1、Designation: C1164 92 (Reapproved 2009)Standard Practice forEvaluation of Limestone or Lime Uniformity From a SingleSource1This standard is issued under the fixed designation C1164; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, t
2、he year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice is intended for use in instances where thepurchaser desires information on the uniformity of
3、limestone orlime produced at a single source. It is intended that this testmethod normally be used for the predominant material manu-factured at a plant. Guidelines for sampling, testing andpresentation of results (Table 1) are given.1.2 The values stated in inch-pound units are to be regardedas sta
4、ndard. The values given in parentheses are mathematicalconversions to SI units that are provided for information onlyand are not considered standard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this s
5、tandard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2C25 Test Methods for Chemical Analysis of Limestone,Quicklime, and Hydrated LimeC50 Practice for Sampling, Sample Preparati
6、on, Packaging,and Marking of Lime and Limestone ProductsC51 Terminology Relating to Lime and Limestone (as usedby the Industry)C110 Test Methods for Physical Testing of Quicklime,Hydrated Lime, and LimestoneC141 Specification for Hydraulic Hydrated Lime for Struc-tural Purposes3. Terminology3.1 Defi
7、nitions:3.1.1 For definitions of terms relating to this practice refer toTerminology C51.4. Significance and Use4.1 This practice is designed to present in a standardizedformat information on the variability of limestone or lime froma single source over a period of time. It can be applied to allmate
8、rials covered in Test Methods C25 and C110, and Speci-fication C141.5. Sampling5.1 The sampling shall be done in accordance with MethodsC50.5.2 All sampling shall be performed by personnel qualifiedby specific training for this purpose.1This practice is under the jurisdiction of ASTM Committee C07 o
9、n Lime andis the direct responsibility of Subcommittee C07.05 on Chemical Tests.Current edition approved Dec. 1, 2009. Published May 2010. Originallyapproved in 1990. Last previous edition approved in 2003 as C1164 92 (2003).DOI: 10.1520/C1164-92R09.2For referenced ASTM standards, visit the ASTM web
10、site, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.TABLE 1 High Calcium Quicklime January 1989NOTE 1This data is presented only as a sample of the correct methodf
11、or presentation. Other tests can be substituted and others omitted.DayTestAcid Insoluble % CaO % MgO Available CaO1 0.66 95.85 2.27 94.902 0.84 95.03 2.87 94.083 1.24 95.85 1.57 94.904 1.22 96.67 1.49 95.715 1.22 96.26 1.32 95.318 0.68 95.85 2.06 94.699 0.96 95.54 2.27 94.8910 1.26 96.15 1.74 95.201
12、1 1.04 96.04 2.00 95.1113 1.26 96.26 1.51 95.3115 1.34 95.23 2.09 94.2816 1.28 95.44 2.34 94.6919 0.68 96.15 1.46 95.2020 1.42 95.85 1.27 94.9022 1.06 95.85 1.86 94.9023 0.58 96.15 2.09 95.3124 0.84 95.03 2.61 94.0826 1.28 95.64 1.39 94.6927 1.48 95.54 1.58 94.3929 0.98 94.82 2.71 93.6730 1.24 94.41
13、 3.42 93.67Avg 1.07 95.70 2.00 94.76Range 0.90 2.26 2.15 2.04Std Dev 0.26 0.54 0.56 0.541Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.5.3 Data points shall be an average of three or more separatedeterminations relative to a specifi
14、ed unit of time. For example:(1) n determinations for daily average, (2) daily determinationsfor weekly average.5.4 The samples shall be identified by the date or dates thatthe represented material was obtained.6. Procedure6.1 The minimum amount of testing (see 5.3) and the typeof test(s) to be perf
15、ormed should be agreed upon by thepurchaser and producer.NOTE 1A single daily analysis does not necessarily characterize aproduct. A minimum of three analyses is more reasonable.6.2 It is desirable that all tests used in a single evaluation beperformed in the same laboratory, preferably by the samep
16、erson, in order for the results to be comparable.NOTE 2In order to obtain comparable results when exchangingsamples between laboratories, methods used in preparation, handling andstorage of those samples must be uniform.6.2.1 When separate evaluations of a single source are madeby two or more labora
17、tories, additional tests of a standardmaterial or exchanged portions of the same sample may benecessary to determine differences in testing that are likely tobe obtained in the different laboratories. Three or more batchesmay be necessary to obtain comparison between laboratories.6.2.2 Where a withi
18、n-laboratory testing standard deviationhistory has not been established, duplicate tests made from asingle sample are required to determine the effect of testingvariation on the uniformity of results made in a singlelaboratory.7. Test Method7.1 The chemical analysis of quicklime, hydrated lime, andl
19、imestone shall be determined in accordance with Test MethodsC25.7.2 The physical analysis of quicklime, hydrated lime, andlimestone shall be determined in accordance with Test MethodsC110.7.3 The analysis of hydraulic hydrated lime shall be deter-mined in accordance with Specification C141.8. Calcul
20、ation8.1 Average X:X5X11 X21 .1 Xn!n(1)where:X1,X2,.,Xn= the individual test results in accordancewith Test Methods C25 or C110,orSpecification C141, andn = the number of individual samples.8.2 Total Standard Deviation:s 5X12 X!21 X22 X!21 .1 Xn2 X!2n 2 1!(2)9. Report9.1 Report the following informa
21、tion. Sufficient informationshall be provided to identify the sample including:9.1.1 Name of manufacturer and location,9.1.2 Type of material or other identification,9.1.3 All sampling and analytical practices used are to benoted (see Note 3), and9.1.4 Period of time represented by the report.9.2 Th
22、e report shall not cover a period of time greater thanone year.NOTE 3Laboratory designations are lost or are meaningless whenaveraging a number of determinations on individual samples. The pur-chaser needs to know the sampling and analytical practices used ingenerating a report to properly evaluate
23、the information they receiveconcerning a specific product.10. Keywords10.1 hydrated lime; limestone; product uniformity; quick-lime; samplingASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this
24、 standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five year
25、s andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committ
26、ee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428
27、-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).C1164 92 (2009)2
