface contamination ; alloying elements: chemical composition including level of impurities, particle size, freedom from foreign particles. continued prE
46、N 4800-007:2009(E)9Table 1 Technical requirements for lines 1 to 29, where appropriate (continued) Frequency of testing Material standard line reference No. Title Requirements Qualification Release Recycling of scrap: See EN 2955. The categories and sub-categories of scrap which may be used by the m
47、anufacturer are given in the following table: Scrap categories and sub-categories (See EN 2955) Melting method which includes cold hearth VAR-only melt method 1 allowed allowed 2 allowed Allowed 3 allowed allowed 4.1 allowedaalloweda4.2.1 allowed aballoweda4.2.2 allowed abnot alloweda4.3.1 allowed a
48、ballowed a4.3.2 allowedabnot alloweda3 Method of melting (continued) 5.1 allowed allowed 5.2 not allowed not allowed 6 not allowed not allowed aOnly turnings produced by the melter shall be used, unless otherwise agreed by the purchaser. bX-ray inspection not required. Bolts or used components shall
49、 not be used. The manufacturer shall maintain a list of his approved scrap processors. The list shall indicate the categories of scrap for which the processors are approved. Each order for scrap shall refer to EN 2955, specify the category and, if necessary, the sub-category of the scrap. In the case of turnings the limits for O2, C and H2shall also be specified. continued prEN 4800-007:2009 (E) 10 Table 1 Technical requirements for lines 1 to 29, where
