1、Designation: A 596/A 596M 95 (Reapproved 2004)1Standard Test Method forDirect-Current Magnetic Properties of Materials Using theBallistic Method and Ring Specimens1This standard is issued under the fixed designationA596/A596M; the number immediately following the designation indicates the yearof ori
2、ginal adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval.A superscript epsilon () indicates an editorial change since the last revision or reapproval.1NOTEMercury warning was editorially added in January 2009.1. Scope1.1 Thi
3、s test method covers dc ballistic testing for thedetermination of basic magnetic properties of materials in theform of ring, toroidal, link, double-lapped Epstein cores, orother standard shapes which may be cut, stamped, machined,or ground from cast, compacted, sintered, forged, or rolledmaterials.
4、It includes tests for normal induction and hysteresistaken under conditions of steep wavefront reversals of thedirect-current magnetic field strength.1.2 This test method shall be used in conjunction withPractice A 34/A 34M.1.3 This test method is suitable for a testing range from verylow magnetic f
5、ield strength up to 200 or more Oe 15.9 or morekA/m. The lower limit is determined by integrator sensitivityand the upper limit by heat generation in the magnetizingwinding. Special techniques and short duration testing mayextend the upper limit of magnetic field strength.1.4 Testing under this test
6、 method is inherently more accu-rate than other methods. When specified dimensional or shaperequirements are observed, the measurements are a goodapproximation to absolute properties.Test accuracy available isprimarily limited by the accuracy of instrumentation.1.5 This test method permits a choice
7、of test specimen topermit measurement of properties in any desired directionrelative to the direction of crystallographic orientation withoutinterference from external yoke systems.1.6 The symbols and abbreviated definitions used in this testmethod appear in Fig. 1 and Sections 5, 6, 9, and 10. For
8、theofficial definitions see Terminology A 340. Note that the termflux density used in this document is synonymous with the termmagnetic induction.1.7 WarningMercury has been designated by EPA andmany state agencies as a hazardous material that can causecentral nervous system, kidney, and liver damag
9、e. Mercury, orits vapor, may be hazardous to health and corrosive tomaterials. Caution should be taken when handling mercury andmercury-containing products. See the applicable product Ma-terial Safety Data Sheet (MSDS) for details and EPAs website(http:/www.epa.gov/mercury/faq.htm) for additional in
10、forma-tion. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited bystate law.1.8 The values stated in either customary (cgs-emu andinch-pound) units or SI units are to be regarded separately asstandard. Within this test method, the SI un
11、its are shown inbrackets except for the sections concerning calculations wherethere are separate sections for the respective unit systems. Thevalues stated in each system are not exact equivalents; there-fore, each system shall be used independently of the other.Combining values from the two systems
12、 may result in noncon-formance with this method.1.9 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of reg
13、ulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:A 34/A 34M Practice for Sampling and Procurement Test-ing of Magnetic Materials2A 340 Terminology of Symbols and Definitions Relating toMagnetic Testing2A 341/A 341M Test Method for Direct Current MagneticProperties of Materi
14、als Using dc Permeameters and theBallistic Test Methods2A 343/A 343M Test Method for Alternating-Current Mag-netic Properties of Materials at Power Frequencies Usingthe Wattmeter-Ammeter-Voltmeter Method and 25-cm Ep-stein Test Frame2A 773/A 773M Test Method for dc Magnetic Properties of1This test m
15、ethod is under the jurisdiction of ASTM Committee A06 onMagnetic Properties and is the direct responsibility of SubcommitteeA06.01 on TestMethods.Current edition approved Oct. 1, 2004. Published October 2004. Originallyapproved in 1969. Last previous edition approved in 1999 as A 596/A 596 95(1999).
16、2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box
17、C700, West Conshohocken, PA 19428-2959, United States.Materials Using Ring and Permeameter Procedures withdc Electronic Hysteresigraphs22.2 IEC Standard:Publication 404-4, Magnetic MaterialsPart 4: Methods ofMeasurement of the D-C Magnetic Properties of SolidSteels, IEC, 198233. Significance and Use
18、3.1 Test methods using suitable ring-type specimens4arethe preferred methods of determining the basic magneticproperties of a material caused by the absence of demagnetiz-ing effects and are well suited for specification acceptance,service evaluation, and research and development.3.2 Provided the te
19、st specimen is representative of the bulkmaterial as is usually the case for thin strip and wire, this testis also suitable for design purposes.3.3 When the test specimen is not necessarily representativeof the bulk material such as a ring machined from a largeforging or casting, the results of this
20、 test method may not be anaccurate indicator of the magnetic properties of the bulkmaterial. In such instances, the test results when viewed incontext of past performance history will be useful for judgingthe suitability of the current material for the intended applica-tion.4. Interferences4.1 This
21、test method has several important requirements.Unless adequate inside diameter to outside diameter ratios aremaintained in the test specimens, the magnetic field strengthwill be excessively nonuniform throughout the test specimenand the measured parameters cannot be represented as materialproperties
22、.4.2 The basic quality of materials having directionallysensitive properties cannot be tested satisfactorily with rings orlaminations. With them it is necessary to use Epstein speci-mens cut with their lengths in the direction of specific interestor to use long link-shaped or spirally wound toroidal
23、 core testspecimens whose long dimensions are similarly located. Theacceptable minimum width of strip used in such test specimensis also sensitive to the material under test. At present, it isbelieved that the grain-oriented silicon steels should have astrip width of at least 3 cm 30 mm.4.3 Unless r
24、ing specimens are large in diameter, it is difficultto provide a sufficient number of primary turns needed to reachthe highest magnetic field strength. In general, magneticmaterials tend to have nonuniform properties throughout thebody of the test specimen; for this reason, uniformly distrib-uted te
25、st windings and uniform specimen cross-sectional areaare highly desirable to suppress nonuniform behavior to atolerable degree.5. Apparatus5.1 The apparatus shall consist of as many of the compo-nents described in 5.2-5.10 as are required to perform thedesired test. The basic circuit is shown in Fig
26、. 1.5.2 Balance and Scales:5.2.1 The balance used to weigh the test specimen shall becapable of weighing to an accuracy of better than 0.1 %.5.2.2 The micrometer, caliper, or other length-measuringdevice used in the determination of magnetic path length andcross-sectional area shall be capable of me
27、asuring to anaccuracy of better than 0.1 %.5.3 dc Power SupplyThe preferred source of dc current isa high quality linear power supply of either unipolar or bipolaroperation. The power supply must exhibit high stability andvery low ripple to achieve the most accurate results. Program-mable bipolar op
28、erational amplifier power supplies haveproven to be very satisfactory for this type of testing. Otherstable sources of dc current such as storage batteries arepermitted.5.4 Main-Current-Control Rheostat R1When nonpro-grammable sources of dc current such as storage batteries areused, rheostats must b
29、e used to control the current. Theserheostats must have sufficient power rating and heat-dissipatingcapability to handle the largest test current without undesirablechanges in resistance and, therefore, magnetizing currentduring conduct of the test.5.5 Hysteresis-Current-Control Rheostat R2Thehyster
30、esis-current-control rheostat, when required, must havethe same power rating and resistance as the main-current-control rheostat.5.6 Main-Current Ammeter A1Measurement of the mag-netizing current can be accomplished with either a dc ammeter3Available from American National Standards Institute (ANSI)
31、, 25 W. 43rd St.,4th Floor, New York, NY 10036.4Lloyd, M. G., “Errors in Magnetic Testing with Ring Specimens, TechnicalNews Bulletin, National Institute for Standards and Technology, Vol 5, 1909, p. 435(S108).NOTE 1A1Multirange ammeter, main-magnetizing current circuitA2Multirange ammeter, hysteres
32、is-current circuitN1Magnetizing (primary) windingN2Flux-sensing (secondary) windingFElectronic integratorR1Main current control rheostatR2Hysteresis current control rheostatS1Reversing switchS2Shunting switch for hysteresis current control rheostatFIG. 1 Basic Circuit Using Ring-Type CoresA 596/A 59
33、6M 95 (2004)12or a combination of a precision shunt resistor and dc voltmeter.The meters and shunt resistor, if used, must have an accuracyof at least 0.25 %. To improve test accuracy multirange digitalammeters or voltmeters are preferred. Autoranging capabilityis desirable for convenience but is no
34、t essential for this testmethod. If analog meters are used, the ranges must be such thatall test readings are made in the upper two thirds of the scale.5.7 Hysteresis-Current Ammeter, A2The hysteresis-current measuring system shall conform to the requirements in5.6. In general, a separate measuring
35、system is not requiredsince the main current ammeter (A1) can also be used tomeasure the hysteresis current.5.8 Reversing Switch, S1Because of the low resistancenature of the magnetizing circuit, it is imperative that highquality switches be used. Changes in switch resistance uponreversal will cause
36、 deviation from the cyclically magnetizedcondition which, if excessive, will impair test accuracy andprecision. Experience has shown that mercury switches are thebest suited for this application. Knife blade switches ormechanical or electrically operated contractors can also beused provided the requ
37、irement for uniform and equal contactresistance can be maintained. Because of the presence ofleakage currents in the open condition, solid state relays are notpermitted. The difficulties inherent in the use of main currentreversing switches can be minimized by use of linear powersupplies capable of
38、accepting a remote programming signal.Such power supplies are permitted provided that the magne-tizing current is equal (to within 0.1 %) in either polarity whennormal induction testing is conducted, current reversals can beconducted with no overshoot or oscillation and the magnetizingcurrent is tru
39、ly zero for the zero current programming signal.5.9 Hysteresis Switch, S2(When Required)This switchshould conform to requirements in 5.8.5.10 Integrator, FBecause of their superior accuracy,stability, and ease of operation, electronic charge integratorsare the preferred means of measuring magnetic f
40、lux. Integra-tors using either operational amplifier and capacitor feedback(analog integrator) or pulse counting are permitted. The accu-racy of the integrator must be better than 1 % full scale. Ifanalog display meters are used to read the value of flux, themeasurement should be made on the upper t
41、wo thirds of thescale. Analog integrators must have drift adjust circuitry andthe drift should not exceed 100 Maxwell-turns 106Wb-turnsper minute on the most sensitive range. It is also desirable thatthe integrator have appropriate scaling circuitry to permit directreading of either flux (f) or flux
42、 density (B). Ballistic galva-nometers or moving coil fluxmeters are allowed provided the1 % full-scale accuracy requirement is met.6. Test Specimen6.1 When the test specimen represents a test lot of material,its selection shall conform to the requirements of PracticeA 34/A 34M or of an individual s
43、pecification.6.2 To qualify as a test specimen suitable for evaluation ofmaterial properties the effective ratio of mean diameter toradial width shall be not less than 10 to 1 (or an inside diameterto outside diameter ratio not less than 0.82). When the testspecimen has smaller ratios than the above
44、 requirements, thetest results should not be represented as material properties butshould be called core properties because of nonuniform fluxdistribution.6.3 When link, oval-shaped, or rectangular test specimenforms are used, the requirements of 6.2 apply to the end orcorner sections where flux cro
45、wding occurs. When straight-sided test specimens are very long relative to the length of thecorner or end sections, they are suitable for basic materialproperties evaluation with relatively unoriented materials pro-vided the uncertainty in determination of true-path (effective)length is less than 5
46、% of the total path length. When thisuncertainty in path length (shortest or longest relative to themean-path length) exceeds 5 %, the test values should bereported as core properties and not basic material properties.6.4 The test specimen may be constructed of solid laminatedor strip materials and
47、in any of the shapes described in 1.1.6.5 Test specimen cores made from strip may be laminated,machined, spirally wound, or Epstein specimens (the methodof selection for Epstein specimens is described in Test MethodA 343/A 343M,Appendix 3). When the material is to be testedhalf transverse and half l
48、ongitudinal, the material shall be cutinto Epstein strips or square laminations of adequate dimen-sional ratio.6.6 Test specimens used for basic material evaluation shallbe cut, machined, ground, slit, or otherwise formed to have across section that remains sufficiently uniform that its nonuni-formi
49、ty will not materially affect the accuracy of establishingand measuring flux density, B, or magnetic field strength, H,inthe test specimen.6.7 When required for material properties development, thetest specimen shall have received a stress relief or other heattreatment after preparation. This heat treatment is subject toagreement between manufacturer and purchaser, manufacturersrecommendation, or the recommended heat treatment providedby the appropriate ASTM standard for the material. The heattreatment used shall be reported with the magnetic test
