1、Designation: D 1151 00 (Reapproved 2006)Standard Practice forEffect of Moisture and Temperature on Adhesive Bonds1This standard is issued under the fixed designation D 1151; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year
2、of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This practice defines conditions
3、for determining theperformance of adhesive bonds when subjected to continuousexposure at specified conditions of moisture and temperature.The performance is expressed as a percentage based on theratio of strength retained after exposure to the original strength.1.2 The values stated in SI units are
4、to be regarded as thestandard. The values given in parentheses are provided forinformation purposes only.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and
5、 health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D 897 Test Method for Tensile Properties of AdhesiveBondsD 903 Test Method for Peel or Stripping Strength of Adhe-sive BondsD 906 Test Method for Strength Properties o
6、f Adhesives inPlywood Type Construction in Shear by Tension LoadingD 907 Terminology of AdhesivesD 1002 Test Method for Apparent Shear Strength of Single-Lap-Joint Adhesively Bonded Metal Specimens by Ten-sion Loading (Metal-to-Metal)3. Terminology3.1 DefinitionsMany of the terms in this practice ar
7、edefined in Terminology D 907.4. Significance and Use4.1 This practice may be used to determine the performance,for suitable materials, in terms of any desired strength propertyof adhesive bonds. Test conditions of temperature and moistureonly are here specified. The duration of exposure is dependen
8、tupon the nature of the adhesive and the type of specimens andwill, therefore, be covered by material specifications.5. Apparatus5.1 Conditioning Cabinets or Ovens, with temperature andhumidity control.6. Test Specimens6.1 Prepare the test specimens in accordance with therecommendations of the manuf
9、acturer of the adhesive. Thespecimens should be of a suitable form and number to meet therequirements of the investigation. The specimens should con-form in detail with the requirements prescribed in the ASTMtest method covering the desired strength property, as listed inSection 2, and any other AST
10、M test method pertaining tostrength properties of adhesives for the desired strength test.6.2 Matched specimens should be selected for control andexposure treatments, the number to be fixed by the variabilityinherent in the method.7. Conditioning7.1 PreconditioningCondition all specimens for 7 days
11、at50 6 2 % relative humidity and 23 6 1C (73.4 6 1.8F)immediately prior to exposure, or prior to testing in the case ofcontrol specimens. Prior history of the test specimens shouldbe known and recorded.7.2 Exposure ConditionsThe exposure conditions shouldconform to one of the standard test exposures
12、 given in Table 1.1Precision and Bias This practice is under the jurisdiction of ASTM CommitteeD14 onAdhesives and is the direct responsibility of Subcommittee D14.80 on MetalBonding Adhesives.Current edition approved Oct. 1, 2006. Published October 2006. Originallyapproved in 1951. Last previous ed
13、ition approved in 2000 as D 1151 00.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.1Copyright ASTM Internati
14、onal, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.8. Procedure8.1 Test the control specimens for strength by the appropri-ate test method immediately after the preconditioning period.Average the values obtained. Record this average as theoriginal strength agai
15、nst which the strength after exposure is tobe compared in calculating performance.8.2 Subject the preconditioned specimens to the designatedexposure conditions (Table 1) for the length of time prescribedby the specification for the adhesive being tested. At the end ofthe exposure period, test the sp
16、ecimens using one of thefollowing procedures:8.2.1 Test the specimens under conditions at which theywere exposed, or8.2.2 Condition the specimens for4hat506 2 % relativehumidity and 23 6 1C (73.4 6 1.8F) and test immediatelythereafter, or8.2.3 Condition the specimens for 7 days at 50 6 2%relative hu
17、midity and 23 6 1C (73.4 6 1.8F) and testimmediately thereafter.8.3 Average the strength values obtained and record thevalue as the average strength of the specimens after exposure.NOTE 1The conditions under which the exposed specimens are testedwill depend upon the nature of the adhesive, the adher
18、end, and the strengthproperty being investigated. This will be prescribed by the materialspecifications or by written agreement between the manufacturer andpurchaser of the adhesive.9. Calculation9.1 Calculate the performance of the adhesive under test, asfollows:Performance A 5 A/D! 3 100, (1)Perfo
19、rmance B 5 B/D! 3 100, (2)orPerformance C 5 C/D! 3 100. (3)where:A = average strength when tested under the designatedexposure condition in accordance with 8.2.1,B = average strength after exposure, when determined inaccordance with 8.2.2,C = average strength after exposure, when determined inaccord
20、ance with 8.2.3, andD = original strength, determined in accordance with 8.1.NOTE 2Alternative methods of expressing results may be used.10. Report10.1 Report the following:10.1.1 Complete identification of the adhesive tested, in-cluding type, source, manufacturers code number, form, andmethod of p
21、reparation for use,10.1.2 Bonding conditions used in preparing test specimens,and history of specimens prior to testing.10.1.3 Description of test specimens, including materials,size, shape, and designation of ASTM test method covering thedetailed requirements,10.1.4 Average thickness of adhesive la
22、yer after formationof the joint, within 0.001 in. The method of obtaining thethickness of the adhesive layer shall be described includingprocedure, location of measurements, and range of measure-ments.10.1.5 Test conditions used, any deviation from conditionslisted in Table 1, duration of exposure,
23、and condition ofspecimens at test (8.2.1 or 8.2.2).10.1.6 Number of specimens tested, strength of each speci-men, and average strength for both control and exposedspecimens, including the types of failure and amounts of eachtype, and10.1.7 Performance expressed as a percentage (Section 9).11.12. Key
24、words12.1 adhesive bonds; moisture; temperatureTABLE 1 Standard Test ExposuresTest ExposureNumberTemperatureAMoisture ConditionsC F1 57 70 as conditioned2 34 30 as conditioned3 34 30 presoakedB4 0 32 as conditioned5 23 73.4 50 % RH6 23 73.4 immersed in water7 38 100 88 % RH8 63 145 oven, uncontrolle
25、dhumidity9 63 145 over waterC10 63 145 immersed in water11 70 158 oven, uncontrolledhumidity12 70 158 over waterC13 82 180 oven, uncontrolledhumidity14 87 188 oven, uncontrolledhumidity15 82 180 over waterC16 100 212 oven, uncontrolledhumidity17 100 212 immersed in water18 105 221 oven, uncontrolled
26、humidity19 149 300 oven, uncontrolledhumidity20 204 400 oven, uncontrolledhumidity21 260 500 oven, uncontrolledhumidity22 316 600 oven, uncontrolledhumidityAThe tolerance for test temperature shall be 61C or 1.8F up to 82C or 180F,and 61 % for temperatures above 82C or 180F.BPresoaking shall consist
27、 of submerging specimens in water and applyingvacuum at 51 cm (20 in.) of mercury until weight equilibrium is reached.CThe relative humidity will ordinarily be 95 to 100 %.D 1151 00 (2006)2ASTM International takes no position respecting the validity of any patent rights asserted in connection with a
28、ny item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technica
29、l committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration
30、at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor
31、 Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org).D 1151 00 (2006)3
