1、Designation: B335 03 (Reapproved 2013)Standard Specification forNickel-Molybdenum Alloy Rod1This standard is issued under the fixed designation B335; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A numb
2、er in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This specification2covers rod of nickel-molybdenumalloys (
3、UNS N10001, N10665, N10675, N10629, andN10624)* as shown in Table 1, for use in general corrosiveservice.1.2 The following products are covered under this specifi-cation:1.2.1 Rods516 to34 in. (7.94 to 19.05 mm) excl in diameter,hot or cold finished, solution annealed and pickled or mechani-cally de
4、scaled.1.2.2 Rods34 to 312 in. (19.05 to 88.9 mm) incl in diameter,hot or cold finished, solution annealed, ground or turned.1.3 The values stated in inch-pound units are to be regardedas standard. The values given in parentheses are mathematicalconversions to SI units that are provided for informat
5、ion onlyand are not considered standard.1.4 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to become familiarwith all hazards including those identified in the appropriateMaterial Safety Data
6、Sheet (MSDS) for this product/materialas provided by the manufacturer, to establish appropriatesafety and health practices, and determine the applicability ofregulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:3B880 Specification for General Requirements for ChemicalCheck A
7、nalysis Limits for Nickel, Nickel Alloys andCobalt AlloysE8 Test Methods for Tension Testing of Metallic MaterialsE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsE55 Practice for Sampling Wrought Nonferrous Metals andAlloys for Determination of Chemi
8、cal CompositionE1473 Test Methods for Chemical Analysis of Nickel,Cobalt, and High-Temperature Alloys3. Terminology3.1 Definitions of Terms Specific to This Standard:3.1.1 rod, na product of round solid section furnished instraight lengths.4. Ordering Information4.1 It is the responsibility of the p
9、urchaser to specify allrequirements that are necessary for material ordered under thisspecification. Examples of such requirements include, but arenot limited to the following:4.1.1 AlloyTable 1.4.1.2 DimensionsNominal diameter and length. Theshortest usable multiple length shall be specified (Table
10、 2).4.1.3 CertificationState if certification or a report of testresults is required (Section 16).4.1.4 Purchaser InspectionState which tests or inspec-tions are to be witnessed (Section 13).4.1.5 Samples for Product (Check) AnalysisState whethersamples should be furnished (9.2.2).5. Chemical Compos
11、ition5.1 The material shall conform to the composition limitsspecified in Table 1.5.2 If a product (check) analysis is made by the purchaser,the material shall conform to the requirements specified inTable 1 subject to the permissible tolerances in B880.6. Mechanical Properties and Other Requirement
12、s6.1 The mechanical properties of the material at roomtemperature shall conform to those shown in Table 3.1This specification is under the jurisdiction of ASTM Committee B02 onNonferrous Metals and Alloys and is the direct responsibility of SubcommitteeB02.07 on Refined Nickel and Cobalt and Their A
13、lloys.Current edition approved Feb. 1, 2013. Published February 2013. Originallyapproved in 1958. Last previous edition approved in 2008 as B335 03 (2008).DOI: 10.1520/B0335-03R13.2For ASME Boiler and Pressure Vessel Code applications see related Specifi-cation SB-335 in Section II of that Code.* Ne
14、w designation established in accordance with ASTM E527 and SAE J1086,Recommended Practice for Numbering Metals and Alloys (UNS).3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume informatio
15、n, refer to the standards Document Summary page onthe ASTM website.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States17. Dimensions and Permissible Variations7.1 DiameterThe permissible variations from the speci-fied diameter shall be as
16、 prescribed in Table 2.7.2 Out of RoundnessThe permissible variation in round-ness shall be as prescribed in Table 2.7.3 Machining AllowancesWhen the surfaces of finishedmaterial are to be machined, the following allowances aresuggested for normal machining operations.7.3.1 As-finished (Annealed and
17、 Descaled)For diametersof516 to1116 in. (7.94 to 17.46 mm) incl., an allowance of116in. (1.59 mm) on the diameter should be made for finishmachining.7.4 Length:7.4.1 Unless multiple, nominal, or cut lengths are specified,random mill lengths shall be furnished.7.4.2 The permissible variations in leng
18、th of multiple,nominal, or cut length rod shall be as prescribed in Table 4.Where rods are ordered in multiple lengths, a14-in. (6.35-mm)length addition shall be allowed for each uncut multiple length.7.5 Ends:7.5.1 Rods ordered to random or nominal lengths shall befurnished with either cropped or s
19、awed ends.7.5.2 Rods ordered to cut lengths shall be furnished withsquare saw-cut or machined ends.7.6 WeightFor calculations of mass or weight, the follow-ing densities shall be used:DensityAlloy lb/in3g/cm3N10001 0.334 9.24N10665 0.333 9.22N10675 0.333 9.22N10629 0.333 9.22N10624 0.322 8.97.7 Stra
20、ightnessThe maximum curvature (depth of chord)shall not exceed 0.050 in. multiplied by the length of the chordin feet (0.04 mm multiplied by the length in centimetres).8. Workmanship, Finish, and Appearance8.1 The material shall be uniform in quality and condition,smooth, and free of injurious imper
21、fections.9. Sampling9.1 Lots for Chemical Analysis and Mechanical Testing:9.1.1 A lot for chemical analysis shall consist of one heat.9.1.2 A lot of bar for mechanical testing shall be defined asthe material from one heat in the same condition and specifieddiameter.9.2 Sampling for Chemical Analysis
22、:9.2.1 A representative sample shall be obtained from eachheat during pouring or subsequent processing.9.2.2 Product (check) analysis shall be wholly the respon-sibility of the purchaser.9.3 Sampling for Mechanical Testing:9.3.1 Arepresentative sample shall be taken from each lot offinished material
23、.10. Number of Tests and Retests10.1 Chemical AnalysisOne test per heat.10.2 Tension TestsOne test per lot.10.3 RetestsIf the specimen used in the mechanical test ofany lot fails to meet the specified requirements, two additionalspecimens shall be taken from different sample pieces andtested. The re
24、sults of the tests on both of these specimens shallmeet the specified requirements.11. Specimen Preparation11.1 Tension test specimens shall be taken from materialafter final heat-treatment and tested in the direction of fabri-cation.11.2 Tension test specimens shall be any of the standard orsubsize
25、d specimens shown in Test Methods E8.11.3 In the event of disagreement, the referee specimenshall be the largest possible round specimen shown in TestMethods E8.12. Test Methods12.1 The chemical composition and mechanical propertiesof the material as enumerated in this specification shall bedetermin
26、ed, in case of disagreement, in accordance with thefollowing ASTM methods:12.1.1 Chemical AnalysisTest Methods E1473. For ele-ments not covered by Test Methods E1473, the referee methodshall be as agreed upon between the manufacturer and theTABLE 1 Chemical RequirementsElementComposition Limits, %Al
27、loyN10001AlloyN10665AlloyN10675AlloyN10629AlloyN10624Nickel remainderAremainderA65.0 min remainderABalMolybdenum 26.030.0 26.030.0 27.032.0 26.030.0 21.0-25.0Iron 4.06.0 2.0 max 1.03.0 1.06.0 5.0-8.0Chromium 1.0 max 1.0 max 1.03.0 0.51.5 6.0-10.0Carbon,max0.05 0.02 0.01 0.01 0.01Silicon, max 1.0 0.1
28、0 0.10 0.05 0.10Cobalt, max 2.5 1.00 3.0 2.5 1.0Manganese,max1.0 1.0 3.0 1.5 1.0Phosphorus,max0.04 0.04 0.030 0.04 0.025Sulfur, max 0.03 0.03 0.010 0.01 0.01Vanadium 0.20.4 . 0.20 max . .Nickel plusMolybdenum. . 94.098.0 .Aluminum . . 0.50 max 0.10.5 0.5Columbium(Nb), max. . 0.20 .Copper, max . . 0.
29、20 0.5 0.5Tantalum,max. . 0.20 .Titanium,max. . 0.20 .Tungsten,max. . 3.0 .Zirconium,max. . 0.10 .Magnesium,max. . . . .ASee 12.1B335 03 (2013)2purchaser. The nickel composition shall be determined arith-metically by difference.12.1.2 Tension TestTest Methods E8.12.1.3 Method of SamplingPractice E55
30、.12.1.4 Determining Significant PlacesPractice E29.12.2 For purposes of determining compliance with thelimits in this specification, an observed value or a calculatedvalue shall be rounded as indicated below, in accordance withthe rounding method of Practice E29:RequirementsRounded Unit for Observed
31、 orCalculated ValueChemical composition and tolerance Nearest unit in the last right-handplace of figures of the specifiedlimitTensile strength and yield strength nearest 1000 psi (7 MPa)Elongation nearest 1 %13. Inspection13.1 Inspection of the material shall be made as agreed uponby the manufactur
32、er and the purchaser as part of the purchasecontract.14. Rejection and Rehearing14.1 Material tested by the purchaser that fails to conform tothe requirements of this specification may be rejected. Rejec-tion should be reported to the producer or supplier promptlyand in writing. In case of dissatisf
33、action with the results of thetest, the producer or supplier may make claim for a rehearing.15. Certification15.1 When specified in the purchase order or contract, amanufacturers certification shall be furnished to the purchaserstating that material has been manufactured, tested, and in-spected in a
34、ccordance with this specification, and that the testresults on representative samples meet specification require-ments. When specified in the purchase order or contract, areport of the test results shall be furnished.16. Product Marking16.1 Each piece of material12 in. (12.7 mm) and over indiameter
35、shall be marked with the specification number, alloy,heat number, manufacturers identification, and size. Themarkings shall have no deleterious effect on the material or itsperformance and shall be sufficiently stable to withstandnormal handling.16.2 Each bundle or shipping container shall be marked
36、with the name of the material; this specification number; alloy;the size; gross, tare, and net weight; consignor and consigneeaddress; contract or order number; and such other informationas may be defined in the contract or order.17. Keywords17.1 rod; N10001; N10624; N10629; N10665; N10675TABLE 2 Pe
37、rmissible Variations in Diameter and Out-of-Roundness of Finished RodsSpecified Diameter,in. (mm)Permissible Variations, in. (mm)Diameter Out of Roundness,maxPlus MinusHot-Finished, Annealed, and Descaled Rods516 to716 (7.9411.11), incl 0.012 (0.30) 0.012 (0.30) 0.018 (0.46)Over716 to58 (11.1115.87)
38、, incl 0.014 (0.36) 0.014 (0.36) 0.020 (0.51)Over58 to34 (15.8719.05), excl 0.016 (0.41) 0.016 (0.41) 0.024 (0.61)Hot-Finished, Annealed, and Ground or Turned Rods34 to 312 (19.0588.9), incl 0.010 (0.25) 0 0.008 (0.20)TABLE 3 Mechanical PropertiesAlloy Thickness, in. (mm)Tensile Strength,min, psi (M
39、Pa)Yield Strength(0.2 % Offset),min, psi (MPa)Elongation in 2in. (50 mm) or4DA, min %Rockwell Hardness,maxN10001516 to 112 (7.94 to 38.1) incl 115 000 (795) 46 000 (315) 35Over 112 to 312 (38.1 to 88.9) incl 100 000 (690) 46 000 (315) 30N10665516 to 312 (7.94 to 88.9) incl 110 000 (760) 51 000 (350)
40、 40N10675516 to 312 (7.94 to 88.9) incl 110 000 (760) 51 000 (350) 40N10629516 to 312 (7.94 to 88.9) incl 110 000 (760) 51 000 (350) 40 100 HRBN10624516 to 312 in. (7.94 to 88.9 mm), incl 104 000 (720) 46 000 (320) 40 100 HRBAD refers to the diameter of the tension specimen.TABLE 4 Permissible Varia
41、tions in Length of RodsRandom milllengths2 to 12 ft (610 to 3660 mm) long with not more than 25weight % under 4 ft (1.22 m).Multiple lengths Furnished in multiples of a specified unit length, within thelength limits indicated above. For each multiple, anallowance of14 in. (6.35 mm) shall be made for
42、 cutting,unless otherwise specified. At the manufacturers option,individual specified unit lengths may be furnished.Nominal lengths Specified nominal lengths having a range of not less than2 ft (610 mm) with no short lengths allowed.Cut lengths A specified length to which all rods shall be cut with
43、apermissible variation of +18 in. (3.17 mm) 0.B335 03 (2013)3APPENDIX(Nonmandatory Information)X1. HEAT TREATMENTX1.1 Proper heat treatment during or subsequent to fabrica-tion is necessary for optimum performance, and the manufac-turer shall be consulted for details.ASTM International takes no posi
44、tion respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibili
45、ty.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to AST
46、M International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address
47、shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).B335 03 (2013)4
