1、Designation: C537 87 (Reapproved 2014)1Standard Test Method forReliability of Glass Coatings on Glassed Steel ReactionEquipment by High Voltage1This standard is issued under the fixed designation C537; the number immediately following the designation indicates the year oforiginal adoption or, in the
2、 case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1NOTEIntroduction added and unit abbreviation corrections made editorially in June 2014.INTRODUCTIO
3、NThis test method covers the determination of the reliability of glass coating on metal using highvoltage. It is intended for use by manufacturers of equipment that is designed to withstand highlycorrosive conditions where a failure of the coating in service would cause extreme damage to theexposed
4、metal. The test method detects not only existing discontinuities in the glass coating, but alsoareas where the glass coating may be thin enough to be likely to result in premature failure in service.1. Scope1.1 This test method covers the determination of the reli-ability of glass coating on metal a
5、nd is intended for use bymanufacturers of equipment that is designed to withstandhighly corrosive conditions where a failure of the coating inservice would cause extreme damage to the exposed metal. Itsuse outside the manufacturers plant is discouraged becauseimproper or indiscriminate testing can c
6、ause punctures that aredifficult to repair without returning the equipment to themanufacturers plant. This test method detects not only exist-ing discontinuities in the glass coating, but also areas where theglass may be thin enough to be likely to result in prematurefailure in service.1.2 The value
7、s stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safe
8、ty and health practices and determine the applica-bility of regulatory limitations prior to use. For specificprecautionary statements, see Section 7.2. Terminology2.1 Definitions:2.1.1 glassed steel, glass-lined steel, or glass-coated steeldesignations generally applied to a class of porcelain ename
9、lsthat have high resistance to chemical attack at elevatedtemperatures and pressures.3. Summary of Test Method3.1 This test method consists essentially of grounding themetal structure of the equipment to the ground side of adirect-current high-voltage generator and sweeping the glasssurface with a h
10、igh-potential probe on the end of an insulatedhandle and cable. Wherever a discontinuity exists or thecoating is thin enough (by reason of a concealed bubble orconducting inclusion, etc.) so that the dielectric strength of theremaining glass is less than some preset desired amount, thedielectric str
11、ength of air-plus-remaining-glass breaks down anda discharge occurs. Built-in current-limiting devices ensureelectrical safety to the operator. A variable voltage controlallows selection of a voltage which assures a predeterminedminimum thickness of glass.4. Significance and Use4.1 The widespread us
12、e of glassed-steel equipment in highlycorrosive chemical processes has made it necessary to detectweak spots in the coating and repair them before catastrophicfailure occurs in service. This test is intended to detectdiscontinuities and thin areas in a glass coating on metal toensure that the coatin
13、g is defect free and has sufficientthickness to withstand the prescribed service conditions. A testvoltage may be selected at any desired value up to 20k V, thusmaking the test applicable to a wide range of thicknessrequirements. When, because of bubbles or defects, the thick-ness of glass at any sp
14、ot is less than enough to withstand theapplied voltage, a puncture results with an accompanying1This test method is under the jurisdiction ofASTM Committee B08 on Metallicand Inorganic Coatings and is the direct responsibility of Subcommittee B08.12 onMaterials for Porcelain Enamel and Ceramic-Metal
15、 Systems.Current edition approved May 1, 2014. Published June 2014. Originallyapproved in 1964. Last previous edition approved in 2009 as C537 87 (2009).DOI: 10.1520/C0537-87R14.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1indicati
16、on of a defect. Remedial action is then required torepair the defect before the equipment can be used forcorrosive service. (When such defects are found before theequipment leaves the manufacturers plant another applicationof glass can usually be applied and fired to become an integralpart of the co
17、ating.)5. Interferences5.1 Since the test method is electrical, it is necessary to havea good ground connection between the instrument and themetal substrate of the equipment being tested. It is alsonecessary that the surface of the glass be reasonably clean anddry. A wet surface will conduct enough
18、 of the high voltage toany exposed metal, including the edges of the glass coating, sothat an indication of a “contact” may be obtained over a largearea instead of at localized spots that can be marked andidentified for repair.6. Apparatus26.1 The tester is composed of a source of high-voltage direc
19、tcurrent with a suitable device to limit the current. A constant-voltage transformer is used to supply a more uniform voltagesource than the usual 115 V, 60 Hz line to which it isconnected. The power supply unit consists of a suitable step-uptransformer along with a voltage-control device, a current
20、-limiting rheostat, a rectifier, and appropriate safety and remotecontrol relays, meters, as well as an insulated cable and probe(see Fig. 1 for schematic wiring diagram). The current outputis limited to 2.5 mA. The output voltage is variable up to 20kV, and the level is indicated by a voltmeter. Th
21、e handle isinsulated and grounded and is designed to use either a wirebrush-type or a point probe. The brush probe is used forsweeping larger surfaces of glass coating while the point probeis better adapted to interior corners and the more restrictedareas.7. Safety Precautions7.1 The instrument and
22、equipment being tested should bewell grounded both to a good ground and to each other. Allgrounding contacts should be clean bare metal and not rustedor painted metal.7.2 Handle the insulated probe handle so that the handcontacts the ground ring to prevent build-up of a static chargewhich causes an
23、unpleasant (although not dangerous) sensationon discharge.7.3 Keep the probe electrode at least 305 mm (12 in.) awayfrom conducting surfaces or personnel. Remember that con-ducting surfaces may lead to personnel at some distance fromthe probe. Discharge the probe tip by grounding it after turningoff
24、 the instrument and before changing probe tips.Although thecurrent is low enough to be electrically safe, the involuntaryreaction from a surprise discharge might cause injury.7.4 Unless the surface to be tested is clean and dry, theremay be sufficient conduction along the surface to cause acapacitan
25、ce discharge even if there is no direct path to ground.Such a capacitance discharge is recognizable from a truefailure because the discharge spark is not confined to certainspots but is a general discharge to a large area of the moist glasssurface. Continuous application of the probe to such areasse
26、rves only to build up a capacitance charge on the surface ofthe vessel eventually resulting in a discharge through theoperator to his discomfort.7.5 A dc tester should never be used in a chemical plant fordiscontinuity testing because of the possibility that a capacitivecharge will be developed in t
27、he dielectric coating, resulting inan explosion hazard.8. Procedure8.1 The following procedure is applicable to commerciallyavailable test equipment:8.1.1 Install ground connections to the instrument and to theequipment to be tested. Provide a separate ground connectionbetween the instrument and the
28、 equipment.2When requesting information, specific reference should be made to the ASTMdesignation.FIG. 1 Circuit Diagram, 20k V dc TesterC537 87 (2014)128.1.2 Set the voltage-control knob near the minimumsetting, connect the instrument to the voltage stabilizer, andconnect the latter to the appropri
29、ate power line. Turn the poweron and allow the test equipment to warm up for 2 to 3 min toensure stabilization of the voltage.8.1.3 Engage the overload relay and then the “DC On”switch to apply voltage to the probe.8.1.4 Hold the probe by the handle with a firm grip on theground ring and with the el
30、ectrode well away from all objectsand personnel, and slowly raise the voltage until the voltmeterindicates the desired value. Maintain hand contact with theground ring of the handle all through the test to avoid a buildupof static electricity in the operator that might result in anuncomfortable and
31、annoying (although not dangerous) sparkdischarge. Pass the test probe across the coating surface at aspeed not to exceed 40 cm/s.NOTE 1The instrument is set to discharge across an internal gap atslightly over 20k V. If the voltage is set high enough to cause such adischarge, ionization of the air us
32、ually causes the arc to persist until thevoltage is reduced to approximately 5k V. Shortly after the arc hasextinguished, the voltage can be reset to the desired value.8.1.5 When a point of failure in the coating is approached,a spark will jump to the point of failure with a visible andaudible disch
33、arge or arc. As the path of the arc is shortened, bybringing the electrode close to the point of failure, the currentin the arc builds up.At a 2.5 mAcurrent in the arc, the overloadrelay will trip and the dc current will cut off. When thishappens it is necessary to engage first the overload relay an
34、dthen the “DC On” switch before the tester is again operative.8.1.6 Mark the point of failure with suitable chalk (orcrayon) for subsequent repair.9. Report9.1 The report shall include the following:9.1.1 Title of test, ASTM designation and issue,9.1.2 Date of test,9.1.3 Description or identificatio
35、n of equipment beingtested,9.1.4 Voltage used in the test, and9.1.5 Number and location of failures.10. Precision and Bias10.1 No justifiable statements can be made regarding theprecision and bias of this test method due to the fact that thismethod is designed for application to full-sized productio
36、nvessels and reactors with the result that variables due to design,metal composition, fabrication, and metal processing, as wellas porcelain enameling, are introduced into the results.11. Keywords11.1 glass coated steel equipment; glass coating; high volt-age test; porcelain enamel; reliability of c
37、oatingsASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such righ
38、ts, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional
39、standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM
40、Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).C537 87 (2014)13
